Molten salt synthesis of (Zn, Mg) TiO3 micro/nano crystals with pure hexagonal ilmenite structure
The pure hexagonal phase (Zn, Mg) TiO 3 (abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt system and the heat treatment temperature on ZMT crystalline powders phase composition and particles morphology were studied. The results show tha...
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| Published in | Journal of materials science. Materials in electronics Vol. 27; no. 8; pp. 8319 - 8324 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.08.2016
Springer Nature B.V |
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| Abstract | The pure hexagonal phase (Zn, Mg) TiO
3
(abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt system and the heat treatment temperature on ZMT crystalline powders phase composition and particles morphology were studied. The results show that the formation of ZMT phase takes place at about 530 °C and the hexagonal phase stability region is 530–810 °C in KCl–NaCl salt system when MgCl
2
·6H
2
O taken in excess. Compared to the conventional solid phase process, the formation temperature of hexagonal ZMT via the molten salt method is lower. The ZMT powders prepared by the molten salt method are indicative more uniform grain size distribution and small grain size (the average grain size is about 150 nm). |
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| AbstractList | The pure hexagonal phase (Zn, Mg) TiO3 (abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt system and the heat treatment temperature on ZMT crystalline powders phase composition and particles morphology were studied. The results show that the formation of ZMT phase takes place at about 530 °C and the hexagonal phase stability region is 530-810 °C in KCl-NaCl salt system when MgCl2·6H2O taken in excess. Compared to the conventional solid phase process, the formation temperature of hexagonal ZMT via the molten salt method is lower. The ZMT powders prepared by the molten salt method are indicative more uniform grain size distribution and small grain size (the average grain size is about 150 nm). The pure hexagonal phase (Zn, Mg) TiO 3 (abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt system and the heat treatment temperature on ZMT crystalline powders phase composition and particles morphology were studied. The results show that the formation of ZMT phase takes place at about 530 °C and the hexagonal phase stability region is 530–810 °C in KCl–NaCl salt system when MgCl 2 ·6H 2 O taken in excess. Compared to the conventional solid phase process, the formation temperature of hexagonal ZMT via the molten salt method is lower. The ZMT powders prepared by the molten salt method are indicative more uniform grain size distribution and small grain size (the average grain size is about 150 nm). |
| Author | Zuo, Chenguang Liu, Xiangchun |
| Author_xml | – sequence: 1 givenname: Xiangchun surname: Liu fullname: Liu, Xiangchun email: liuxc@126.com organization: Department of Materials Science and Engineering, Xi’an University of Science and Technology – sequence: 2 givenname: Chenguang surname: Zuo fullname: Zuo, Chenguang organization: Department of Materials Science and Engineering, Xi’an University of Science and Technology |
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| Cites_doi | 10.1016/j.jeurceramsoc.2012.02.043 10.1016/j.jallcom.2008.03.090 10.1007/s10853-011-5984-8 10.1016/j.matlet.2012.04.048 10.1016/j.ceramint.2015.04.036 10.1016/j.materresbull.2007.03.029 10.1007/s10853-007-1807-3 10.1016/j.jallcom.2006.10.120 10.1007/s10853-010-4732-9 10.1016/j.powtec.2013.02.041 10.1016/j.ceramint.2015.04.111 10.1016/j.mseb.2011.01.013 10.1016/j.mseb.2013.09.002 10.1016/j.jeurceramsoc.2011.12.025 10.1016/j.ceramint.2004.09.017 10.1021/cg070232a 10.1111/j.1151-2916.1999.tb02268.x |
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| Keywords | Microwave Dielectric Property Hexagonal Phase Grain Size Distribution Molten Salt TiO2 |
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| Snippet | The pure hexagonal phase (Zn, Mg) TiO
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(abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt... The pure hexagonal phase (Zn, Mg) TiO3 (abbreviated to ZMT) micro/nano crystals were prepared by a molten salt method. The influences of the molten salt system... |
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| Title | Molten salt synthesis of (Zn, Mg) TiO3 micro/nano crystals with pure hexagonal ilmenite structure |
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