Diferrocenylcyclopropenyl cations. Synthesis, structures, and some chemical properties

Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclo-propenyl tetrafluorobo...

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Published in	Journal of organometallic chemistry Vol. 690; no. 14; pp. 3333 - 3339
Main Authors	Klimova, Elena I., Berestneva, Tatiana Klimova, Ortega, Simon Hernández, Iturbide, Daniel Méndez, Marquez, Alfonso García, García, Marcos Martínez
Format	Journal Article
Language	English
Published	LAUSANNE Elsevier B.V 15.07.2005 Elsevier
Subjects	Chemistry Chemistry, Inorganic & Nuclear Chemistry, Organic Derivatives of 2,3-diferrocenylacrylic acid Diferrocenylcyclopropenes Diferrocenylcyclopropenyl tetrafluoroborates Ferrocene Physical Sciences Ring opening Science & Technology X-ray structural analysis X-ray structural analysis Diferrocenylcyclopropenyl tetrafluoroborates Derivatives of 2,3-diferrocenylacrylic acid Ring opening Ferrocene Diferrocenylcyclopropenes ring opening diferrocenylcyclopropenes RING derivatives of 2,3-diferrocenylacrytic acid SYSTEMS ferrocene diferrocenylcyclopropenyl tetrafluoroborates
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ISSN	0022-328X 1872-8561
DOI	10.1016/j.jorganchem.2005.04.014

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Abstract	Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclo-propenyl tetrafluoroborate was established based on the data from X-ray diffraction analysis. Under the action of potassium tert-butoxide, all the diferrocenylcyclopropenyl tetrafluoroborates undergo three-membered ring-opening with formation of the corresponding 2,3-diferrocenylacrylic acid derivatives. Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclopropenyl tetrafluoroborate was established based on the data from X-ray diffraction analysis. Under the action of potassium tert-butoxide, all the diferrocenylcyclopropenyl tetrafluoroborates undergo three-membered ring-opening with formation of the corresponding 2,3-diferrocenylacrylic acid derivatives. A mechanism of the ring-opening is suggested.
AbstractList	Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclo-propenyl tetrafluoroborate was established based on the data from X-ray diffraction analysis. Under the action of potassium tert-butoxide, all the diferrocenylcyclopropenyl tetrafluoroborates undergo three-membered ring-opening with formation of the corresponding 2,3-diferrocenylacrylic acid derivatives. Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclopropenyl tetrafluoroborate was established based on the data from X-ray diffraction analysis. Under the action of potassium tert-butoxide, all the diferrocenylcyclopropenyl tetrafluoroborates undergo three-membered ring-opening with formation of the corresponding 2,3-diferrocenylacrylic acid derivatives. A mechanism of the ring-opening is suggested. Synthesis of diferrocenyleyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy, ferrocenyl(phenyl)methoxy, N,N-diethylamino, piperidino, and morpholino, is described. The spatial structure of diferrocenyl(morpholino)cyclopropenyl tetralluoroborate was established based on the data from X-ray diffraction analysis. Under the action of potassium tert-butoxide, all the diferrocenylcyclopropenyl tetrafluoroborates undergo three-membered ring-opening with formation of the corresponding 2,3-diferrocenylacrylic acid derivatives. A mechanism of the ring-opening is suggested. (c) 2005 Elsevier B.V. All rights reserved.
Author	Marquez, Alfonso García García, Marcos Martínez Ortega, Simon Hernández Iturbide, Daniel Méndez Klimova, Elena I. Berestneva, Tatiana Klimova
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Keywords	X-ray structural analysis Diferrocenylcyclopropenyl tetrafluoroborates Derivatives of 2,3-diferrocenylacrylic acid Ring opening Ferrocene Diferrocenylcyclopropenes ring opening diferrocenylcyclopropenes RING derivatives of 2,3-diferrocenylacrytic acid SYSTEMS ferrocene diferrocenylcyclopropenyl tetrafluoroborates
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Snippet	Synthesis of diferrocenylcyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy,... Synthesis of diferrocenyleyclopropenyl tetrafluoroborates with hetero-substituents in the three-membered ring, viz., ethoxy, trityloxy,...
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SubjectTerms	Chemistry Chemistry, Inorganic & Nuclear Chemistry, Organic Derivatives of 2,3-diferrocenylacrylic acid Diferrocenylcyclopropenes Diferrocenylcyclopropenyl tetrafluoroborates Ferrocene Physical Sciences Ring opening Science & Technology X-ray structural analysis
Title	Diferrocenylcyclopropenyl cations. Synthesis, structures, and some chemical properties
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