One-Step Synthesis of TiN/C Nanocomposites for the Sensitive Determination of Ofloxacin
Regulating the heterostructure of electrode materials has a great influence on electron migration and subsequent electrochemical reactions, which play a critical role in the sensing process. Herein, a facile method has been demonstrated to synthesize TiN/graphitic carbon (TiN/gC) nanocomposites by t...
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Published in | Journal of the Electrochemical Society Vol. 169; no. 8; pp. 87512 - 87518 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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01.08.2022
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Abstract | Regulating the heterostructure of electrode materials has a great influence on electron migration and subsequent electrochemical reactions, which play a critical role in the sensing process. Herein, a facile method has been demonstrated to synthesize TiN/graphitic carbon (TiN/gC) nanocomposites by the in situ growth of TiN nanoparticles on C nanosheets. The formation of TiN/gC heterojunctions was evidenced by X-ray diffraction (XRD), Raman microscopy and transmission electron microscopy (TEM). This heterostructure can effectively facilitate electron transfer and increase the electrochemically active area, which improves the electrocatalytic performance. Interestingly, the TiN/gC-modified glassy carbon electrode (TiN-gC/GCE) exhibited excellent electrocatalytic activity toward ofloxacin (OFLX) redox. With the change in the OFLX concentration, the electrochemical response of the sensor also changes. By using a differential pulse voltammetry (DPV) technique, the designed sensor showed a wide detection range: the DPV response was linearly dependent on the concentrations in the range of 0.05 – 1.0 and 1.0 – 100
μ
M. Moreover, TiN-gC/GCE demonstrated outstanding analytical performances in the quantitative OFLX assay, such as a high sensitivity of 2876
μ
A·mM
−1
·cm
–2
, low detection limit of 0.016
μ
M, good selectivity and stability. The proposed method was successfully applied for OFLX detection in eye drops and environmental water with satisfactory results. |
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AbstractList | Regulating the heterostructure of electrode materials has a great influence on electron migration and subsequent electrochemical reactions, which play a critical role in the sensing process. Herein, a facile method has been demonstrated to synthesize TiN/graphitic carbon (TiN/gC) nanocomposites by the in situ growth of TiN nanoparticles on C nanosheets. The formation of TiN/gC heterojunctions was evidenced by X-ray diffraction (XRD), Raman microscopy and transmission electron microscopy (TEM). This heterostructure can effectively facilitate electron transfer and increase the electrochemically active area, which improves the electrocatalytic performance. Interestingly, the TiN/gC-modified glassy carbon electrode (TiN-gC/GCE) exhibited excellent electrocatalytic activity toward ofloxacin (OFLX) redox. With the change in the OFLX concentration, the electrochemical response of the sensor also changes. By using a differential pulse voltammetry (DPV) technique, the designed sensor showed a wide detection range: the DPV response was linearly dependent on the concentrations in the range of 0.05 – 1.0 and 1.0 – 100
μ
M. Moreover, TiN-gC/GCE demonstrated outstanding analytical performances in the quantitative OFLX assay, such as a high sensitivity of 2876
μ
A·mM
−1
·cm
–2
, low detection limit of 0.016
μ
M, good selectivity and stability. The proposed method was successfully applied for OFLX detection in eye drops and environmental water with satisfactory results. |
Author | Wang, Chensheng Jing, Huan Long, Yumei Li, Weifeng |
Author_xml | – sequence: 1 givenname: Chensheng surname: Wang fullname: Wang, Chensheng organization: The Key Lab of Health Chemistry and Molecular Diagnosis of Suzhou, Suzhou 215123, People’s Republic of China – sequence: 2 givenname: Huan surname: Jing fullname: Jing, Huan organization: The Key Lab of Health Chemistry and Molecular Diagnosis of Suzhou, Suzhou 215123, People’s Republic of China – sequence: 3 givenname: Weifeng orcidid: 0000-0002-8497-8166 surname: Li fullname: Li, Weifeng organization: Soochow University College of Chemistry, Chemical engineering and Materials Science, Suzhou 215123, People’s Republic of China – sequence: 4 givenname: Yumei surname: Long fullname: Long, Yumei organization: The Key Lab of Health Chemistry and Molecular Diagnosis of Suzhou, Suzhou 215123, People’s Republic of China |
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