SYSTHESIS OF DOUBLE-HYDROPHILIC CORE-SHELL TYPE MULTIARM STAR COPOLYMER POLYETHYLENIMINE-block-POLY（2-HYDROXYETHYL METHACRYLATE）
Multiarm star block copolymers hyperbranched polyethylenimine-b-poly（2-hydroxyethyl methacrylate） （HPEI-b- PHEMA） with average 28 PHEMA arms have been prepared by atom transfer radical polymerization （ATRP） of HEMA in a mixed solvent of methanol and water using a core-first strategy. The hyperbranch...
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| Published in | Chinese journal of polymer science Vol. 31; no. 7; pp. 1046 - 1055 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Heidelberg
Chinese Chemical Society and Institute of Chemistry, CAS
01.07.2013
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| Abstract | Multiarm star block copolymers hyperbranched polyethylenimine-b-poly（2-hydroxyethyl methacrylate） （HPEI-b- PHEMA） with average 28 PHEMA arms have been prepared by atom transfer radical polymerization （ATRP） of HEMA in a mixed solvent of methanol and water using a core-first strategy. The hyperbranched macroinitiator employed was prepared on the basis of well-defined hyperbranched polyethylenimine with Mw/Mn of 1.04 by amidation with 2-bromo-isobutyryl bromide. The polymerization condition was optimized to prepare star copolymers with narrow dispersity, and the variables included the volume ratio of methanol to water, the molar ratio of initiating site to CuC1 and the molar ratio of [CuCl]：[CuBr2]. Under the optimized polymerization condition, the lowest Mw/Mn value of the obtained star copolymers was around 1.3. Kinetic analysis showed that an induction period existed in the polymerization of HEMA. After this induction period, a linear dependence of ln（[M]0/[M]t） on time was observed. The obtained HPEI-b-PHEMA could adsorb hydrophilic molecules. The comparison with the star copolymer with hydrophobic core and hydrophilic PHEMA shell verified that both the hydrophilic core and shell could host the hydrophilic guests, but the amidated HPEI core was more effective than the PHEMA shell. |
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| AbstractList | Multiarm star block copolymers hyperbranched polyethylenimine-b-poly（2-hydroxyethyl methacrylate） （HPEI-b- PHEMA） with average 28 PHEMA arms have been prepared by atom transfer radical polymerization （ATRP） of HEMA in a mixed solvent of methanol and water using a core-first strategy. The hyperbranched macroinitiator employed was prepared on the basis of well-defined hyperbranched polyethylenimine with Mw/Mn of 1.04 by amidation with 2-bromo-isobutyryl bromide. The polymerization condition was optimized to prepare star copolymers with narrow dispersity, and the variables included the volume ratio of methanol to water, the molar ratio of initiating site to CuC1 and the molar ratio of [CuCl]：[CuBr2]. Under the optimized polymerization condition, the lowest Mw/Mn value of the obtained star copolymers was around 1.3. Kinetic analysis showed that an induction period existed in the polymerization of HEMA. After this induction period, a linear dependence of ln（[M]0/[M]t） on time was observed. The obtained HPEI-b-PHEMA could adsorb hydrophilic molecules. The comparison with the star copolymer with hydrophobic core and hydrophilic PHEMA shell verified that both the hydrophilic core and shell could host the hydrophilic guests, but the amidated HPEI core was more effective than the PHEMA shell. Multiarm star block copolymers hyperbranched polyethylenimine- b -poly(2-hydroxyethyl methacrylate) (HPEI- b -PHEMA) with average 28 PHEMA arms have been prepared by atom transfer radical polymerization (ATRP) of HEMA in a mixed solvent of methanol and water using a core-first strategy. The hyperbranched macroinitiator employed was prepared on the basis of well-defined hyperbranched polyethylenimine with M w / M n of 1.04 by amidation with 2-bromo-isobutyryl bromide. The polymerization condition was optimized to prepare star copolymers with narrow dispersity, and the variables included the volume ratio of methanol to water, the molar ratio of initiating site to CuCl and the molar ratio of [CuCl]:[CuBr 2 ]. Under the optimized polymerization condition, the lowest M w / M n value of the obtained star copolymers was around 1.3. Kinetic analysis showed that an induction period existed in the polymerization of HEMA. After this induction period, a linear dependence of ln([M] 0 /[M] t ) on time was observed. The obtained HPEI- b -PHEMA could adsorb hydrophilic molecules. The comparison with the star copolymer with hydrophobic core and hydrophilic PHEMA shell verified that both the hydrophilic core and shell could host the hydrophilic guests, but the amidated HPEI core was more effective than the PHEMA shell. |
