3D derived N-doped carbon matrix from 2D ZIF-L as an enhanced stable catalyst for chemical fixation
3D metal N-doped carbon frameworks (M-NCFs) are produced from the direct pyrolysis of 2D zeolitic imidazolate frameworks (ZIF-L Zn and Co) in a reducing atmosphere. The effects of the thermal treatment were studied in order to achieve the desired catalyst. The results show that metal nanoparticles a...
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| Published in | Microporous and mesoporous materials Vol. 285; pp. 80 - 88 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.09.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | 3D metal N-doped carbon frameworks (M-NCFs) are produced from the direct pyrolysis of 2D zeolitic imidazolate frameworks (ZIF-L Zn and Co) in a reducing atmosphere. The effects of the thermal treatment were studied in order to achieve the desired catalyst. The results show that metal nanoparticles and N-doping species present in the carbon matrix have a direct influence on the catalytic performance. Zn/NCF-1000 displayed quantitative conversion and selectivity towards the chemical fixation of carbon dioxide through the cycloaddition with epoxides. Furthermore, the magnetic property of the newly synthesized Co/NCF-600 was used to demonstrate its superior stability and recyclability, retaining the same catalytic activity for more than 10 cycles.
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•3D Zn/NCFs and Co/NCFs derived from 2D ZIF-L crystals were easily prepared.•Comparative study of the different M/NCFs as function of the thermal treatment.•Zn/NCF-1000 and Co/NCF-600 are excellent catalysts for CO2 fixation.•Enhanced structural stability ensures 10 recycles without activity loss. |
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| AbstractList | 3D metal N-doped carbon frameworks (M-NCFs) are produced from the direct pyrolysis of 2D zeolitic imidazolate frameworks (ZIF-L Zn and Co) in a reducing atmosphere. The effects of the thermal treatment were studied in order to achieve the desired catalyst. The results show that metal nanoparticles and N-doping species present in the carbon matrix have a direct influence on the catalytic performance. Zn/NCF-1000 displayed quantitative conversion and selectivity towards the chemical fixation of carbon dioxide through the cycloaddition with epoxides. Furthermore, the magnetic property of the newly synthesized Co/NCF-600 was used to demonstrate its superior stability and recyclability, retaining the same catalytic activity for more than 10 cycles.
[Display omitted]
•3D Zn/NCFs and Co/NCFs derived from 2D ZIF-L crystals were easily prepared.•Comparative study of the different M/NCFs as function of the thermal treatment.•Zn/NCF-1000 and Co/NCF-600 are excellent catalysts for CO2 fixation.•Enhanced structural stability ensures 10 recycles without activity loss. |
| Author | Wang, Tingting Tu, Rong Zhuiykov, Serge Chaemchuen, Somboon Ruiz, Karla Hernandez Ciprian, Matteo Kassymova, Meruyert Verpoort, Francis |
| Author_xml | – sequence: 1 givenname: Matteo surname: Ciprian fullname: Ciprian, Matteo organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 2 givenname: Karla Hernandez surname: Ruiz fullname: Ruiz, Karla Hernandez organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 3 givenname: Meruyert surname: Kassymova fullname: Kassymova, Meruyert organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 4 givenname: Tingting surname: Wang fullname: Wang, Tingting organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 5 givenname: Serge surname: Zhuiykov fullname: Zhuiykov, Serge organization: Ghent University Global Campus Songdo, 119 Songdomunhwa-Ro, Yeonsu-Gu, Incheon, 406-840, South Korea – sequence: 6 givenname: Somboon surname: Chaemchuen fullname: Chaemchuen, Somboon organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 7 givenname: Rong surname: Tu fullname: Tu, Rong organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China – sequence: 8 givenname: Francis orcidid: 0000-0002-5184-5500 surname: Verpoort fullname: Verpoort, Francis email: francis.verpoort@ku.ac.ae organization: State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, China |
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| Keywords | ZIF-L Pyrolysis Heterogeneous catalyst CO2 fixation Carbonates |
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| Snippet | 3D metal N-doped carbon frameworks (M-NCFs) are produced from the direct pyrolysis of 2D zeolitic imidazolate frameworks (ZIF-L Zn and Co) in a reducing... |
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| SubjectTerms | Carbonates CO2 fixation Heterogeneous catalyst Pyrolysis ZIF-L |
| Title | 3D derived N-doped carbon matrix from 2D ZIF-L as an enhanced stable catalyst for chemical fixation |
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