Molten salt synthesis of carbon anode for high-performance sodium-ion batteries
•Carbon materials were prepared in an easy, efficient and low-temperature way.•Molten salt promoted the reaction effectively in dynamics.•Carbon materials presented the characteristics of highly porous and disordered.•Carbon materials exhibited excellent performance superior to many carbon anodes.•C...
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| Published in | Electrochimica acta Vol. 447; p. 142150 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
10.04.2023
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| Subjects | |
| Online Access | Get full text |
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| Abstract | •Carbon materials were prepared in an easy, efficient and low-temperature way.•Molten salt promoted the reaction effectively in dynamics.•Carbon materials presented the characteristics of highly porous and disordered.•Carbon materials exhibited excellent performance superior to many carbon anodes.•CO2 can be utilized as a raw material to synthesize carbon materials.
Preparation of high-performance anode materials in a convenient, efficient and environment friendly way is a challenge for the commercialization of sodium-ion batteries (SIBs). Herein, a carbon material was fabricated via a facile reaction between CaC2 and CaCO3 in CaCl2NaCl molten salt. The microstructure of the carbon materials was systemically characterized and the electrochemical performance was investigated. By optimizing temperature and duration, the carbon product has porous and disordered structures. These characteristics facilitate the reversible capacity of Na storage. The optimized carbon anode exhibits excellent rate capabilities (179 and 129 mAh·g−1 at 5 and 20 A·g−1, respectively) and high reversible capacities (295 mAh·g−1 at a low current density of 0.1 A·g−1). The carbon anode also presents attractive stability with 0.0275% capacity decay per cycle at 5 A·g−1 over 1000 cycles. Furthermore, the utilization of this route to transform CO2 to high-performance carbon anode was evaluated. |
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| AbstractList | •Carbon materials were prepared in an easy, efficient and low-temperature way.•Molten salt promoted the reaction effectively in dynamics.•Carbon materials presented the characteristics of highly porous and disordered.•Carbon materials exhibited excellent performance superior to many carbon anodes.•CO2 can be utilized as a raw material to synthesize carbon materials.
Preparation of high-performance anode materials in a convenient, efficient and environment friendly way is a challenge for the commercialization of sodium-ion batteries (SIBs). Herein, a carbon material was fabricated via a facile reaction between CaC2 and CaCO3 in CaCl2NaCl molten salt. The microstructure of the carbon materials was systemically characterized and the electrochemical performance was investigated. By optimizing temperature and duration, the carbon product has porous and disordered structures. These characteristics facilitate the reversible capacity of Na storage. The optimized carbon anode exhibits excellent rate capabilities (179 and 129 mAh·g−1 at 5 and 20 A·g−1, respectively) and high reversible capacities (295 mAh·g−1 at a low current density of 0.1 A·g−1). The carbon anode also presents attractive stability with 0.0275% capacity decay per cycle at 5 A·g−1 over 1000 cycles. Furthermore, the utilization of this route to transform CO2 to high-performance carbon anode was evaluated. |
| ArticleNumber | 142150 |
| Author | Ning, Zhiqiang Chen, Denghui Xu, Qian Xie, Hongwei Song, Qiushi Zhao, Hengpeng Zhao, Jie Yu, Kai |
| Author_xml | – sequence: 1 givenname: Qiushi orcidid: 0000-0002-4039-8194 surname: Song fullname: Song, Qiushi email: songqs@smm.neu.edu.cn organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 2 givenname: Hengpeng surname: Zhao fullname: Zhao, Hengpeng organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 3 givenname: Jie surname: Zhao fullname: Zhao, Jie organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 4 givenname: Denghui surname: Chen fullname: Chen, Denghui organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 5 givenname: Qian surname: Xu fullname: Xu, Qian organization: Shanghai Key Laboratory of Advanced Ferrometallurgy, Shanghai University, Shanghai, China – sequence: 6 givenname: Hongwei orcidid: 0000-0001-6530-5006 surname: Xie fullname: Xie, Hongwei organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 7 givenname: Zhiqiang surname: Ning fullname: Ning, Zhiqiang organization: School of Metallurgy, Northeastern University, Shenyang, China – sequence: 8 givenname: Kai orcidid: 0000-0002-0565-4690 surname: Yu fullname: Yu, Kai organization: School of Metallurgy, Northeastern University, Shenyang, China |
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| Keywords | High performance CaC2/CaCO3 Carbon anode Molten salt synthesis Sodium-ion batteries |
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| SubjectTerms | CaC2/CaCO3 Carbon anode High performance Molten salt synthesis Sodium-ion batteries |
| Title | Molten salt synthesis of carbon anode for high-performance sodium-ion batteries |
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