| Author | Qiang Tang Fa Cheng Jin Cui Yu Chen |
| AuthorAffiliation | School of Chemical and Environmental Engineering, Hubei University of Technology, Wuhan 430068, China Department of Chemistry, School of Sciences, Tianfin University, Tianjin 300072, China National Foodstuff lnspection Center, Tianjin Product Quality Inspection Technology Research Institute, Tianjin 300384, China |
| Author_xml | – sequence: 1 givenname: Qiang surname: Tang fullname: Tang, Qiang organization: School of Chemical and Environmental Engineering, Hubei University of Technology – sequence: 2 givenname: Fa surname: Cheng fullname: Cheng, Fa organization: Department of Chemistry, School of Sciences, Tianjin University – sequence: 3 givenname: Jin surname: Cui fullname: Cui, Jin organization: National Foodstuff Inspection Center, Tianjin Product Quality Inspection Technology Research Institute – sequence: 4 givenname: Yu surname: Chen fullname: Chen, Yu email: chenyu@tju.edu.cn organization: Department of Chemistry, School of Sciences, Tianjin University |
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| CitedBy_id | crossref_primary_10_4028_www_scientific_net_MSF_956_218 crossref_primary_10_1016_j_polymer_2015_01_059 crossref_primary_10_1007_s10118_015_1651_x crossref_primary_10_1007_s10118_014_1481_2 crossref_primary_10_1002_marc_201300513 |
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| Keywords | Atom transfer radical polymerization Star polymers Polyethylenimine Hyperbranched Poly(2-hydroxyethyl methacrylate) |
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| Notes | Multiarm star block copolymers hyperbranched polyethylenimine-b-poly（2-hydroxyethyl methacrylate） （HPEI-b- PHEMA） with average 28 PHEMA arms have been prepared by atom transfer radical polymerization （ATRP） of HEMA in a mixed solvent of methanol and water using a core-first strategy. The hyperbranched macroinitiator employed was prepared on the basis of well-defined hyperbranched polyethylenimine with Mw/Mn of 1.04 by amidation with 2-bromo-isobutyryl bromide. The polymerization condition was optimized to prepare star copolymers with narrow dispersity, and the variables included the volume ratio of methanol to water, the molar ratio of initiating site to CuC1 and the molar ratio of [CuCl]：[CuBr2]. Under the optimized polymerization condition, the lowest Mw/Mn value of the obtained star copolymers was around 1.3. Kinetic analysis showed that an induction period existed in the polymerization of HEMA. After this induction period, a linear dependence of ln（[M]0/[M]t） on time was observed. The obtained HPEI-b-PHEMA could adsorb hydrophilic molecules. The comparison with the star copolymer with hydrophobic core and hydrophilic PHEMA shell verified that both the hydrophilic core and shell could host the hydrophilic guests, but the amidated HPEI core was more effective than the PHEMA shell. Atom transfer radical polymerization; Hyperbranched; Polyethylenimine; Poly（2-hydroxyethyl methacrylate）; Star polymers. 11-2015/O6 |
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| PublicationTitle | Chinese journal of polymer science |
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| Snippet | Multiarm star block copolymers hyperbranched polyethylenimine-b-poly（2-hydroxyethyl methacrylate） （HPEI-b- PHEMA） with average 28 PHEMA arms have been prepared... Multiarm star block copolymers hyperbranched polyethylenimine- b -poly(2-hydroxyethyl methacrylate) (HPEI- b -PHEMA) with average 28 PHEMA arms have been... |
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| SubjectTerms | Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Condensed Matter Physics GPC Industrial Chemistry/Chemical Engineering Polymer Sciences 化学 化学分子式 高分子化学 |
| Title | SYSTHESIS OF DOUBLE-HYDROPHILIC CORE-SHELL TYPE MULTIARM STAR COPOLYMER POLYETHYLENIMINE-block-POLY（2-HYDROXYETHYL METHACRYLATE） |
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