Precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment
The precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for quantitatively evaluating the content of δ phase was proposed based on SEM micrograph, which was verified by X-ray diffraction (XRD) analysis...
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| Published in | Applied physics. A, Materials science & processing Vol. 125; no. 6; pp. 1 - 14 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Berlin/Heidelberg
Springer Berlin Heidelberg
01.06.2019
Springer Nature B.V |
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| Abstract | The precipitation and dissolution behaviors of
δ
phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for quantitatively evaluating the content of
δ
phase was proposed based on SEM micrograph, which was verified by X-ray diffraction (XRD) analysis. The effects of recrystallization during pre-annealing at 980 °C on the precipitation and dissolution behaviors of
δ
phase in the subsequent annealing treatment at 900 °C and 980 °C are discussed. Moreover, the improved precipitation and dissolution kinetics models are proposed to consider the effects of recrystallization fraction. The results show that: (1) for the precipitation of
δ
phase at 900 °C,
δ
phases precipitate first in grain boundaries and then within grains after a long incubation period. Moreover, the interval between adjacent
δ
phases increases first and then drops with the increasing recrystallization fraction during pre-annealing treatment. A balance between the precipitation and solution of
δ
phase at the aging temperature of 900 °C can be reached when the holding time is about 12 h; (2) for the dissolution of
δ
phase at 980 °C, the dissolution equilibrium can be obtained at approximate 200 min. Moreover, more rod-like
δ
phases can be remained with the increasing recrystallization fraction in pre-annealing treatment. |
|---|---|
| AbstractList | The precipitation and dissolution behaviors of
δ
phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for quantitatively evaluating the content of
δ
phase was proposed based on SEM micrograph, which was verified by X-ray diffraction (XRD) analysis. The effects of recrystallization during pre-annealing at 980 °C on the precipitation and dissolution behaviors of
δ
phase in the subsequent annealing treatment at 900 °C and 980 °C are discussed. Moreover, the improved precipitation and dissolution kinetics models are proposed to consider the effects of recrystallization fraction. The results show that: (1) for the precipitation of
δ
phase at 900 °C,
δ
phases precipitate first in grain boundaries and then within grains after a long incubation period. Moreover, the interval between adjacent
δ
phases increases first and then drops with the increasing recrystallization fraction during pre-annealing treatment. A balance between the precipitation and solution of
δ
phase at the aging temperature of 900 °C can be reached when the holding time is about 12 h; (2) for the dissolution of
δ
phase at 980 °C, the dissolution equilibrium can be obtained at approximate 200 min. Moreover, more rod-like
δ
phases can be remained with the increasing recrystallization fraction in pre-annealing treatment. The precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for quantitatively evaluating the content of δ phase was proposed based on SEM micrograph, which was verified by X-ray diffraction (XRD) analysis. The effects of recrystallization during pre-annealing at 980 °C on the precipitation and dissolution behaviors of δ phase in the subsequent annealing treatment at 900 °C and 980 °C are discussed. Moreover, the improved precipitation and dissolution kinetics models are proposed to consider the effects of recrystallization fraction. The results show that: (1) for the precipitation of δ phase at 900 °C, δ phases precipitate first in grain boundaries and then within grains after a long incubation period. Moreover, the interval between adjacent δ phases increases first and then drops with the increasing recrystallization fraction during pre-annealing treatment. A balance between the precipitation and solution of δ phase at the aging temperature of 900 °C can be reached when the holding time is about 12 h; (2) for the dissolution of δ phase at 980 °C, the dissolution equilibrium can be obtained at approximate 200 min. Moreover, more rod-like δ phases can be remained with the increasing recrystallization fraction in pre-annealing treatment. |
| ArticleNumber | 447 |
| Author | Zou, Zong-Huai Chen, Ming-Song Lin, Y. C. He, Dao-Guang Wang, Guan-Qiang Ma, Yan-Yong Li, Hong-Bin Zeng, Wei-Dong |
| Author_xml | – sequence: 1 givenname: Ming-Song surname: Chen fullname: Chen, Ming-Song email: chenms18@csu.edu.cn organization: School of Mechanical and Electrical Engineering, Central South University, Light Alloy Research Institute of Central South University – sequence: 2 givenname: Guan-Qiang surname: Wang fullname: Wang, Guan-Qiang organization: School of Mechanical and Electrical Engineering, Central South University, State Key Laboratory of High Performance Complex Manufacturing – sequence: 3 givenname: Hong-Bin surname: Li fullname: Li, Hong-Bin organization: School of Mechanical and Electrical Engineering, Central South University, College of Metallurgies and Energy, North China Science and Technologies University – sequence: 4 givenname: Y. C. surname: Lin fullname: Lin, Y. C. email: yclin@csu.edu.cn organization: School of Mechanical and Electrical Engineering, Central South University, Light Alloy Research Institute of Central South University, State Key Laboratory of High Performance Complex Manufacturing – sequence: 5 givenname: Zong-Huai surname: Zou fullname: Zou, Zong-Huai organization: School of Mechanical and Electrical Engineering, Central South University, State Key Laboratory of High Performance Complex Manufacturing – sequence: 6 givenname: Yan-Yong surname: Ma fullname: Ma, Yan-Yong organization: School of Mechanical and Electrical Engineering, Central South University, State Key Laboratory of High Performance Complex Manufacturing – sequence: 7 givenname: Dao-Guang surname: He fullname: He, Dao-Guang organization: School of Mechanical and Electrical Engineering, Central South University, Light Alloy Research Institute of Central South University – sequence: 8 givenname: Wei-Dong surname: Zeng fullname: Zeng, Wei-Dong organization: School of Mechanical and Electrical Engineering, Central South University, State Key Laboratory of High Performance Complex Manufacturing |
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δ
phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for... The precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for... |
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| SubjectTerms | Annealing Applied physics Characterization and Evaluation of Materials Chemical precipitation Condensed Matter Physics Deformation Dissolution Grain boundaries Machines Manufacturing Materials science Nanotechnology Nickel Nickel base alloys Optical and Electronic Materials Phases Photomicrographs Physics Physics and Astronomy Processes Reaction kinetics Recrystallization Superalloys Surfaces and Interfaces Thin Films X-ray diffraction |
| Title | Precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment |
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