Detection of Gasoline Residues Present in Household Materials Via Headspace-solid Phase Microextraction and Gas Chromatography‒mass Spectrometry
This paper describes the detection and persistence of gasoline residues present in household materials, cotton fabric, cardboard, and carpet. These samples were spiked with 50 μL of gasoline and dried for a controlled period of time at room temperature prior to chemical analysis. The extraction and...
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| Published in | Journal of analytical chemistry (New York, N.Y.) Vol. 75; no. 1; pp. 44 - 55 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
2020
Springer Nature B.V |
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| Online Access | Get full text |
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| Abstract | This paper describes the detection and persistence of gasoline residues present in household materials, cotton fabric, cardboard, and carpet. These samples were spiked with 50 μL of gasoline and dried for a controlled period of time at room temperature prior to chemical analysis. The extraction and chemical analysis of gasoline residues were conducted via headspace-solid phase microextraction and gas chromatography‒mass spectrometry, respectively. Our data showed that gasoline residues were detected in the cotton fabric samples after up to 7 days of drying, while both the cardboard and carpet samples could retain gasoline residues for longer than 3 weeks. The adoption of small-sized vials for headspace analysis improved the detection limit of gasoline residues in the samples. The physical features of the samples, such as porosity, thickness, and number of layers, were found to be more important than chemical compositions for the increased persistence of gasoline residues. |
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| AbstractList | This paper describes the detection and persistence of gasoline residues present in household materials, cotton fabric, cardboard, and carpet. These samples were spiked with 50 μL of gasoline and dried for a controlled period of time at room temperature prior to chemical analysis. The extraction and chemical analysis of gasoline residues were conducted via headspace-solid phase microextraction and gas chromatography‒mass spectrometry, respectively. Our data showed that gasoline residues were detected in the cotton fabric samples after up to 7 days of drying, while both the cardboard and carpet samples could retain gasoline residues for longer than 3 weeks. The adoption of small-sized vials for headspace analysis improved the detection limit of gasoline residues in the samples. The physical features of the samples, such as porosity, thickness, and number of layers, were found to be more important than chemical compositions for the increased persistence of gasoline residues. |
| Author | Michael J. Swierczynski Kim, Joonyeong Grau, Kelly Schmitz, Michelli |
| Author_xml | – sequence: 1 surname: Michael J. Swierczynski fullname: Michael J. Swierczynski organization: Department of Chemistry, Buffalo State, State University of New York – sequence: 2 givenname: Kelly surname: Grau fullname: Grau, Kelly organization: Department of Chemistry, Buffalo State, State University of New York – sequence: 3 givenname: Michelli surname: Schmitz fullname: Schmitz, Michelli organization: Erie County Central Police Services – sequence: 4 givenname: Joonyeong surname: Kim fullname: Kim, Joonyeong email: kimj@buffalostate.edu organization: Department of Chemistry, Buffalo State, State University of New York |
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| Keywords | gasoline residues persistence mass spectrometry solid phase microextraction headspace gas chromatography |
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| Snippet | This paper describes the detection and persistence of gasoline residues present in household materials, cotton fabric, cardboard, and carpet. These samples... |
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| SubjectTerms | Analytical Chemistry Cardboard Chemical analysis Chemical composition Chemistry Chemistry and Materials Science Chromatography Cotton Cotton fabrics Gas chromatography Gasoline Mass spectrometry Organic chemistry Porosity Residues Room temperature Scientific imaging Solid phases Spectroscopy Thickness |
| Title | Detection of Gasoline Residues Present in Household Materials Via Headspace-solid Phase Microextraction and Gas Chromatography‒mass Spectrometry |
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