A green route of isobutane-butene alkylation catalyzed by Y zeolite modified with synergistic F-containing solution
Fast deactivation is a long-standing problem for zeolite catalyzed isobutane-butene alkylation that hinders its massive industrialization, and the optimization of the zeolites' acidity and pore structure is the key problem. A synergistic F-containing solution modification method was proposed to...
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| Published in | Microporous and mesoporous materials Vol. 364; p. 112874 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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15.01.2024
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| Abstract | Fast deactivation is a long-standing problem for zeolite catalyzed isobutane-butene alkylation that hinders its massive industrialization, and the optimization of the zeolites' acidity and pore structure is the key problem. A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the zeolites’ acidity. The low-temperature ammonium fluoride treatment precise partly opened the cage windows of the zeolites to increase the acidity accessibility and diffusion performance. And the following acid treatment of ammonium fluosilicate effectively removed the extra-framework aluminum generated by the former treatment to achieve a high acidity and Brönsted acid amount to Lewis acid amount ratio. The best modified zeolite Y-11 has a lifetime of 60 h, which is 32% higher compared to that of the reference zeolite. Our primary results provide a promising strategy for designing superior zeolite catalysts for alkylation reactions.
A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the zeolites' acidity, which have promoted the catalyst's alkylation stability. [Display omitted]
•A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the acidity.•The ammonium fluoride treatment precise opened the cage windows of the zeolites to increase the acidity accessibility and diffusion.•The best modified zeolite Y-11 has a lifetime of 60 h, which is 32% higher compared to that of the reference zeolite. |
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| AbstractList | Fast deactivation is a long-standing problem for zeolite catalyzed isobutane-butene alkylation that hinders its massive industrialization, and the optimization of the zeolites' acidity and pore structure is the key problem. A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the zeolites’ acidity. The low-temperature ammonium fluoride treatment precise partly opened the cage windows of the zeolites to increase the acidity accessibility and diffusion performance. And the following acid treatment of ammonium fluosilicate effectively removed the extra-framework aluminum generated by the former treatment to achieve a high acidity and Brönsted acid amount to Lewis acid amount ratio. The best modified zeolite Y-11 has a lifetime of 60 h, which is 32% higher compared to that of the reference zeolite. Our primary results provide a promising strategy for designing superior zeolite catalysts for alkylation reactions.
A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the zeolites' acidity, which have promoted the catalyst's alkylation stability. [Display omitted]
•A synergistic F-containing solution modification method was proposed to improve the diffusion performance without damaging the acidity.•The ammonium fluoride treatment precise opened the cage windows of the zeolites to increase the acidity accessibility and diffusion.•The best modified zeolite Y-11 has a lifetime of 60 h, which is 32% higher compared to that of the reference zeolite. |
| ArticleNumber | 112874 |
| Author | Lin, Meng Li, Yongxiang Zhou, Shunli Zhang, Chengxi Shu, Xingtian |
| Author_xml | – sequence: 1 givenname: Chengxi orcidid: 0000-0003-3641-3467 surname: Zhang fullname: Zhang, Chengxi email: zhangcx.ripp@sinopec.com – sequence: 2 givenname: Meng surname: Lin fullname: Lin, Meng – sequence: 3 givenname: Shunli surname: Zhou fullname: Zhou, Shunli – sequence: 4 givenname: Yongxiang surname: Li fullname: Li, Yongxiang email: liyx.ripp@sinopec.com – sequence: 5 givenname: Xingtian surname: Shu fullname: Shu, Xingtian |
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| Keywords | Zeolite Y Isobutane-butene alkylation Cage window Diffusion performance Synergistic F-containing solution modification |
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| SubjectTerms | Cage window Diffusion performance Isobutane-butene alkylation Synergistic F-containing solution modification Zeolite Y |
| Title | A green route of isobutane-butene alkylation catalyzed by Y zeolite modified with synergistic F-containing solution |
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