Crystal Structure and Hydrogen Storage Behaviors of Mg/MoS2 Composites from Ball Milling
The Mg/MoS2 composites were prepared by ball milling under argon atmosphere,and the effect of MoS2 on the crystal structure and hydrogen storage properties of Mg was investigated.It is found that 10 wt% of MoS2 is sufficient to prevent particle aggregation and cold welding during the milling process...
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| Published in | Journal of Wuhan University of Technology. Materials science edition Vol. 31; no. 4; pp. 773 - 778 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Wuhan
Wuhan University of Technology
01.08.2016
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| Abstract | The Mg/MoS2 composites were prepared by ball milling under argon atmosphere,and the effect of MoS2 on the crystal structure and hydrogen storage properties of Mg was investigated.It is found that 10 wt% of MoS2 is sufficient to prevent particle aggregation and cold welding during the milling process.The crystallite size of Mg will remain constant at slightly less than 38.8 nm with the milling process due to the size confinement effect of MoS2.The dehydrogenation temperature of MgH2 is reduced to 390.4-429.4 ℃ due to the crystallite size reduction.Through fitting by Johnson-Mehl-Avrami model,it is found that Mg crystal grows by three dimension controlled by interface transformation during the process of MgH2 decomposition.MoS2 has a weak catalyst effect on the decomposition of MgH2 and activation energy of 148.9 k J/mol is needed for the dehydrogenation process calculated by the Arrhenius equation. |
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| AbstractList | The Mg/MoS
2
composites were prepared by ball milling under argon atmosphere, and the effect of MoS
2
on the crystal structure and hydrogen storage properties of Mg was investigated. It is found that 10 wt% of MoS
2
is sufficient to prevent particle aggregation and cold welding during the milling process. The crystallite size of Mg will remain constant at slightly less than 38.8 nm with the milling process due to the size confinement effect of MoS
2
. The dehydrogenation temperature of MgH
2
is reduced to 390.4-429.4 °C due to the crystallite size reduction. Through fitting by Johnson-Mehl-Avrami model, it is found that Mg crystal grows by three dimension controlled by interface transformation during the process of MgH
2
decomposition. MoS
2
has a weak catalyst effect on the decomposition of MgH
2
and activation energy of 148.9 kJ/mol is needed for the dehydrogenation process calculated by the Arrhenius equation. The Mg/MoS2 composites were prepared by ball milling under argon atmosphere,and the effect of MoS2 on the crystal structure and hydrogen storage properties of Mg was investigated.It is found that 10 wt% of MoS2 is sufficient to prevent particle aggregation and cold welding during the milling process.The crystallite size of Mg will remain constant at slightly less than 38.8 nm with the milling process due to the size confinement effect of MoS2.The dehydrogenation temperature of MgH2 is reduced to 390.4-429.4 ℃ due to the crystallite size reduction.Through fitting by Johnson-Mehl-Avrami model,it is found that Mg crystal grows by three dimension controlled by interface transformation during the process of MgH2 decomposition.MoS2 has a weak catalyst effect on the decomposition of MgH2 and activation energy of 148.9 k J/mol is needed for the dehydrogenation process calculated by the Arrhenius equation. |
| Author | HAN Zongying 周仕学 WANG Naifei ZHANG Qianqian ZHANG Tonghuan RAN Weixian |
| AuthorAffiliation | College of Chemical and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266590, China School of Chemical and Environmental Engineering, China University of Mining and Technology, Beijing 100083, China |
| Author_xml | – sequence: 1 givenname: Zongying surname: Han fullname: Han, Zongying organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology, School of Chemical and Environmental Engineering, China University of Mining and Technology – sequence: 2 givenname: Shixue surname: Zhou fullname: Zhou, Shixue email: zhoushixue66@163.com organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology – sequence: 3 givenname: Naifei surname: Wang fullname: Wang, Naifei organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology – sequence: 4 givenname: Qianqian surname: Zhang fullname: Zhang, Qianqian organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology – sequence: 5 givenname: Tonghuan surname: Zhang fullname: Zhang, Tonghuan organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology – sequence: 6 givenname: Weixian surname: Ran fullname: Ran, Weixian organization: College of Chemical and Environmental Engineering, Shandong University of Science and Technology |
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| Cites_doi | 10.1038/35025020 10.1016/j.cattod.2006.09.022 10.1016/j.jallcom.2013.12.246 10.1021/ja201269b 10.1016/0043-1648(72)90124-X 10.1016/j.electacta.2004.02.001 10.1038/35104634 10.1016/S0925-8388(99)00474-0 10.1002/er.1284 10.1016/j.ijhydene.2012.12.018 10.1016/S0921-5093(01)01767-1 10.1039/B802882F 10.1016/0040-6031(95)02466-2 10.1021/ja710667v 10.1016/j.pmatsci.2012.07.001 10.1063/1.325832 10.1063/1.1750872 10.1016/j.corsci.2010.06.028 10.1016/S0079-6425(99)00010-9 10.1016/j.ijhydene.2006.11.022 10.1016/j.fuel.2012.09.002 10.1103/PhysRev.56.978 10.1007/s11244-006-0014-9 10.1016/S0040-6031(01)00769-9 10.1039/b921645f 10.1016/j.ijhydene.2009.08.088 10.1016/0360-3199(84)90152-6 10.1016/S0925-8388(99)00073-0 10.1016/0043-1648(67)90187-1 10.1021/ed061p494 10.1016/0043-1648(72)90416-4 |
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| Keywords | crystal structure molybdenum disulfide decomposition kinetics dehydrogenation temperature |
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| Notes | crystallite milling confinement aggregation fitting argon agglomeration magnesium subsequent hydrogenation 42-1680/TB The Mg/MoS2 composites were prepared by ball milling under argon atmosphere,and the effect of MoS2 on the crystal structure and hydrogen storage properties of Mg was investigated.It is found that 10 wt% of MoS2 is sufficient to prevent particle aggregation and cold welding during the milling process.The crystallite size of Mg will remain constant at slightly less than 38.8 nm with the milling process due to the size confinement effect of MoS2.The dehydrogenation temperature of MgH2 is reduced to 390.4-429.4 ℃ due to the crystallite size reduction.Through fitting by Johnson-Mehl-Avrami model,it is found that Mg crystal grows by three dimension controlled by interface transformation during the process of MgH2 decomposition.MoS2 has a weak catalyst effect on the decomposition of MgH2 and activation energy of 148.9 k J/mol is needed for the dehydrogenation process calculated by the Arrhenius equation. |
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| Snippet | The Mg/MoS2 composites were prepared by ball milling under argon atmosphere,and the effect of MoS2 on the crystal structure and hydrogen storage properties of... The Mg/MoS 2 composites were prepared by ball milling under argon atmosphere, and the effect of MoS 2 on the crystal structure and hydrogen storage properties... |
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| SubjectTerms | Advanced Materials Avrami模型 Chemistry and Materials Science Materials Science MgH2 二硫化钼 储氢性能 复合材料 晶体结构 晶粒尺寸 脱氢工艺 |
| Title | Crystal Structure and Hydrogen Storage Behaviors of Mg/MoS2 Composites from Ball Milling |
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