Development of magnetically separable MoS2/NiFe2O4 heterostructure for improved photocatalytic efficiency of malachite green (MG) degradation

Photocatalysis is a multifaceted phenomenon that can be employed for diverse applications, such as waste management and the treatment of water resources. Through a hydrothermal process, a magnetic nanocomposite comprising MoS 2 and NiFe 2 O 4 with optical activity was effectively synthesized. The pr...

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Published in	Journal of materials science. Materials in electronics Vol. 35; no. 16; p. 1045
Main Authors	Alanazi, Meznah M., Abdelmohsen, Shaimaa A. M., Alahmari, Saeed D., Abdullah, Muhammad, Aman, Salma, Al-Sehemi, Abdullah G., Farid, Hafiz Muhammad Tahir
Format	Journal Article
Language	English
Published	New York Springer US 01.06.2024 Springer Nature B.V
Subjects	Absorption spectra Characterization and Evaluation of Materials Chemistry and Materials Science Current carriers Degradation Free radicals Heterostructures Magnetic separation Malachite green Materials Science Molybdenum disulfide Nanocomposites Nickel ferrites Optical activity Optical and Electronic Materials Optical properties Photocatalysis Physiochemistry Synthesis Waste management Water resources
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Abstract	Photocatalysis is a multifaceted phenomenon that can be employed for diverse applications, such as waste management and the treatment of water resources. Through a hydrothermal process, a magnetic nanocomposite comprising MoS 2 and NiFe 2 O 4 with optical activity was effectively synthesized. The produced photocatalysts were subjected to different methods to investigate the physiochemical properties of the materials. The optical band-gap values of the fabricated nanocomposite were measured to be 1.75 and 1.57 eV accordingly for NiFe 2 O 4 and MoS 2 /NiFe 2 O 4 which were established by UV–Visible absorption spectrum via Tauc’s relation. From the BET study, the surface area of prepared MoS 2 /NiFe 2 O 4 NCs was achieved to be 71.05 m 2 g −1 . The photocatalytic efficacy was assessed by observing malachite green degradation in the existence of visible light conditions. The MoS 2 /NiFe 2 O 4 nanocomposite contains degradation efficiency of 98.28% in 140 min under visible source toward malachite green and demonstrated favorable reusability potential through magnetic separation. This finding indicates that the activity of synthesized nanocomposite is superior to that of isolated MoS 2 and NiFe 2 O 4 NPs. A plausible mechanism for photocatalysis was explicated with charge carriers and scavengers of free radicals. The primary contributors to dye degradation were responsible to be the OH radical and holes species.
AbstractList	Photocatalysis is a multifaceted phenomenon that can be employed for diverse applications, such as waste management and the treatment of water resources. Through a hydrothermal process, a magnetic nanocomposite comprising MoS 2 and NiFe 2 O 4 with optical activity was effectively synthesized. The produced photocatalysts were subjected to different methods to investigate the physiochemical properties of the materials. The optical band-gap values of the fabricated nanocomposite were measured to be 1.75 and 1.57 eV accordingly for NiFe 2 O 4 and MoS 2 /NiFe 2 O 4 which were established by UV–Visible absorption spectrum via Tauc’s relation. From the BET study, the surface area of prepared MoS 2 /NiFe 2 O 4 NCs was achieved to be 71.05 m 2 g −1 . The photocatalytic efficacy was assessed by observing malachite green degradation in the existence of visible light conditions. The MoS 2 /NiFe 2 O 4 nanocomposite contains degradation efficiency of 98.28% in 140 min under visible source toward malachite green and demonstrated favorable reusability potential through magnetic separation. This finding indicates that the activity of synthesized nanocomposite is superior to that of isolated MoS 2 and NiFe 2 O 4 NPs. A plausible mechanism for photocatalysis was explicated with charge carriers and scavengers of free radicals. The primary contributors to dye degradation were responsible to be the OH radical and holes species. Photocatalysis is a multifaceted phenomenon that can be employed for diverse applications, such as waste management and the treatment of water resources. Through a hydrothermal process, a magnetic nanocomposite comprising MoS2 and NiFe2O4 with optical activity was effectively synthesized. The produced photocatalysts were subjected to different methods to investigate the physiochemical properties of the materials. The optical band-gap values of the fabricated nanocomposite were measured to be 1.75 and 1.57 eV accordingly for NiFe2O4 and MoS2/NiFe2O4 which were established by UV–Visible absorption spectrum via Tauc’s relation. From the BET study, the surface area of prepared MoS2/NiFe2O4 NCs was achieved to be 71.05 m2 g−1. The photocatalytic efficacy was assessed by observing malachite green degradation in the existence of visible light conditions. The MoS2/NiFe2O4 nanocomposite contains degradation efficiency of 98.28% in 140 min under visible source toward malachite green and demonstrated favorable reusability potential through magnetic separation. This finding indicates that the activity of synthesized nanocomposite is superior to that of isolated MoS2 and NiFe2O4 NPs. A plausible mechanism for photocatalysis was explicated with charge carriers and scavengers of free radicals. The primary contributors to dye degradation were responsible to be the OH radical and holes species.
ArticleNumber	1045
Author	Al-Sehemi, Abdullah G. Farid, Hafiz Muhammad Tahir Abdelmohsen, Shaimaa A. M. Alanazi, Meznah M. Abdullah, Muhammad Aman, Salma Alahmari, Saeed D.
Author_xml	– sequence: 1 givenname: Meznah M. surname: Alanazi fullname: Alanazi, Meznah M. organization: Department of Physics, College of Science, Princess Nourah bint Abdulrahman University – sequence: 2 givenname: Shaimaa A. M. surname: Abdelmohsen fullname: Abdelmohsen, Shaimaa A. M. organization: Department of Physics, College of Science, Princess Nourah bint Abdulrahman University – sequence: 3 givenname: Saeed D. surname: Alahmari fullname: Alahmari, Saeed D. organization: Department of Chemistry, Faculty of Science, Jazan University – sequence: 4 givenname: Muhammad surname: Abdullah fullname: Abdullah, Muhammad organization: Department of Chemistry, Government College University Lahore – sequence: 5 givenname: Salma orcidid: 0000-0001-5970-8036 surname: Aman fullname: Aman, Salma email: salma.physics.kfu@gmail.com organization: Institute of Physics, Khwaja Fareed University of Engineering and Information Technology – sequence: 6 givenname: Abdullah G. surname: Al-Sehemi fullname: Al-Sehemi, Abdullah G. organization: Research Center for Advanced Materials Science (RCAMS), King Khalid University, Department of Chemistry, College of Science, King Khalid University – sequence: 7 givenname: Hafiz Muhammad Tahir surname: Farid fullname: Farid, Hafiz Muhammad Tahir organization: Department of Physics, Government Graduate College Taunsa Sharif
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SubjectTerms	Absorption spectra Characterization and Evaluation of Materials Chemistry and Materials Science Current carriers Degradation Free radicals Heterostructures Magnetic separation Malachite green Materials Science Molybdenum disulfide Nanocomposites Nickel ferrites Optical activity Optical and Electronic Materials Optical properties Photocatalysis Physiochemistry Synthesis Waste management Water resources
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Title	Development of magnetically separable MoS2/NiFe2O4 heterostructure for improved photocatalytic efficiency of malachite green (MG) degradation
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