Electrochemical polishing versus mechanical polishing of AISI 304: surface and electrochemical study
AISI 304 is essential for vital industries, e.g., aerospace, nuclear plants, pharmaceutical, chemical, and medical industries. Enhancement of AISI 304 surface characteristics is required for protection, durability, and better performance. Different methods were used for surface modification like mec...
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Published in | Journal of solid state electrochemistry Vol. 26; no. 1; pp. 121 - 129 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
Berlin/Heidelberg
Springer Berlin Heidelberg
2022
Springer Nature B.V |
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Abstract | AISI 304 is essential for vital industries, e.g., aerospace, nuclear plants, pharmaceutical, chemical, and medical industries. Enhancement of AISI 304 surface characteristics is required for protection, durability, and better performance. Different methods were used for surface modification like mechanical polishing (MP) and electrochemical polishing (EP). Scanning electron microscopy, atomic force microscopy, and gloss values revealed the alleviation of humps, imperfection and roughness, and leveling. Smoothness and brightening of the surface after EP (∆
R
= − 1.206 nm) was more than that of MP treatment (∆
R
= − 0.562 nm). Energy dispersive X-ray analysis showed increase of Cr, Ni, and Mn content while the content of Fe decreased after EP treatment. Potentiodynamic polarization of EP AISI 304 in 3.5% NaCl revealed a high polarization resistance (
R
p
= 2786 kΩ) and low corrosion rate of 2.74 × 10
−5
mm year
−1
). These parameters were compared to that of MP AISI 304 of lower polarization resistance (
R
p
= 168 kΩ) and higher corrosion rate of 6.01 × 10
−5
mm year
−1
). Potentiodynamic polarization shows that the
E
corr
was −61.09 mV for EP samples compared to −127 mV for MP samples and that the corrosion rate for MP samples was higher than that of EP samples. Mott-Schottky analysis shows a donor densities of 1.370 × 10
22
cm
−3
for the EP samples vs. 3.014 × 10
21
cm
−3
for MP samples, while acceptor densities of 8.304 × 10
21
cm
−3
for EP samples vs. 7.389 × 10
22
cm
−3
for MP samples compared to unpolished sample of donor density of 2.036 × 10
21
cm
−3
and acceptor density of 8.784 × 10
20
cm
−3
which evidenced the better performance for EP treatment. The results were supported by electrochemical impedance spectroscopy as well. |
---|---|
AbstractList | AISI 304 is essential for vital industries, e.g., aerospace, nuclear plants, pharmaceutical, chemical, and medical industries. Enhancement of AISI 304 surface characteristics is required for protection, durability, and better performance. Different methods were used for surface modification like mechanical polishing (MP) and electrochemical polishing (EP). Scanning electron microscopy, atomic force microscopy, and gloss values revealed the alleviation of humps, imperfection and roughness, and leveling. Smoothness and brightening of the surface after EP (∆
R
= − 1.206 nm) was more than that of MP treatment (∆
R
= − 0.562 nm). Energy dispersive X-ray analysis showed increase of Cr, Ni, and Mn content while the content of Fe decreased after EP treatment. Potentiodynamic polarization of EP AISI 304 in 3.5% NaCl revealed a high polarization resistance (
R
p
= 2786 kΩ) and low corrosion rate of 2.74 × 10
−5
mm year
−1
). These parameters were compared to that of MP AISI 304 of lower polarization resistance (
R
p
= 168 kΩ) and higher corrosion rate of 6.01 × 10
−5
mm year
−1
). Potentiodynamic polarization shows that the
E
corr
was −61.09 mV for EP samples compared to −127 mV for MP samples and that the corrosion rate for MP samples was higher than that of EP samples. Mott-Schottky analysis shows a donor densities of 1.370 × 10
22
cm
−3
for the EP samples vs. 3.014 × 10
21
cm
−3
for MP samples, while acceptor densities of 8.304 × 10
21
cm
−3
for EP samples vs. 7.389 × 10
22
cm
−3
for MP samples compared to unpolished sample of donor density of 2.036 × 10
21
cm
−3
and acceptor density of 8.784 × 10
20
cm
−3
