Copper-nitrogen doped carbon nanosheet-based electrochemical sensors for the detection of luteolin and baicalein
Metal-containing copper-nitrogen doped porous carbon materials (Cu@NC) were prepared by a one-step pyrolysis method, and an electrochemical sensor capable of simultaneously detecting luteolin and baicalein was fasbricated. Cu@NC has been characterized by scanning electron microscopy, transmission el...
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| Published in | Journal of materials science. Materials in electronics Vol. 35; no. 5; p. 340 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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New York
Springer US
01.02.2024
Springer Nature B.V |
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| Abstract | Metal-containing copper-nitrogen doped porous carbon materials (Cu@NC) were prepared by a one-step pyrolysis method, and an electrochemical sensor capable of simultaneously detecting luteolin and baicalein was fasbricated. Cu@NC has been characterized by scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The electrochemical properties of the Cu@NC sensor were studied by electrochemical impedance spectroscopy and cyclic voltammetry. In addition, the electrochemical behavior of the sensor on different electrodes was studied by differential pulse voltammetry. The calibration curve was linear in the range of (0.05–20.0) × 10
–6
mol/L. The detection limits of luteolin and baicalein were 5.30 × 10
–8
mol/L and 9.10 × 10
–8
mol/L, respectively (S/N = 3). The sensor has also been successfully used to detect luteolin and baicalin in actual drugs. It has broad potential applications in the field of medicine due to its simple production and low technical cost requirements. |
|---|---|
| AbstractList | Metal-containing copper-nitrogen doped porous carbon materials (Cu@NC) were prepared by a one-step pyrolysis method, and an electrochemical sensor capable of simultaneously detecting luteolin and baicalein was fasbricated. Cu@NC has been characterized by scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The electrochemical properties of the Cu@NC sensor were studied by electrochemical impedance spectroscopy and cyclic voltammetry. In addition, the electrochemical behavior of the sensor on different electrodes was studied by differential pulse voltammetry. The calibration curve was linear in the range of (0.05–20.0) × 10–6 mol/L. The detection limits of luteolin and baicalein were 5.30 × 10–8 mol/L and 9.10 × 10–8 mol/L, respectively (S/N = 3). The sensor has also been successfully used to detect luteolin and baicalin in actual drugs. It has broad potential applications in the field of medicine due to its simple production and low technical cost requirements. Metal-containing copper-nitrogen doped porous carbon materials (Cu@NC) were prepared by a one-step pyrolysis method, and an electrochemical sensor capable of simultaneously detecting luteolin and baicalein was fasbricated. Cu@NC has been characterized by scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. The electrochemical properties of the Cu@NC sensor were studied by electrochemical impedance spectroscopy and cyclic voltammetry. In addition, the electrochemical behavior of the sensor on different electrodes was studied by differential pulse voltammetry. The calibration curve was linear in the range of (0.05–20.0) × 10 –6 mol/L. The detection limits of luteolin and baicalein were 5.30 × 10 –8 mol/L and 9.10 × 10 –8 mol/L, respectively (S/N = 3). The sensor has also been successfully used to detect luteolin and baicalin in actual drugs. It has broad potential applications in the field of medicine due to its simple production and low technical cost requirements. |
| ArticleNumber | 340 |
| Author | Chu, Tingting Gao, Yi Zheng, Yin Liu, Yaopeng Huang, Wensheng Zhou, Chengyu |
| Author_xml | – sequence: 1 givenname: Tingting surname: Chu fullname: Chu, Tingting organization: Hubei Key Laboratory of Selenium Resources Research and Biological Applications, Institute of Selenium Science and Industry, Hubei Minzu University, School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 2 givenname: Yaopeng surname: Liu fullname: Liu, Yaopeng organization: Hubei Key Laboratory of Selenium Resources Research and Biological Applications, Institute of Selenium Science and Industry, Hubei Minzu University, School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 3 givenname: Yi surname: Gao fullname: Gao, Yi organization: Hubei Key Laboratory of Selenium Resources Research and Biological Applications, Institute of Selenium Science and Industry, Hubei Minzu University, School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 4 givenname: Chengyu surname: Zhou fullname: Zhou, Chengyu organization: Hubei Key Laboratory of Selenium Resources Research and Biological Applications, Institute of Selenium Science and Industry, Hubei Minzu University, School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 5 givenname: Wensheng surname: Huang fullname: Huang, Wensheng organization: School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 6 givenname: Yin orcidid: 0000-0001-5248-7381 surname: Zheng fullname: Zheng, Yin email: zhengyin0617@163.com organization: Hubei Key Laboratory of Selenium Resources Research and Biological Applications, Institute of Selenium Science and Industry, Hubei Minzu University, School of Chemical and Environmental Engineering, Hubei Minzu University |
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| SubjectTerms | Carbon Characterization and Evaluation of Materials Chemical sensors Chemistry and Materials Science Chromatography Copper Electrochemical analysis Electrochemical impedance spectroscopy Electrodes Electron microscopy Materials Science Nanosheets Nitrogen Optical and Electronic Materials Photoelectrons Porous materials Pyrolysis Scanning electron microscopy Selenium Sensors Voltammetry Work stations X ray photoelectron spectroscopy |
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| Title | Copper-nitrogen doped carbon nanosheet-based electrochemical sensors for the detection of luteolin and baicalein |
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