SULFONATED POLYIMIDES CONTAINING PYRIDINE GROUPS AS PROTON EXCHANGE MEMBRANE MATERIALS
A series of sulfonated polyimides （SPIs） containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic dianhydride （NTDA）, 4,4＇-diaminodiphenyl ether-2,2＇-disulfonic acid （ODADS） and 4-（4-methoxy）phenyl-2,6-bis（4-aminophenyl）pyridine （DAM）. The resulting...
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| Published in | Chinese journal of polymer science Vol. 29; no. 5; pp. 532 - 539 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
Chinese Chemical Society and Institute of Chemistry, CAS
01.09.2011
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| Subjects | |
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| Abstract | A series of sulfonated polyimides （SPIs） containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic dianhydride （NTDA）, 4,4＇-diaminodiphenyl ether-2,2＇-disulfonic acid （ODADS） and 4-（4-methoxy）phenyl-2,6-bis（4-aminophenyl）pyridine （DAM）. The resulting copolymers displayed good solubility in common organic solvents. Flexible, transparent, tough membranes were obtained via solution casting. All the films showed high thermal stability with desulfonation temperature over 300℃. They exhibited prominent mechanical properties with Young＇s modulus around 2.0 GPa. High proton conductivity （0.23 S/cm at 100% RH） was also observed. More importantly, the new materials exhibited low water uptake （30 wt%-75 wt% at 80℃） and improved water stability, which were attributed to the acid-base interaction between sulfonic acid and pyridine functional groups. |
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| AbstractList | A series of sulfonated polyimides (SPIs) containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic dianhydride (NTDA), 4,4′-diaminodiphenyl ether-2,2′-disulfonic acid (ODADS) and 4-(4-methoxy)phenyl-2,6-bis(4-aminophenyl)pyridine (DAM). The resulting copolymers displayed good solubility in common organic solvents. Flexible, transparent, tough membranes were obtained
via
solution casting. All the films showed high thermal stability with desulfonation temperature over 300°C. They exhibited prominent mechanical properties with Young’s modulus around 2.0 GPa. High proton conductivity (0.23 S/cm at 100% RH) was also observed. More importantly, the new materials exhibited low water uptake (30 wt%–75 wt% at 80°C) and improved water stability, which were attributed to the acid-base interaction between sulfonic acid and pyridine functional groups. A series of sulfonated polyimides （SPIs） containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic dianhydride （NTDA）, 4,4＇-diaminodiphenyl ether-2,2＇-disulfonic acid （ODADS） and 4-（4-methoxy）phenyl-2,6-bis（4-aminophenyl）pyridine （DAM）. The resulting copolymers displayed good solubility in common organic solvents. Flexible, transparent, tough membranes were obtained via solution casting. All the films showed high thermal stability with desulfonation temperature over 300℃. They exhibited prominent mechanical properties with Young＇s modulus around 2.0 GPa. High proton conductivity （0.23 S/cm at 100% RH） was also observed. More importantly, the new materials exhibited low water uptake （30 wt%-75 wt% at 80℃） and improved water stability, which were attributed to the acid-base interaction between sulfonic acid and pyridine functional groups. |
| Author | Rui Lei Chuan-qing Kang Yun-jie Huang Xue-peng Qiu Xiang-ling Ji Wei Xing Lian-xun Gao |
| AuthorAffiliation | State Key Laboratory of Polymer Physics and Chemistry, Changehun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China Graduate School of the Chinese Academy of Sciences, Beijing 100049, China |
| Author_xml | – sequence: 1 givenname: Rui surname: Lei fullname: Lei, Rui organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Graduate School of the Chinese Academy of Sciences – sequence: 2 givenname: Chuan-qing surname: Kang fullname: Kang, Chuan-qing organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Graduate School of the Chinese Academy of Sciences – sequence: 3 givenname: Yun-jie surname: Huang fullname: Huang, Yun-jie organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Graduate School of the Chinese Academy of Sciences – sequence: 4 givenname: Xue-peng surname: Qiu fullname: Qiu, Xue-peng organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences – sequence: 5 givenname: Xiang-ling surname: Ji fullname: Ji, Xiang-ling organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences – sequence: 6 givenname: Wei surname: Xing fullname: Xing, Wei organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences – sequence: 7 givenname: Lian-xun surname: Gao fullname: Gao, Lian-xun email: lxgao@ciac.jl.cn organization: State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences |
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| Keywords | Acid-base interaction Proton conductivity Pyridine Sulfonated polyimide |
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| Notes | A series of sulfonated polyimides （SPIs） containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic dianhydride （NTDA）, 4,4＇-diaminodiphenyl ether-2,2＇-disulfonic acid （ODADS） and 4-（4-methoxy）phenyl-2,6-bis（4-aminophenyl）pyridine （DAM）. The resulting copolymers displayed good solubility in common organic solvents. Flexible, transparent, tough membranes were obtained via solution casting. All the films showed high thermal stability with desulfonation temperature over 300℃. They exhibited prominent mechanical properties with Young＇s modulus around 2.0 GPa. High proton conductivity （0.23 S/cm at 100% RH） was also observed. More importantly, the new materials exhibited low water uptake （30 wt%-75 wt% at 80℃） and improved water stability, which were attributed to the acid-base interaction between sulfonic acid and pyridine functional groups. Sulfonated polyimide; Pyridine; Acid-base interaction; Proton conductivity. ： Sulfonated polyimide; Pyridine; Acid-base interaction; Proton conductivity. 11-2015/O6 |
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| PublicationTitle | Chinese journal of polymer science |
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| Publisher | Chinese Chemical Society and Institute of Chemistry, CAS |
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| Snippet | A series of sulfonated polyimides （SPIs） containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic... A series of sulfonated polyimides (SPIs) containing pyridine groups were prepared by direct polycondensation from 1,4,5,8-naphthalenetetracarboxylic... |
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| SubjectTerms | Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Condensed Matter Physics Industrial Chemistry/Chemical Engineering Polymer Sciences 二氨基二苯醚 吡啶 氨基苯基 直接缩聚 磺化聚酰亚胺 膜材料 质子交换 质子传导率 |
| Title | SULFONATED POLYIMIDES CONTAINING PYRIDINE GROUPS AS PROTON EXCHANGE MEMBRANE MATERIALS |
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