Photocatalytic and antibacterial activities of ZnO nanoparticles synthesized by chemical method

In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO 3 ) 2 and KOH as precipitating agent. The obtained samples were thoroughly characterized by different techniques like XRD, UV–Vis. DRS, PL, FE-SEM and HR-TEM. The XRD patterns of ZnO NPs (calcined at...

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Published in	Journal of materials science. Materials in electronics Vol. 32; no. 15; pp. 20510 - 20524
Main Authors	Bhosale, A. S., Abitkar, K. K., Sadalage, P. S., Pawar, K. D., Garadkar, K. M.
Format	Journal Article
Language	English
Published	New York Springer US 01.08.2021 Springer Nature B.V
Subjects	Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Dyes E coli Infrared spectroscopy Materials Science Nanoparticles Optical and Electronic Materials Photocatalysis Photodegradation Roasting Wurtzite Zinc oxide
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Abstract	In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO 3 ) 2 and KOH as precipitating agent. The obtained samples were thoroughly characterized by different techniques like XRD, UV–Vis. DRS, PL, FE-SEM and HR-TEM. The XRD patterns of ZnO NPs (calcined at 300–500 °C) show wurtzite hexagonal nanocrystalline structure. The structural parameters were studied in detail. The bandgap of ZnO NPs calcined at 400 °C is found to be 3.13 eV. The FT-IR spectra represent the characteristic Zn–O–Zn stretching vibrational band. The FE-SEM and HR-TEM images reveal that the ZnO NPs calcined at 400 °C are in spherical shape with 15–20 nm size. The EDS spectrum showed elemental compositions of ZnO NPs with oxygen vacancies. The photocatalytic properties of the calcined samples are investigated by studying the photodegradation of Methyl Orange (MO) which showed a photodegradation efficiency of 92.69% within 120 min under UV–Vis. light ( λ = 365 nm). In addition, antibacterial activity of ZnO NPs calcined at 400 °C was studied against five different bacterial strains by agar well diffusion method. The test of antibacterial activity indicated the highest antibacterial activity of ZnO NPs against S. aureus followed by E. coli and B. subtilis .
AbstractList	In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO3)2 and KOH as precipitating agent. The obtained samples were thoroughly characterized by different techniques like XRD, UV–Vis. DRS, PL, FE-SEM and HR-TEM. The XRD patterns of ZnO NPs (calcined at 300–500 °C) show wurtzite hexagonal nanocrystalline structure. The structural parameters were studied in detail. The bandgap of ZnO NPs calcined at 400 °C is found to be 3.13 eV. The FT-IR spectra represent the characteristic Zn–O–Zn stretching vibrational band. The FE-SEM and HR-TEM images reveal that the ZnO NPs calcined at 400 °C are in spherical shape with 15–20 nm size. The EDS spectrum showed elemental compositions of ZnO NPs with oxygen vacancies. The photocatalytic properties of the calcined samples are investigated by studying the photodegradation of Methyl Orange (MO) which showed a photodegradation efficiency of 92.69% within 120 min under UV–Vis. light (λ = 365 nm). In addition, antibacterial activity of ZnO NPs calcined at 400 °C was studied against five different bacterial strains by agar well diffusion method. The test of antibacterial activity indicated the highest antibacterial activity of ZnO NPs against S. aureus followed by E. coli and B. subtilis. In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO 3 ) 2 and KOH as precipitating agent. The obtained samples were thoroughly characterized by different techniques like XRD, UV–Vis. DRS, PL, FE-SEM and HR-TEM. The XRD patterns of ZnO NPs (calcined at 300–500 °C) show wurtzite hexagonal nanocrystalline structure. The structural parameters were studied in detail. The bandgap of ZnO NPs calcined at 400 °C is found to be 3.13 eV. The FT-IR spectra represent the characteristic Zn–O–Zn stretching vibrational band. The FE-SEM and HR-TEM images reveal that the ZnO NPs calcined at 400 °C are in spherical shape with 15–20 nm size. The EDS spectrum showed elemental compositions of ZnO NPs with oxygen vacancies. The photocatalytic properties of the calcined samples are investigated by studying the photodegradation of Methyl Orange (MO) which showed a photodegradation efficiency of 92.69% within 120 min under UV–Vis. light ( λ = 365 nm). In addition, antibacterial activity of ZnO NPs calcined at 400 °C was studied against five different bacterial strains by agar well diffusion method. The test of antibacterial activity indicated the highest antibacterial activity of ZnO NPs against S. aureus followed by E. coli and B. subtilis .
Author	Sadalage, P. S. Bhosale, A. S. Pawar, K. D. Abitkar, K. K. Garadkar, K. M.
Author_xml	– sequence: 1 givenname: A. S. surname: Bhosale fullname: Bhosale, A. S. organization: Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University – sequence: 2 givenname: K. K. surname: Abitkar fullname: Abitkar, K. K. organization: Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, Department of Agrochemicals and Pest Management, Shivaji University – sequence: 3 givenname: P. S. surname: Sadalage fullname: Sadalage, P. S. organization: School of Nanoscience and Technology, Shivaji University – sequence: 4 givenname: K. D. surname: Pawar fullname: Pawar, K. D. organization: School of Nanoscience and Technology, Shivaji University – sequence: 5 givenname: K. M. orcidid: 0000-0002-5733-9895 surname: Garadkar fullname: Garadkar, K. M. email: kmg_chem@unishivaji.ac.in organization: Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University
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Snippet	In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO 3 ) 2 and KOH as precipitating agent. The obtained samples... In this study, ZnO NPs were synthesized and reporting first time using capping agent SDS with Zn (NO3)2 and KOH as precipitating agent. The obtained samples...
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SubjectTerms	Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Dyes E coli Infrared spectroscopy Materials Science Nanoparticles Optical and Electronic Materials Photocatalysis Photodegradation Roasting Wurtzite Zinc oxide
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Title	Photocatalytic and antibacterial activities of ZnO nanoparticles synthesized by chemical method
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