Room-Temperature Synthesis of Sn2P2S6

• Published in: Journal of solid state chemistry Vol. 129; no. 1; pp. 157 - 159
• Main Authors: Bourdon, X., Prouzet, E., Cajipe, V.B.
• Format: Journal Article
• Language: English
• Published: San Diego, CA Elsevier Inc 15.02.1997; Elsevier
• Subjects: Chemistry; Exact sciences and technology; Inorganic chemistry and origins of life; Preparations and properties; Salts; Tin Thiophosphates; Chemical preparation; Room temperature

Twenty-nanometer particles of Sn2P2S6are prepared at room temperature (RT) via a metathesis reaction in aqueous media. Mössbauer and Raman spectroscopy and X-ray diffraction characterization of these powders accord with data on Sn2P2S6synthesized at high temperature (HT). The phase transition and se...