In situ damage precursor detection in fiber reinforced composites using anthracene-based mechanophore
A pioneering approach to in situ damage precursor detection in fiber reinforced polymer composites is developed using anthracene-based stress-sensitive mechanophore material. In this research, the anthracene-based mechanophore, which emits ultraviolet (UV) excited fluorescence on chemical bond break...
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Published in | Smart materials and structures Vol. 28; no. 11; pp. 115035 - 115045 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
IOP Publishing
01.11.2019
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Subjects | |
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Abstract | A pioneering approach to in situ damage precursor detection in fiber reinforced polymer composites is developed using anthracene-based stress-sensitive mechanophore material. In this research, the anthracene-based mechanophore, which emits ultraviolet (UV) excited fluorescence on chemical bond breakage under the influence of external mechanical loads, is effectually used as a nanoscale damage sensor. Dimeric 9-anthracene carboxylic acid (Di-AC) is synthesized and incorporated into glass fiber reinforced polymer (GFRP) composites through a hand layup process. A quasi-static uniaxial tensile load is applied to the specimens, and UV excited fluorescence from the activated Di-AC mechanophore during the tensile loading tests is captured through UV camera. The results indicate that the activation of Di-AC starts at a very early stage in the tests ( 0.33% strain for single-ply and 0.5% strain for three-ply laminate specimens) and exhibits a linear increase prior to failure ( 1.6% strain for single-ply and 2.28% strain for three-ply laminate specimens). Nonlinear optical response is captured when the specimen is close to failure. The mechanophore response to interlaminar damage is also investigated using composite specimens with induced delamination. The potential of anthracene-based mechanophore for early damage detection as well as barely visible damage detection in GFRP is successfully demonstrated. |
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AbstractList | A pioneering approach to in situ damage precursor detection in fiber reinforced polymer composites is developed using anthracene-based stress-sensitive mechanophore material. In this research, the anthracene-based mechanophore, which emits ultraviolet (UV) excited fluorescence on chemical bond breakage under the influence of external mechanical loads, is effectually used as a nanoscale damage sensor. Dimeric 9-anthracene carboxylic acid (Di-AC) is synthesized and incorporated into glass fiber reinforced polymer (GFRP) composites through a hand layup process. A quasi-static uniaxial tensile load is applied to the specimens, and UV excited fluorescence from the activated Di-AC mechanophore during the tensile loading tests is captured through UV camera. The results indicate that the activation of Di-AC starts at a very early stage in the tests ( 0.33% strain for single-ply and 0.5% strain for three-ply laminate specimens) and exhibits a linear increase prior to failure ( 1.6% strain for single-ply and 2.28% strain for three-ply laminate specimens). Nonlinear optical response is captured when the specimen is close to failure. The mechanophore response to interlaminar damage is also investigated using composite specimens with induced delamination. The potential of anthracene-based mechanophore for early damage detection as well as barely visible damage detection in GFRP is successfully demonstrated. |
Author | Koo, Bonsung Miller, Jack Gunckel, Ryan Hall, Asha Chattopadhyay, Aditi Dai, Lenore |
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Cites_doi | 10.1038/nchem.1720 10.1021/ja1008932 10.1021/ja9036548 10.1002/admi.201601018 10.1038/nature07970 10.1088/2053-1591/3/3/035701 10.1021/ma4014862 10.1021/ma500598t 10.1039/c3ta14803c 10.1002/adfm.201302341 10.1166/jnn.2010.2953 10.1038/pj.2012.18 10.1021/am100050v 10.1021/cm049394+ 10.1016/j.polymer.2014.06.019 10.1021/mz500031q 10.1039/c0jm04015k 10.1039/c0jm03967e 10.1039/c0jm04117c 10.1021/ja2086728 10.1002/adma.201205226 10.1038/nchem.1358 |
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References | 22 23 Zou J (17) 2014; 23 (24) 2008 Nofen E M (20) 2016; 3 10 11 12 13 14 15 16 18 19 1 2 3 4 5 6 7 8 9 21 Piccardi M (25) 2004 |
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SubjectTerms | damage precursor dimeric anthracene glass fiber reinforced polymer composites mechanophore thermoset |
Title | In situ damage precursor detection in fiber reinforced composites using anthracene-based mechanophore |
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