Synthesis and Structural Characterization of Two Novel Copper(II) Schiff Base Complexes and their Water-Containing Supramolecular Structures
Two novel copper(II) complexes, Cu 2 L 2 (bipy) and Cu 2 L 2 (H 2 O) 4 ·3H 2 O of Schiff base ligands derived from the condensation of L- tert -leucine and L-isoleucine with 2,4-dihydroxybenzaldehyde, are synthesized and characterized by single crystal X-ray diffraction. Compounds crystallize in the...
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Published in | Journal of structural chemistry Vol. 60; no. 1; pp. 151 - 158 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Moscow
Pleiades Publishing
2019
Springer Nature B.V |
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Abstract | Two novel copper(II) complexes, Cu
2
L
2
(bipy) and Cu
2
L
2
(H
2
O)
4
·3H
2
O of Schiff base ligands derived from the condensation of L-
tert
-leucine and L-isoleucine with 2,4-dihydroxybenzaldehyde, are synthesized and characterized by single crystal X-ray diffraction. Compounds crystallize in the orthorhombic crystal system. The Cu
2
L
2
(bipy) complex has a
distorted square planar
geometry with an N
2
O
2
coordination environment. Water is contained in supramolecular network pores. On the other hand, in the Cu
2
L
2
(H
2
O)
4
·3H
2
O complex, both copper atoms adopt a five-coordinated
distorted square-pyramidal
geometry with an NO
4
coordination environment and guest water molecules form a 1D water chain. Both complexes build a 2D supramolecular network. |
---|---|
AbstractList | Two novel copper(II) complexes, Cu2L2(bipy) and Cu2L2(H2O)4·3H2O of Schiff base ligands derived from the condensation of L-tert-leucine and L-isoleucine with 2,4-dihydroxybenzaldehyde, are synthesized and characterized by single crystal X-ray diffraction. Compounds crystallize in the orthorhombic crystal system. The Cu2L2(bipy) complex has a distorted square planar geometry with an N2O2 coordination environment. Water is contained in supramolecular network pores. On the other hand, in the Cu2L2(H2O)4·3H2O complex, both copper atoms adopt a five-coordinated distorted square-pyramidal geometry with an NO4 coordination environment and guest water molecules form a 1D water chain. Both complexes build a 2D supramolecular network. Two novel copper(II) complexes, Cu 2 L 2 (bipy) and Cu 2 L 2 (H 2 O) 4 ·3H 2 O of Schiff base ligands derived from the condensation of L- tert -leucine and L-isoleucine with 2,4-dihydroxybenzaldehyde, are synthesized and characterized by single crystal X-ray diffraction. Compounds crystallize in the orthorhombic crystal system. The Cu 2 L 2 (bipy) complex has a distorted square planar geometry with an N 2 O 2 coordination environment. Water is contained in supramolecular network pores. On the other hand, in the Cu 2 L 2 (H 2 O) 4 ·3H 2 O complex, both copper atoms adopt a five-coordinated distorted square-pyramidal geometry with an NO 4 coordination environment and guest water molecules form a 1D water chain. Both complexes build a 2D supramolecular network. |
Author | Korkmaz, N. Barut Celepci, D. Astley, S. T. Aygün, M. |
Author_xml | – sequence: 1 givenname: D. surname: Barut Celepci fullname: Barut Celepci, D. email: duygu.barut@deu.edu.tr organization: Department of Physics, Faculty of Science, Dokuz Eylül University – sequence: 2 givenname: N. surname: Korkmaz fullname: Korkmaz, N. organization: Department of Chemistry, Faculty of Science, Ege University – sequence: 3 givenname: S. T. surname: Astley fullname: Astley, S. T. organization: Department of Chemistry, Faculty of Science, Ege University – sequence: 4 givenname: M. surname: Aygün fullname: Aygün, M. organization: Department of Physics, Faculty of Science, Dokuz Eylül University |
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Keywords | copper(II) complexes crystal structure Schiff bases hydrogen bonding supramolecular structure |
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Snippet | Two novel copper(II) complexes, Cu
2
L
2
(bipy) and Cu
2
L
2
(H
2
O)
4
·3H
2
O of Schiff base ligands derived from the condensation of L-
tert
-leucine and... Two novel copper(II) complexes, Cu2L2(bipy) and Cu2L2(H2O)4·3H2O of Schiff base ligands derived from the condensation of L-tert-leucine and L-isoleucine with... |
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SubjectTerms | Atomic Atomic/Molecular Structure and Spectra Chemistry Chemistry and Materials Science Coordination compounds Copper Copper compounds Crystals Imines Inorganic Chemistry Leucine Molecular Optical and Plasma Physics Physical Chemistry Single crystals Solid State Physics Structural analysis Water chemistry X-ray diffraction |
Title | Synthesis and Structural Characterization of Two Novel Copper(II) Schiff Base Complexes and their Water-Containing Supramolecular Structures |
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