Crystallization‐Induced Enhanced Electrochemiluminescence from a New Tris(bipyridine)ruthenium(II) Derivative
Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused quenching (ACQ) problem, which greatly weakens its ECL efficiency to restrict further applications in solid‐state ECL imaging and light‐emitting...
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| Published in | Advanced functional materials Vol. 33; no. 12 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
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| Abstract | Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused quenching (ACQ) problem, which greatly weakens its ECL efficiency to restrict further applications in solid‐state ECL imaging and light‐emitting devices. Herein, the crystallization‐induced enhanced ECL (CIE‐ECL) of tris(bipyridine)ruthenium(II) derivatives (Ru‐TPE) are reported by decorating Ru‐bpy with inherent aggregation‐induced emission active tetraphenylethene (TPE), which effectively eliminates the detrimental π–π stacking interactions and thus helps Ru‐bpy surmount notorious ACQ effect in the aqueous phase. The Ru‐TPE shows negligible ECL emission in solution but produces a strong ECL emission upon crystallization. Surprisingly, the ECL efficiency of Ru‐TPE crystals is 20 and 3 times higher than that of its solution and Ru‐bpy crystals, respectively. Experimental and structural analysis reveals that such a CIE‐ECL effect originates from the restricted intramolecular rotation and ordered molecular packing. Moreover, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. This work provides a new design strategy for achieving high efficiency in solid‐state ECL imaging and devices.
A new tris(bipyridine)ruthenium(II) derivative (Ru‐TPE) is synthesized and realizes the crystallization‐induced enhanced electrochemiluminescence (CIE‐ECL), which originates from the restricted intramolecular rotation and ordered molecular packing. Besides, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. |
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| AbstractList | Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused quenching (ACQ) problem, which greatly weakens its ECL efficiency to restrict further applications in solid‐state ECL imaging and light‐emitting devices. Herein, the crystallization‐induced enhanced ECL (CIE‐ECL) of tris(bipyridine)ruthenium(II) derivatives (Ru‐TPE) are reported by decorating Ru‐bpy with inherent aggregation‐induced emission active tetraphenylethene (TPE), which effectively eliminates the detrimental
π–π
stacking interactions and thus helps Ru‐bpy surmount notorious ACQ effect in the aqueous phase. The Ru‐TPE shows negligible ECL emission in solution but produces a strong ECL emission upon crystallization. Surprisingly, the ECL efficiency of Ru‐TPE crystals is 20 and 3 times higher than that of its solution and Ru‐bpy crystals, respectively. Experimental and structural analysis reveals that such a CIE‐ECL effect originates from the restricted intramolecular rotation and ordered molecular packing. Moreover, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. This work provides a new design strategy for achieving high efficiency in solid‐state ECL imaging and devices. Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused quenching (ACQ) problem, which greatly weakens its ECL efficiency to restrict further applications in solid‐state ECL imaging and light‐emitting devices. Herein, the crystallization‐induced enhanced ECL (CIE‐ECL) of tris(bipyridine)ruthenium(II) derivatives (Ru‐TPE) are reported by decorating Ru‐bpy with inherent aggregation‐induced emission active tetraphenylethene (TPE), which effectively eliminates the detrimental π–π stacking interactions and thus helps Ru‐bpy surmount notorious ACQ effect in the aqueous phase. The Ru‐TPE shows negligible ECL emission in solution but produces a strong ECL emission upon crystallization. Surprisingly, the ECL efficiency of Ru‐TPE crystals is 20 and 3 times higher than that of its solution and Ru‐bpy crystals, respectively. Experimental and structural analysis reveals that such a CIE‐ECL effect originates from the restricted intramolecular rotation and ordered molecular packing. Moreover, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. This work provides a new design strategy for achieving high efficiency in solid‐state ECL imaging and devices. Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused quenching (ACQ) problem, which greatly weakens its ECL efficiency to restrict further applications in solid‐state ECL imaging and light‐emitting devices. Herein, the crystallization‐induced enhanced ECL (CIE‐ECL) of tris(bipyridine)ruthenium(II) derivatives (Ru‐TPE) are reported by decorating Ru‐bpy with inherent aggregation‐induced emission active tetraphenylethene (TPE), which effectively eliminates the detrimental π–π stacking interactions and thus helps Ru‐bpy surmount notorious ACQ effect in the aqueous phase. The Ru‐TPE shows negligible ECL emission in solution but produces a strong ECL emission upon crystallization. Surprisingly, the ECL efficiency of Ru‐TPE crystals is 20 and 3 times higher than that of its solution and Ru‐bpy crystals, respectively. Experimental and structural analysis reveals that such a CIE‐ECL effect originates from the restricted intramolecular rotation and ordered molecular packing. Moreover, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. This work provides a new design strategy for achieving high efficiency in solid‐state ECL imaging and devices. A new tris(bipyridine)ruthenium(II) derivative (Ru‐TPE) is synthesized and realizes the crystallization‐induced enhanced electrochemiluminescence (CIE‐ECL), which originates from the restricted intramolecular rotation and ordered molecular packing. Besides, the high‐resolution ECL imaging of a single Ru‐TPE crystal is successfully demonstrated. |
| Author | Zhu, Jun‐Jie Ma, Cheng Cao, Yue Han, Tingting Song, You Wang, Jia Jiao, Jianmin Wang, Leyong Chen, Hong‐Yuan |
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| Snippet | Classic tris(bipyridine)ruthenium(II) complex (Ru‐bpy) with high electrochemiluminescence (ECL) efficiency still suffers from a serious aggregation‐caused... |
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| SubjectTerms | Agglomeration Crystallization crystallization‐induced emissions Efficiency Electrochemiluminescence Emission Imaging Materials science Ruthenium Ruthenium compounds Structural analysis tetraphenylethene tris(bipyridine)ruthenium(II) derivatives |
| Title | Crystallization‐Induced Enhanced Electrochemiluminescence from a New Tris(bipyridine)ruthenium(II) Derivative |
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