Preparation of chitosan modified fly ash under acid condition and its adsorption mechanism for Cr(VI) in water

Chitosan-coated fly ash (CWF) was prepared by the acid leaching-coating method. Chitosan and fly ash were crosslinked in the solution of acetic acid and sulfuric acid. The microstructure of CWF was conducted by scanning electron microscope (SEM) and X-ray diffraction (XRD). The removal of Cr(VI) fro...

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Published inJournal of Central South University Vol. 28; no. 6; pp. 1652 - 1664
Main Authors Jiang, Chun-lu, Wang, Rui, Chen, Xing, Zheng, Liu-gen, Cheng, Hua
Format Journal Article
LanguageEnglish
Published Changsha Central South University 01.06.2021
Springer Nature B.V
Subjects
Acetic acid
Adsorption
Ammonia
Chitosan
Crystal structure
Engineering
Fly ash
Functional groups
Liquid phases
Liquid surfaces
Metallic Materials
Silicon dioxide
Sulfuric acid leaching
Surface chemistry
Surface roughness
fly ash (CWF)
chitosan
adsorption
壳聚糖
改性
Cr(VI)
粉煤灰
吸附
六价铬
modification
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Abstract Chitosan-coated fly ash (CWF) was prepared by the acid leaching-coating method. Chitosan and fly ash were crosslinked in the solution of acetic acid and sulfuric acid. The microstructure of CWF was conducted by scanning electron microscope (SEM) and X-ray diffraction (XRD). The removal of Cr(VI) from water by CWF was studied by adsorption experiments. The composite prepared by the experiment developed a pore structure and a crystal structure similar to SiO 2 and chitosan chain-like coating was formed on the surface of fly ash. The new modified material has larger surface roughness, specific surface area and more adsorption channels. The Cr(VI) was enriched in modified materials by electrostatic adsorption between CrO 4 2− , CrO 7 2− and —NH 3 + group and surface acid functional groups. The movement of Cr(VI) in solution is a diffusion process from the main body of the liquid phase to the surface of the liquid film.
AbstractList Chitosan-coated fly ash (CWF) was prepared by the acid leaching-coating method. Chitosan and fly ash were crosslinked in the solution of acetic acid and sulfuric acid. The microstructure of CWF was conducted by scanning electron microscope (SEM) and X-ray diffraction (XRD). The removal of Cr(VI) from water by CWF was studied by adsorption experiments. The composite prepared by the experiment developed a pore structure and a crystal structure similar to SiO 2 and chitosan chain-like coating was formed on the surface of fly ash. The new modified material has larger surface roughness, specific surface area and more adsorption channels. The Cr(VI) was enriched in modified materials by electrostatic adsorption between CrO 4 2− , CrO 7 2− and —NH 3 + group and surface acid functional groups. The movement of Cr(VI) in solution is a diffusion process from the main body of the liquid phase to the surface of the liquid film.
Chitosan-coated fly ash (CWF) was prepared by the acid leaching-coating method. Chitosan and fly ash were crosslinked in the solution of acetic acid and sulfuric acid. The microstructure of CWF was conducted by scanning electron microscope (SEM) and X-ray diffraction (XRD). The removal of Cr(VI) from water by CWF was studied by adsorption experiments. The composite prepared by the experiment developed a pore structure and a crystal structure similar to SiO2 and chitosan chain-like coating was formed on the surface of fly ash. The new modified material has larger surface roughness, specific surface area and more adsorption channels. The Cr(VI) was enriched in modified materials by electrostatic adsorption between CrO42−, CrO72− and —NH3+ group and surface acid functional groups. The movement of Cr(VI) in solution is a diffusion process from the main body of the liquid phase to the surface of the liquid film.
Author Jiang, Chun-lu
Chen, Xing
Zheng, Liu-gen
Wang, Rui
Cheng, Hua
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  surname: Jiang
  fullname: Jiang, Chun-lu
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  organization: School of Resource and Environmental Engineering, Anhui Province Engineering Laboratory for Mine Ecological Remediation, Anhui University, College of Geoscience and Surveying Engineering, China University of Mining & Technology (Beijing)
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  givenname: Rui
  surname: Wang
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  organization: School of Resource and Environmental Engineering, Anhui Province Engineering Laboratory for Mine Ecological Remediation, Anhui University
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  givenname: Xing
  surname: Chen
  fullname: Chen, Xing
  organization: School of Resource and Environmental Engineering, Anhui Province Engineering Laboratory for Mine Ecological Remediation, Anhui University
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  givenname: Liu-gen
  surname: Zheng
  fullname: Zheng, Liu-gen
  organization: School of Resource and Environmental Engineering, Anhui Province Engineering Laboratory for Mine Ecological Remediation, Anhui University
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  givenname: Hua
  surname: Cheng
  fullname: Cheng, Hua
  organization: School of Resource and Environmental Engineering, Anhui Province Engineering Laboratory for Mine Ecological Remediation, Anhui University
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Issue 6
Keywords fly ash (CWF)
chitosan
adsorption
壳聚糖
改性
Cr(VI)
粉煤灰
吸附
六价铬
modification
Language English
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Snippet Chitosan-coated fly ash (CWF) was prepared by the acid leaching-coating method. Chitosan and fly ash were crosslinked in the solution of acetic acid and...
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SubjectTerms Acetic acid
Adsorption
Ammonia
Chitosan
Crystal structure
Engineering
Fly ash
Functional groups
Liquid phases
Liquid surfaces
Metallic Materials
Silicon dioxide
Sulfuric acid leaching
Surface chemistry
Surface roughness
Title Preparation of chitosan modified fly ash under acid condition and its adsorption mechanism for Cr(VI) in water
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Volume 28
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