Synthesis of ferrocene and azobenzene-based copolymers P(FHEMA-co-MAZOHE)s and their redox and photo-responsive properties
Herein, poly(2-(methacryloyloxy) ethyl ferrocene carboxylate-co-(methacrylohydroxyhexane azobenzene)s) (P(FHEMA-co-MAZOHE)s) were prepared by random copolymerization and were characterized by proton nuclear magnetic resonance (1H NMR) and gel permeation chromatography (GPC) to confirm the structures...
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| Published in | Journal of organometallic chemistry Vol. 895; pp. 37 - 47 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.09.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Herein, poly(2-(methacryloyloxy) ethyl ferrocene carboxylate-co-(methacrylohydroxyhexane azobenzene)s) (P(FHEMA-co-MAZOHE)s) were prepared by random copolymerization and were characterized by proton nuclear magnetic resonance (1H NMR) and gel permeation chromatography (GPC) to confirm the structures and molecular weights respectively. Thermal variations were analyzed by thermogravimetric (TG), differential thermogravimetric (DTG) and differential scanning calorimetry (DSC) techniques. Finally, redox and photo stimuli-responsive properties were confirmed by cyclic voltammetry (CV) and ultraviolet–visible spectroscopy (UV–vis) respectively. The results revealed that (P(FHEMA-co-MAZOHE)s) can be useful as information storage materials.
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•Ferrocene and azobenzene-based copolymers were synthesized using conventional free radical polymerization.•Photoresponsive behavior was confirmed by UV/vis spectroscopy.•Electroactive behavior was analyzed by Cyclic Voltammetry.•The results indicated that the synthesized copolymers can provide a pathway regarding the four states of information storage. |
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| AbstractList | Herein, poly(2-(methacryloyloxy) ethyl ferrocene carboxylate-co-(methacrylohydroxyhexane azobenzene)s) (P(FHEMA-co-MAZOHE)s) were prepared by random copolymerization and were characterized by proton nuclear magnetic resonance (1H NMR) and gel permeation chromatography (GPC) to confirm the structures and molecular weights respectively. Thermal variations were analyzed by thermogravimetric (TG), differential thermogravimetric (DTG) and differential scanning calorimetry (DSC) techniques. Finally, redox and photo stimuli-responsive properties were confirmed by cyclic voltammetry (CV) and ultraviolet–visible spectroscopy (UV–vis) respectively. The results revealed that (P(FHEMA-co-MAZOHE)s) can be useful as information storage materials.
[Display omitted]
•Ferrocene and azobenzene-based copolymers were synthesized using conventional free radical polymerization.•Photoresponsive behavior was confirmed by UV/vis spectroscopy.•Electroactive behavior was analyzed by Cyclic Voltammetry.•The results indicated that the synthesized copolymers can provide a pathway regarding the four states of information storage. |
| Author | Zhizhko, Pavel A. Zarubin, Dmitry N. Yu, Haojie Wang, Li Lemenovskiy, Dmitry A. Nazir, Ahsan Khan, Amin Usman, Muhammad Haq, Fazal Naveed, Kaleem-ur-Rehman |
| Author_xml | – sequence: 1 givenname: Amin orcidid: 0000-0002-2179-1003 surname: Khan fullname: Khan, Amin organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 2 givenname: Haojie surname: Yu fullname: Yu, Haojie email: hjyu@zju.edu.cn organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 3 givenname: Li orcidid: 0000-0001-9356-9930 surname: Wang fullname: Wang, Li email: opl_wl@dial.zju.edu.cn organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 4 givenname: Pavel A. surname: Zhizhko fullname: Zhizhko, Pavel A. organization: A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Vavilov str., 28, 119991, Moscow, Russia – sequence: 5 givenname: Dmitry N. surname: Zarubin fullname: Zarubin, Dmitry N. organization: A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Vavilov str., 28, 119991, Moscow, Russia – sequence: 6 givenname: Dmitry A. surname: Lemenovskiy fullname: Lemenovskiy, Dmitry A. organization: Department of Chemistry, Moscow State University, Vorob'evy Gory 1, 119992, Moscow, Russia – sequence: 7 givenname: Fazal surname: Haq fullname: Haq, Fazal organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 8 givenname: Muhammad surname: Usman fullname: Usman, Muhammad organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 9 givenname: Ahsan surname: Nazir fullname: Nazir, Ahsan organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China – sequence: 10 givenname: Kaleem-ur-Rehman surname: Naveed fullname: Naveed, Kaleem-ur-Rehman organization: State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, PR China |
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| SubjectTerms | Azobenzene Ferrocene Information storage Materials |
| Title | Synthesis of ferrocene and azobenzene-based copolymers P(FHEMA-co-MAZOHE)s and their redox and photo-responsive properties |
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