which evidenced the better performance for EP treatment. The results were supported by electrochemical impedance spectroscopy as well. AISI 304 is essential for vital industries, e.g., aerospace, nuclear plants, pharmaceutical, chemical, and medical industries. Enhancement of AISI 304 surface characteristics is required for protection, durability, and better performance. Different methods were used for surface modification like mechanical polishing (MP) and electrochemical polishing (EP). Scanning electron microscopy, atomic force microscopy, and gloss values revealed the alleviation of humps, imperfection and roughness, and leveling. Smoothness and brightening of the surface after EP (∆R = − 1.206 nm) was more than that of MP treatment (∆R = − 0.562 nm). Energy dispersive X-ray analysis showed increase of Cr, Ni, and Mn content while the content of Fe decreased after EP treatment. Potentiodynamic polarization of EP AISI 304 in 3.5% NaCl revealed a high polarization resistance (Rp = 2786 kΩ) and low corrosion rate of 2.74 × 10−5 mm year−1). These parameters were compared to that of MP AISI 304 of lower polarization resistance (Rp = 168 kΩ) and higher corrosion rate of 6.01 × 10−5 mm year−1). Potentiodynamic polarization shows that the Ecorr was −61.09 mV for EP samples compared to −127 mV for MP samples and that the corrosion rate for MP samples was higher than that of EP samples. Mott-Schottky analysis shows a donor densities of 1.370 × 1022 cm−3 for the EP samples vs. 3.014 × 1021 cm−3 for MP samples, while acceptor densities of 8.304 × 1021 cm−3 for EP samples vs. 7.389 × 1022 cm−3 for MP samples compared to unpolished sample of donor density of 2.036 × 1021 cm−3 and acceptor density of 8.784 × 1020 cm−3 which evidenced the better performance for EP treatment. The results were supported by electrochemical impedance spectroscopy as well. |
Author | Abouelata, Ahmed M. Awad Attia, Adel Youssef, Gehan I. |
Author_xml | – sequence: 1 givenname: Ahmed M. Awad surname: Abouelata fullname: Abouelata, Ahmed M. Awad organization: Department of Chemical Engineering and Pilot Plant, Engineering Research Division, National Research Centre – sequence: 2 givenname: Adel orcidid: 0000-0001-6406-2890 surname: Attia fullname: Attia, Adel email: adel_attia@hotmail.com organization: Electrochemistry and Corrosion Laboratory, Physical Chemistry Department, National Research Centre – sequence: 3 givenname: Gehan I. surname: Youssef fullname: Youssef, Gehan I. organization: Electrochemistry and Corrosion Laboratory, Physical Chemistry Department, National Research Centre |
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CitedBy_id | crossref_primary_10_23939_chcht17_02_262 crossref_primary_10_1007_s10800_022_01843_2 crossref_primary_10_1016_j_surfcoat_2024_131011 crossref_primary_10_1016_j_matchemphys_2023_127329 crossref_primary_10_3390_coatings12111672 |
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Copyright | The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021. corrected publication 2021 The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021. corrected publication 2021. |
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Keywords | Mott-Schottky analysis Mechanical polishing Stainless steel Roughness electrochemical polishing Potentiodynamic polarization Impedance spectroscopy |
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Snippet | AISI 304 is essential for vital industries, e.g., aerospace, nuclear plants, pharmaceutical, chemical, and medical industries. Enhancement of AISI 304 surface... |
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SubjectTerms | Aerospace industry Analytical Chemistry Atomic force microscopy Brightening Characterization and Evaluation of Materials Chemical polishing Chemistry Chemistry and Materials Science Condensed Matter Physics Corrosion Corrosion rate Corrosion resistance Density Electrochemical impedance spectroscopy Electrochemistry Electrode polarization Electropolishing Energy dispersive X ray analysis Energy Storage Gloss Manganese Mechanical polishing Microscopy Original Paper Physical Chemistry Smoothness Surface properties X ray analysis |
Title | Electrochemical polishing versus mechanical polishing of AISI 304: surface and electrochemical study |
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