Antibacterial Silicone-Urea/Organoclay Nanocomposites
Montmorillonite modified with distearyldimethyl ammonium chloride (C18-QAC) (Nanofil-15) (NF15) was incorporated into polydimethylsiloxane-urea (silicone-urea, PSU) copolymers. PSU was obtained by the reaction of equimolar amounts of aminopropyl terminated polydimethylsiloxane (PDMS) oligomer (<M...
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Published in | SILICON Vol. 1; no. 3; pp. 183 - 190 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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01.07.2009
Springer Nature B.V |
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Abstract | Montmorillonite modified with distearyldimethyl ammonium chloride (C18-QAC) (Nanofil-15) (NF15) was incorporated into polydimethylsiloxane-urea (silicone-urea, PSU) copolymers. PSU was obtained by the reaction of equimolar amounts of aminopropyl terminated polydimethylsiloxane (PDMS) oligomer (<M
n
> = 3,200 g/mol) and bis(4-isocyanatohexyl)methane (HMDI). A series of PSU/NF15 nanocomposites were prepared by solution blending with organoclay loadings ranging from 0.80 to 9.60% by weight, corresponding to 0.30 to 3.60% C18-QAC. Colloidal dispersions of organophilic clay (NF15) in isopropanol were mixed with the PSU solution in isopropanol and were subjected to ultrasonic treatment. Composite films were obtained by solution casting. FTIR spectroscopy confirmed that the organoclay mainly interacted with the urea groups but not with PDMS. XRD analysis showed that nanocomposites containing up to 6.40% by weight of organoclay had fully exfoliated silicate layers in the polymer matrix, whereas 9.60% loading had an intercalated structure. Physicochemical properties of nanocomposites were determined. PSU/NF15 nanocomposites displayed excellent long-term antibacterial properties against
E. coli
. |
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AbstractList | Montmorillonite modified with distearyldimethyl ammonium chloride (C18-QAC) (Nanofil-15) (NF15) was incorporated into polydimethylsiloxane-urea (silicone-urea, PSU) copolymers. PSU was obtained by the reaction of equimolar amounts of aminopropyl terminated polydimethylsiloxane (PDMS) oligomer ( = 3,200 g/mol) and bis(4-isocyanatohexyl)methane (HMDI). A series of PSU/NF15 nanocomposites were prepared by solution blending with organoclay loadings ranging from 0.80 to 9.60% by weight, corresponding to 0.30 to 3.60% C18-QAC. Colloidal dispersions of organophilic clay (NF15) in isopropanol were mixed with the PSU solution in isopropanol and were subjected to ultrasonic treatment. Composite films were obtained by solution casting. FTIR spectroscopy confirmed that the organoclay mainly interacted with the urea groups but not with PDMS. XRD analysis showed that nanocomposites containing up to 6.40% by weight of organoclay had fully exfoliated silicate layers in the polymer matrix, whereas 9.60% loading had an intercalated structure. Physicochemical properties of nanocomposites were determined. PSU/NF15 nanocomposites displayed excellent long-term antibacterial properties against E. coli. Montmorillonite modified with distearyldimethyl ammonium chloride (C18-QAC) (Nanofil-15) (NF15) was incorporated into polydimethylsiloxane-urea (silicone-urea, PSU) copolymers. PSU was obtained by the reaction of equimolar amounts of aminopropyl terminated polydimethylsiloxane (PDMS) oligomer (<M n > = 3,200 g/mol) and bis(4-isocyanatohexyl)methane (HMDI). A series of PSU/NF15 nanocomposites were prepared by solution blending with organoclay loadings ranging from 0.80 to 9.60% by weight, corresponding to 0.30 to 3.60% C18-QAC. Colloidal dispersions of organophilic clay (NF15) in isopropanol were mixed with the PSU solution in isopropanol and were subjected to ultrasonic treatment. Composite films were obtained by solution casting. FTIR spectroscopy confirmed that the organoclay mainly interacted with the urea groups but not with PDMS. XRD analysis showed that nanocomposites containing up to 6.40% by weight of organoclay had fully exfoliated silicate layers in the polymer matrix, whereas 9.60% loading had an intercalated structure. Physicochemical properties of nanocomposites were determined. PSU/NF15 nanocomposites displayed excellent long-term antibacterial properties against E. coli . |
Author | Nugay, Isik Isil Yilgor, Iskender Yilgor, Emel Bakan, Murat |
Author_xml | – sequence: 1 givenname: Emel surname: Yilgor fullname: Yilgor, Emel organization: Department of Chemistry, Koc University – sequence: 2 givenname: Isik Isil surname: Nugay fullname: Nugay, Isik Isil organization: Department of Chemical and Biochemical Engineering, Koc University – sequence: 3 givenname: Murat surname: Bakan fullname: Bakan, Murat organization: Department of Chemistry, Koc University – sequence: 4 givenname: Iskender surname: Yilgor fullname: Yilgor, Iskender email: iyilgor@ku.edu.tr organization: Department of Chemistry, Koc University |
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Keywords | Antibacterial Nanocomposites Organoclay Silicone Elastomer |
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SubjectTerms | Ammonium chloride Chemistry Chemistry and Materials Science Copolymers E coli Environmental Chemistry Inorganic Chemistry Isopropanol Lasers Materials Science Montmorillonite Nanocomposites Optical Devices Optics Original Paper Photonics Polydimethylsiloxane Polymer Sciences Silicones Solution blending Ultrasonic processing Ureas |
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Title | Antibacterial Silicone-Urea/Organoclay Nanocomposites |
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