Synthesis and Structure of New Rare Earth Cadmium Tellurite Halides
Single crystals of novel rare earth–cadmium tellurite halides, [Ln 12 (TeO 3 ) 12 ][Cd 6 X 24 ] (Ln = La, X = Cl ( 1 ); Ln = La, X= Br ( 2 ), and Ln = Pr, X = Br ( 3 )), were obtained from melts. All three compounds are isostructural to layered tellurite halides [Ln 12 (TeO 3 ) 12 ][Cd 6 Cl 24 ] (Ln...
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| Published in | Russian journal of inorganic chemistry Vol. 65; no. 4; pp. 466 - 471 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
01.04.2020
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Single crystals of novel rare earth–cadmium tellurite halides, [Ln
12
(TeO
3
)
12
][Cd
6
X
24
] (Ln = La, X = Cl (
1
); Ln = La, X= Br (
2
), and Ln = Pr, X = Br (
3
)), were obtained from melts. All three compounds are isostructural to layered tellurite halides [Ln
12
(TeO
3
)
12
][Cd
6
Cl
24
] (Ln = Sm, Eu), described earlier, and crystallize in space group
P
4/
nbm
with unit cell parameters
a
~ 16 Å and
c
~ 13 Å. Their crystal structures have been refined to
R
obs
= 0.052, 0.047, and 0.049, respectively. Bromides adopting this structure have been synthesized for the first time. Crystal-chemical features and prospects for development are discussed for the family of rare earth chalcogenite halides containing [Ln
11
M
x
(ChO
3
)
12
] rare earth–chalcogenite slabs. |
|---|---|
| AbstractList | Single crystals of novel rare earth–cadmium tellurite halides, [Ln
12
(TeO
3
)
12
][Cd
6
X
24
] (Ln = La, X = Cl (
1
); Ln = La, X= Br (
2
), and Ln = Pr, X = Br (
3
)), were obtained from melts. All three compounds are isostructural to layered tellurite halides [Ln
12
(TeO
3
)
12
][Cd
6
Cl
24
] (Ln = Sm, Eu), described earlier, and crystallize in space group
P
4/
nbm
with unit cell parameters
a
~ 16 Å and
c
~ 13 Å. Their crystal structures have been refined to
R
obs
= 0.052, 0.047, and 0.049, respectively. Bromides adopting this structure have been synthesized for the first time. Crystal-chemical features and prospects for development are discussed for the family of rare earth chalcogenite halides containing [Ln
11
M
x
(ChO
3
)
12
] rare earth–chalcogenite slabs. Single crystals of novel rare earth–cadmium tellurite halides, [Ln12(TeO3)12][Cd6X24] (Ln = La, X = Cl (1); Ln = La, X= Br (2), and Ln = Pr, X = Br (3)), were obtained from melts. All three compounds are isostructural to layered tellurite halides [Ln12(TeO3)12][Cd6Cl24] (Ln = Sm, Eu), described earlier, and crystallize in space group P4/nbm with unit cell parameters a ~ 16 Å and c ~ 13 Å. Their crystal structures have been refined to Robs = 0.052, 0.047, and 0.049, respectively. Bromides adopting this structure have been synthesized for the first time. Crystal-chemical features and prospects for development are discussed for the family of rare earth chalcogenite halides containing [Ln11Mx(ChO3)12] rare earth–chalcogenite slabs. |
| Author | Dolgikh, V. A. Volkov, S. N. Charkin, D. O. Grishaev, V. Yu |
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| Snippet | Single crystals of novel rare earth–cadmium tellurite halides, [Ln
12
(TeO
3
)
12
][Cd
6
X
24
] (Ln = La, X = Cl (
1
); Ln = La, X= Br (
2
), and Ln = Pr, X =... Single crystals of novel rare earth–cadmium tellurite halides, [Ln12(TeO3)12][Cd6X24] (Ln = La, X = Cl (1); Ln = La, X= Br (2), and Ln = Pr, X = Br (3)), were... |
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| SubjectTerms | Bromides Bromine Cadmium Chemistry Chemistry and Materials Science Crystal structure Crystals Earth Halides Inorganic Chemistry Lanthanum Single crystals Synthesis and Properties of Inorganic Compounds Tellurium dioxide Unit cell |
| Title | Synthesis and Structure of New Rare Earth Cadmium Tellurite Halides |
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