Citral hydrogenation over Rh and Pt catalysts supported on TiO2: Influence of the preparation and activation protocols of the catalysts
During citral hydrogenation, the products distribution obtained on Rh/TiO2 and Pt/TiO2 catalysts depends on their preparation and activation protocols: (i) the unsaturated alcohols (the intended products) are formed in higher quantity on samples reduced at 500 degrees C and more notably with Pt/TiO2...
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| Published in | Journal of molecular catalysis. A, Chemical Vol. 337; no. 1-2; pp. 82 - 88 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier
01.03.2011
Elsevier [1995, Vol. 95, n° 1-janvier 2017, vol. 426, part B] |
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| Abstract | During citral hydrogenation, the products distribution obtained on Rh/TiO2 and Pt/TiO2 catalysts depends on their preparation and activation protocols: (i) the unsaturated alcohols (the intended products) are formed in higher quantity on samples reduced at 500 degrees C and more notably with Pt/TiO2 catalyst; (ii) samples prepared by impregnation of the metallic precursor salt in HCl medium and activated at 300 degrees C are the only ones to lead to the formation of isopulegol as by-product. On the catalysts activated at 500 degrees C, these results can be explained by the presence of the SMSI effect beneficial to hydrogenate selectively the C=O bond of citral towards unsaturated alcohols. |
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| AbstractList | During citral hydrogenation, the products distribution obtained on Rh/TiO2 and Pt/TiO2 catalysts depends on their preparation and activation protocols: (i) the unsaturated alcohols (the intended products) are formed in higher quantity on samples reduced at 500 degrees C and more notably with Pt/TiO2 catalyst; (ii) samples prepared by impregnation of the metallic precursor salt in HCl medium and activated at 300 degrees C are the only ones to lead to the formation of isopulegol as by-product. On the catalysts activated at 500 degrees C, these results can be explained by the presence of the SMSI effect beneficial to hydrogenate selectively the C=O bond of citral towards unsaturated alcohols. |
| Author | EKOU, Lynda LAFAYE, Gwendoline MARECOT, Patrice PRONIER, Stephane ESPECEL, Catherine VICENTE, Aurelie EKOU, Tchirioua |
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| Keywords | Citral hydrogenation Unsaturated alcohols Binary compound Pt Transition element compounds Alcohol Activation Transition metal Aldehyde Titania Hydrogenation Supported catalyst Heterogeneous catalysis Isopulegol Rhodium Platinum Preparation Rh Titanium oxide Citral Platinoid |
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| Title | Citral hydrogenation over Rh and Pt catalysts supported on TiO2: Influence of the preparation and activation protocols of the catalysts |
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