Inorganic capsule based on expansive mineral for self-healing concrete

Expansive minerals are extensively used to promote the self-healing performance of the cracked concrete. Nonetheless, the expansive minerals will be consumed prematurely by participating in cement hydration. In this study, two types of inorganic capsules based on magnesium oxide expansive agent were...

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Published inCement & concrete composites Vol. 144; p. 105305
Main Authors Li, Jinglu, Guan, Xinchun, Zhang, Chenchen
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.11.2023
Subjects
Inorganic capsule
Magnesium oxide expansive agent
Microstructure analysis
Permeability coefficient
Self-healing
Superabsorbent polymer
Inorganic capsule
Superabsorbent polymer
Magnesium oxide expansive agent
Self-healing
Permeability coefficient
Microstructure analysis
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Abstract Expansive minerals are extensively used to promote the self-healing performance of the cracked concrete. Nonetheless, the expansive minerals will be consumed prematurely by participating in cement hydration. In this study, two types of inorganic capsules based on magnesium oxide expansive agent were developed by the techniques of granulation and encapsulation. The superabsorbent polymer was also embedded in inorganic capsules to enhance the healing ability. To investigate the healing potential and durability of the inorganic capsules in cement matrix, the mineralogy of inner core, granule strength and encapsulation effect were measured. The self-healing efficiency was evaluated by the tests of crack observation, water permeability and microstructure analysis. Results showed that the inner core of inorganic capsules remained stable during granulation, and the protective shell endowed the capsules with considerable strength and erosion resistance. Due to the addition of inorganic capsules, especially the capsules containing two-component healing agents, the effects of crack closure and impermeability recovery of the cracked mortar were significantly increased after healing in wet-dry cycles. The self-healing products consisting of calcite and Mg-rich phases were formed by the reaction of healing agents. The formation of the Mg-rich products was further accelerated owing to the continuous water supply by the superabsorbent polymer inside inorganic capsules. •Inorganic capsule with great healing potential and erosion resistance was developed.•Addition of capsules obviously improved crack closure and impermeability recovery.•Capsules enriched the composition and content of the healing products in cracks.•Healing process was further accelerated by the superabsorbent polymer in capsules.
AbstractList Expansive minerals are extensively used to promote the self-healing performance of the cracked concrete. Nonetheless, the expansive minerals will be consumed prematurely by participating in cement hydration. In this study, two types of inorganic capsules based on magnesium oxide expansive agent were developed by the techniques of granulation and encapsulation. The superabsorbent polymer was also embedded in inorganic capsules to enhance the healing ability. To investigate the healing potential and durability of the inorganic capsules in cement matrix, the mineralogy of inner core, granule strength and encapsulation effect were measured. The self-healing efficiency was evaluated by the tests of crack observation, water permeability and microstructure analysis. Results showed that the inner core of inorganic capsules remained stable during granulation, and the protective shell endowed the capsules with considerable strength and erosion resistance. Due to the addition of inorganic capsules, especially the capsules containing two-component healing agents, the effects of crack closure and impermeability recovery of the cracked mortar were significantly increased after healing in wet-dry cycles. The self-healing products consisting of calcite and Mg-rich phases were formed by the reaction of healing agents. The formation of the Mg-rich products was further accelerated owing to the continuous water supply by the superabsorbent polymer inside inorganic capsules. •Inorganic capsule with great healing potential and erosion resistance was developed.•Addition of capsules obviously improved crack closure and impermeability recovery.•Capsules enriched the composition and content of the healing products in cracks.•Healing process was further accelerated by the superabsorbent polymer in capsules.
ArticleNumber 105305
Author Guan, Xinchun
Zhang, Chenchen
Li, Jinglu
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Keywords Inorganic capsule
Superabsorbent polymer
Magnesium oxide expansive agent
Self-healing
Permeability coefficient
Microstructure analysis
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Snippet Expansive minerals are extensively used to promote the self-healing performance of the cracked concrete. Nonetheless, the expansive minerals will be consumed...
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elsevier
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StartPage 105305
SubjectTerms Inorganic capsule
Magnesium oxide expansive agent
Microstructure analysis
Permeability coefficient
Self-healing
Superabsorbent polymer
Title Inorganic capsule based on expansive mineral for self-healing concrete
URI https://dx.doi.org/10.1016/j.cemconcomp.2023.105305
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