Developing hierarchical CdS/NiO hollow heterogeneous architectures for boosting photocatalytic hydrogen generation

The hierarchical binary CdS/NiO hollow heterogeneous architectures (HHAs) with p-n heterojunction are constructed by a facile microwave-assisted wet chemical process for high-efficient photocatalytic hydrogen evolution reaction (HER) from water. The asdesigned CdS/NiO HHAs are composed of hexagonal...

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Published in	Nano research Vol. 15; no. 3; pp. 2003 - 2012
Main Authors	Deng, Chonghai, Ye, Fan, Wang, Tao, Ling, Xiaohui, Peng, Lulu, Yu, Hong, Ding, Kangzhe, Hu, Hanmei, Dong, Qiang, Le, Huirong, Han, Yongsheng
Format	Journal Article
Language	English
Published	Beijing Tsinghua University Press 01.03.2022
Subjects	Atomic/Molecular Structure and Spectra Biomedicine Biotechnology Chemistry and Materials Science Condensed Matter Physics Electromagnetic absorption Heterojunctions Hydrogen Hydrogen evolution reactions Hydrogen production Irradiation Materials Science Microspheres Morphology Nanoparticles Nanotechnology Nickel oxides P-n junctions Photocatalysis Research Article Solar energy Synergistic effect Thickness Water splitting CdS nanoparticls NiO hollow microspheres photocatalytic hydrogen evolution p-n heterojunction hierarchical structure
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Abstract	The hierarchical binary CdS/NiO hollow heterogeneous architectures (HHAs) with p-n heterojunction are constructed by a facile microwave-assisted wet chemical process for high-efficient photocatalytic hydrogen evolution reaction (HER) from water. The asdesigned CdS/NiO HHAs are composed of hexagonal n-type CdS nanoparticles with a size in the range of 20–40 nm attaching to cubic p-type NiO hollow microspheres (HMSs) which are aggregates of porous nanoplates with a thickness of about 20 nm. The photocatalytic water splitting over CdS/NiO HHAs is significantly increased under simulated solar irradiation, among which the most active sample of CdS/NiO-3 (the mass ratio of CdS to NiO is 1:3) exhibits the fastest photocatalytic HER rate of 1.77 mmol·g −1 ·h −1 , being 16.2 times than that of pure CdS. The boosted photocatalytic HER could be attributed to the synergistic effect on the proportional p-n heterojunction with special hierarchical hollow and porous morphology, an enhancement of visible light absorption, and an improvement of photoinduced charge separation as well as the photo-stability given by the composite heterojunction. This work shows a viable strategy to design the heterojunction with special morphology for the efficient hydrogen generation by water splitting utilizing solar energy.
AbstractList	The hierarchical binary CdS/NiO hollow heterogeneous architectures (HHAs) with p-n heterojunction are constructed by a facile microwave-assisted wet chemical process for high-efficient photocatalytic hydrogen evolution reaction (HER) from water. The asdesigned CdS/NiO HHAs are composed of hexagonal n-type CdS nanoparticles with a size in the range of 20–40 nm attaching to cubic p-type NiO hollow microspheres (HMSs) which are aggregates of porous nanoplates with a thickness of about 20 nm. The photocatalytic water splitting over CdS/NiO HHAs is significantly increased under simulated solar irradiation, among which the most active sample of CdS/NiO-3 (the mass ratio of CdS to NiO is 1:3) exhibits the fastest photocatalytic HER rate of 1.77 mmol·g−1·h−1, being 16.2 times than that of pure CdS. The boosted photocatalytic HER could be attributed to the synergistic effect on the proportional p-n heterojunction with special hierarchical hollow and porous morphology, an enhancement of visible light absorption, and an improvement of photoinduced charge separation as well as the photo-stability given by the composite heterojunction. This work shows a viable strategy to design the heterojunction with special morphology for the efficient hydrogen generation by water splitting utilizing solar energy. The hierarchical binary CdS/NiO hollow heterogeneous architectures (HHAs) with p-n heterojunction are constructed by a facile microwave-assisted wet chemical process for high-efficient photocatalytic hydrogen evolution reaction (HER) from water. The asdesigned CdS/NiO HHAs are composed of hexagonal n-type CdS nanoparticles with a size in the range of 20–40 nm attaching to cubic p-type NiO hollow microspheres (HMSs) which are aggregates of porous nanoplates with a thickness of about 20 nm. The photocatalytic water splitting over CdS/NiO HHAs is significantly increased under simulated solar irradiation, among which the most active sample of CdS/NiO-3 (the mass ratio of CdS to NiO is 1:3) exhibits the fastest photocatalytic HER rate of 1.77 mmol·g −1 ·h −1 , being 16.2 times than that of pure CdS. The boosted photocatalytic HER could be attributed to the synergistic effect on the proportional p-n heterojunction with special hierarchical hollow and porous morphology, an enhancement of visible light absorption, and an improvement of photoinduced charge separation as well as the photo-stability given by the composite heterojunction. This work shows a viable strategy to design the heterojunction with special morphology for the efficient hydrogen generation by water splitting utilizing solar energy.
Author	Peng, Lulu Dong, Qiang Le, Huirong Ding, Kangzhe Han, Yongsheng Deng, Chonghai Wang, Tao Ling, Xiaohui Ye, Fan Yu, Hong Hu, Hanmei
Author_xml	– sequence: 1 givenname: Chonghai surname: Deng fullname: Deng, Chonghai email: chdeng@hfuu.edu.cn organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 2 givenname: Fan surname: Ye fullname: Ye, Fan organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 3 givenname: Tao surname: Wang fullname: Wang, Tao organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 4 givenname: Xiaohui surname: Ling fullname: Ling, Xiaohui organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 5 givenname: Lulu surname: Peng fullname: Peng, Lulu organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 6 givenname: Hong surname: Yu fullname: Yu, Hong organization: Anhui Province Key Laboratory of Advanced Building Materials, Anhui Jianzhu University – sequence: 7 givenname: Kangzhe surname: Ding fullname: Ding, Kangzhe organization: Anhui Province Key Laboratory of Advanced Building Materials, Anhui Jianzhu University – sequence: 8 givenname: Hanmei surname: Hu fullname: Hu, Hanmei organization: Anhui Province Key Laboratory of Advanced Building Materials, Anhui Jianzhu University – sequence: 9 givenname: Qiang surname: Dong fullname: Dong, Qiang email: qdong@hfuu.edu.cn organization: School of Energy Materials and Chemical Engineering, Hefei University – sequence: 10 givenname: Huirong surname: Le fullname: Le, Huirong organization: The Future Lab, Tsinghua University – sequence: 11 givenname: Yongsheng surname: Han fullname: Han, Yongsheng email: yshan@ipe.ac.cn organization: State Key Laboratory of Multiphase Complex Systems, Institute of Process Engineering, Chinese Academy of Sciences
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Snippet	The hierarchical binary CdS/NiO hollow heterogeneous architectures (HHAs) with p-n heterojunction are constructed by a facile microwave-assisted wet chemical...
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SubjectTerms	Atomic/Molecular Structure and Spectra Biomedicine Biotechnology Chemistry and Materials Science Condensed Matter Physics Electromagnetic absorption Heterojunctions Hydrogen Hydrogen evolution reactions Hydrogen production Irradiation Materials Science Microspheres Morphology Nanoparticles Nanotechnology Nickel oxides P-n junctions Photocatalysis Research Article Solar energy Synergistic effect Thickness Water splitting
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Title	Developing hierarchical CdS/NiO hollow heterogeneous architectures for boosting photocatalytic hydrogen generation
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