Robust iron-doped nickel phosphides in membrane-electrode assembly for industrial water electrolysis
Water electrolysis, a pivotal process for the production of green hydrogen, is a crucial step toward realizing the hydrogen economy. To advance its industrialization, it is essential to develop a highly efficient and economical catalyst along with a low-resistance electrolyzers. In pursuit of this g...
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| Published in | Electrochimica acta Vol. 500; p. 144744 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Water electrolysis, a pivotal process for the production of green hydrogen, is a crucial step toward realizing the hydrogen economy. To advance its industrialization, it is essential to develop a highly efficient and economical catalyst along with a low-resistance electrolyzers. In pursuit of this goal, we synthesize a cost-effective iron-doped nickel phosphide electrocatalyst through a hydrothermal synthesis followed by post-phosphorization process. This catalyst exhibits exceptional performance, with an overpotential at 10 mA cm-2 (η10) of 216 mV for oxygen evolution reaction, the rate-determining step for water electrolysis. It overperforms the that of pristine nickel phosphide (NiPx, η10 = 284 mV). Operando X-ray absorption spectroscopy reveals the robust nature of the iron-doped nickel phosphide catalyst during water electrolysis, in stark contrast to the pristine nickel phosphide, which undergoes oxidation, thereby impacting overall catalytic activity. When integrated into a membrane-electrode assembly (MEA) system, our iron-doped nickel phosphide displays voltages of 1.51 V at 10 mA cm-2 (EE = 81.5%) and 1.66 V at 100 mA cm-2 (EE = 76.4%) without iR-correction. Moreover, it achieves a current density of 345 mA cm-2 at an applied voltage of 2 V without iR-correction, meeting industrial criteria. These findings underscore the superior catalytic activity of the robust phosphide phase for water electrolysis. |
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| AbstractList | Water electrolysis, a pivotal process for the production of green hydrogen, is a crucial step toward realizing the hydrogen economy. To advance its industrialization, it is essential to develop a highly efficient and economical catalyst along with a low-resistance electrolyzers. In pursuit of this goal, we synthesize a cost-effective iron-doped nickel phosphide electrocatalyst through a hydrothermal synthesis followed by post-phosphorization process. This catalyst exhibits exceptional performance, with an overpotential at 10 mA cm-2 (η10) of 216 mV for oxygen evolution reaction, the rate-determining step for water electrolysis. It overperforms the that of pristine nickel phosphide (NiPx, η10 = 284 mV). Operando X-ray absorption spectroscopy reveals the robust nature of the iron-doped nickel phosphide catalyst during water electrolysis, in stark contrast to the pristine nickel phosphide, which undergoes oxidation, thereby impacting overall catalytic activity. When integrated into a membrane-electrode assembly (MEA) system, our iron-doped nickel phosphide displays voltages of 1.51 V at 10 mA cm-2 (EE = 81.5%) and 1.66 V at 100 mA cm-2 (EE = 76.4%) without iR-correction. Moreover, it achieves a current density of 345 mA cm-2 at an applied voltage of 2 V without iR-correction, meeting industrial criteria. These findings underscore the superior catalytic activity of the robust phosphide phase for water electrolysis. |
| ArticleNumber | 144744 |
| Author | Chen, Yi-Yu Lu, Ying-Rui Hsu, Yung-Hsi Shao, Yu-Cheng Hung, Sung-Fu Chueh, Yu-Ting Hsu, Shao-Hui Liu, Yu-Chun Ma, Jian-Jie Peng, Kang-Shun Hu, Chih-Wei |
| Author_xml | – sequence: 1 givenname: Jian-Jie surname: Ma fullname: Ma, Jian-Jie organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 2 givenname: Yu-Ting surname: Chueh fullname: Chueh, Yu-Ting organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 3 givenname: Yi-Yu surname: Chen fullname: Chen, Yi-Yu organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 4 givenname: Yung-Hsi surname: Hsu fullname: Hsu, Yung-Hsi organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 5 givenname: Yu-Chun surname: Liu fullname: Liu, Yu-Chun organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 6 givenname: Kang-Shun surname: Peng fullname: Peng, Kang-Shun organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan – sequence: 7 givenname: Chih-Wei surname: Hu fullname: Hu, Chih-Wei organization: National Synchrotron Radiation Research Center, Hsinchu 300, Taiwan – sequence: 8 givenname: Ying-Rui surname: Lu fullname: Lu, Ying-Rui organization: National Synchrotron Radiation Research Center, Hsinchu 300, Taiwan – sequence: 9 givenname: Yu-Cheng surname: Shao fullname: Shao, Yu-Cheng organization: National Synchrotron Radiation Research Center, Hsinchu 300, Taiwan – sequence: 10 givenname: Shao-Hui surname: Hsu fullname: Hsu, Shao-Hui organization: Taiwan Semiconductor Research Institute, National Applied Research Laboratories, Hsinchu 300, Taiwan – sequence: 11 givenname: Sung-Fu surname: Hung fullname: Hung, Sung-Fu email: sungfuhung@nycu.edu.tw organization: Department of Applied Chemistry and Center for Emergent Functional Matter Science, National Yang Ming Chiao Tung University, Hsinchu 300, Taiwan |
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| Title | Robust iron-doped nickel phosphides in membrane-electrode assembly for industrial water electrolysis |
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