A high-throughput strategy for rapid synthesis and characterization of Ni-based superalloys
This study developed a new high-throughput strategy, designated as hot-isostatic-pressing-based micro-synthesis approach (HIP-MSA), to optimize high-performance nickel-based superalloys in a rapid, efficient, and cost-effective manner. A specific honeycomb-array structure containing 106 discrete cel...
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| Published in | Rare metals Vol. 41; no. 8; pp. 2693 - 2700 |
|---|---|
| Main Authors | , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Beijing
Nonferrous Metals Society of China
01.08.2022
Springer Nature B.V |
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| Abstract | This study developed a new high-throughput strategy, designated as hot-isostatic-pressing-based micro-synthesis approach (HIP-MSA), to optimize high-performance nickel-based superalloys in a rapid, efficient, and cost-effective manner. A specific honeycomb-array structure containing 106 discrete cells was designed and optimized using finite element analysis (FEA) and then applied to create a combinatorial library consisting of 106 Ni-based superalloys with various Co, Nb and Ta concentrations. By integration with high-throughput characterization tools, extensive composition and phase structure data were collected quickly and efficiently. In the superalloys with higher amounts of Nb and Ta, the detrimental η phase displaying needle-like morphology was observed, and its content (wt%) increased drastically with Ta and Nb contents increasing. However, the increase of Co addition in those alloys was confirmed to be surprisingly beneficial by significantly suppressing the formation of η phase that was induced by high Nb and Ta contents. The zero-phase-fraction (ZPF) line of η phase was established, which is critical to design superalloy chemistry for superior microstructural stability at high-temperature service conditions.
Graphical abstract |
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| AbstractList | This study developed a new high-throughput strategy, designated as hot-isostatic-pressing-based micro-synthesis approach (HIP-MSA), to optimize high-performance nickel-based superalloys in a rapid, efficient, and cost-effective manner. A specific honeycomb-array structure containing 106 discrete cells was designed and optimized using finite element analysis (FEA) and then applied to create a combinatorial library consisting of 106 Ni-based superalloys with various Co, Nb and Ta concentrations. By integration with high-throughput characterization tools, extensive composition and phase structure data were collected quickly and efficiently. In the superalloys with higher amounts of Nb and Ta, the detrimental η phase displaying needle-like morphology was observed, and its content (wt%) increased drastically with Ta and Nb contents increasing. However, the increase of Co addition in those alloys was confirmed to be surprisingly beneficial by significantly suppressing the formation of η phase that was induced by high Nb and Ta contents. The zero-phase-fraction (ZPF) line of η phase was established, which is critical to design superalloy chemistry for superior microstructural stability at high-temperature service conditions. This study developed a new high-throughput strategy, designated as hot-isostatic-pressing-based micro-synthesis approach (HIP-MSA), to optimize high-performance nickel-based superalloys in a rapid, efficient, and cost-effective manner. A specific honeycomb-array structure containing 106 discrete cells was designed and optimized using finite element analysis (FEA) and then applied to create a combinatorial library consisting of 106 Ni-based superalloys with various Co, Nb and Ta concentrations. By integration with high-throughput characterization tools, extensive composition and phase structure data were collected quickly and efficiently. In the superalloys with higher amounts of Nb and Ta, the detrimental η phase displaying needle-like morphology was observed, and its content (wt%) increased drastically with Ta and Nb contents increasing. However, the increase of Co addition in those alloys was confirmed to be surprisingly beneficial by significantly suppressing the formation of η phase that was induced by high Nb and Ta contents. The zero-phase-fraction (ZPF) line of η phase was established, which is critical to design superalloy chemistry for superior microstructural stability at high-temperature service conditions. Graphical abstract |
| Author | Zhang, Wen-Yu Wang, Hui Wang, Hai-Zhou Jiang, Liang Broeckmann, Christoph Huang, Zai-Wang Zhao, Lei Zhu, Li-Long Huang, Hai-Liang Deng, Yuan-Bin Liu, Su-Ran Yang, Li-Xia |
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| Keywords | Honeycomb-array structure Superalloy Zero-phase-fraction (ZPF) line Finite element analysis (FEA) Bulk combinatorial synthesis |
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| SubjectTerms | Biomaterials Chemistry and Materials Science Combinatorial analysis Energy Finite element method High temperature Materials Engineering Materials Science Metallic Materials Nanoscale Science and Technology Nickel Nickel base alloys Niobium Original Article Physical Chemistry Solid phases Superalloys Synthesis Tantalum |
| Title | A high-throughput strategy for rapid synthesis and characterization of Ni-based superalloys |
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