Arylation of quinoxalinones at room temperature under metal and base free-conditions
A mild and efficient method for the arylation of quinoxalinones are described using aryldiazonium tetrafluoroborates as aryl source. Reactions proceeds at room temperature in a short reaction time of 1 h without metal catalysts and bases. Broad functional group tolerance was observed with good yield...
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| Published in | Monatshefte für Chemie Vol. 155; no. 6; pp. 613 - 619 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Vienna
Springer Vienna
01.06.2024
Springer Nature Springer Nature B.V |
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| Abstract | A mild and efficient method for the arylation of quinoxalinones are described using aryldiazonium tetrafluoroborates as aryl source. Reactions proceeds at room temperature in a short reaction time of 1 h without metal catalysts and bases. Broad functional group tolerance was observed with good yields of products even at gram scale reaction. Control experiments suggest that the reactions proceed through a radical pathway. Furthermore, the present protocol applied for the successive synthesis of three biologically active molecules. Overall, the method offers a convenient and versatile approach for the synthesis of arylated quinoxalinones.
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| AbstractList | A mild and efficient method for the arylation of quinoxalinones are described using aryldiazonium tetrafluoroborates as aryl source. Reactions proceeds at room temperature in a short reaction time of 1 h without metal catalysts and bases. Broad functional group tolerance was observed with good yields of products even at gram scale reaction. Control experiments suggest that the reactions proceed through a radical pathway. Furthermore, the present protocol applied for the successive synthesis of three biologically active molecules. Overall, the method offers a convenient and versatile approach for the synthesis of arylated quinoxalinones. A mild and efficient method for the arylation of quinoxalinones are described using aryldiazonium tetrafluoroborates as aryl source. Reactions proceeds at room temperature in a short reaction time of 1 h without metal catalysts and bases. Broad functional group tolerance was observed with good yields of products even at gram scale reaction. Control experiments suggest that the reactions proceed through a radical pathway. Furthermore, the present protocol applied for the successive synthesis of three biologically active molecules. Overall, the method offers a convenient and versatile approach for the synthesis of arylated quinoxalinones. Graphical abstract |
| Author | Badhani, Gaurav Adimurthy, Subbarayappa |
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| Keywords | Arylation Regioselective Quinoxalinone Aryldiazonium salt Catalyst-free reaction DESIGN POTENT C-H ARYLATION SULFENYLATION QUINOXALIN-2(1H)-ONES INHIBITORS |
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| Snippet | A mild and efficient method for the arylation of quinoxalinones are described using aryldiazonium tetrafluoroborates as aryl source. Reactions proceeds at room... |
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| SubjectTerms | Analytical Chemistry Base metal Chemical synthesis Chemistry Chemistry and Materials Science Chemistry, Multidisciplinary Chemistry/Food Science Functional groups Inorganic Chemistry Organic Chemistry Original Paper Physical Chemistry Physical Sciences Room temperature Science & Technology Theoretical and Computational Chemistry |
| Title | Arylation of quinoxalinones at room temperature under metal and base free-conditions |
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