Nickel decorated MoO3 single crystal microflakes with multi-site functionality for enhanced hydrogen evolution reaction
Role of hybrid material with metal-oxide interface has been explored by coating 2 nm nickel on α-MoO3 single crystals for hydrogen evolution reaction (HER). The investigated aspects reveal that α-MoO3/Ni hybrid exhibits a remarkable performance in HER showing +6 mV onset potential and 37 mV overpote...
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| Published in | International journal of hydrogen energy Vol. 46; no. 2; pp. 1945 - 1954 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
06.01.2021
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| Subjects | |
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| Abstract | Role of hybrid material with metal-oxide interface has been explored by coating 2 nm nickel on α-MoO3 single crystals for hydrogen evolution reaction (HER). The investigated aspects reveal that α-MoO3/Ni hybrid exhibits a remarkable performance in HER showing +6 mV onset potential and 37 mV overpotential at 10 mA/cm2 current density along with Tafel slope of 47 mV/dec. The single crystalline-stepped CVD-grown MoO3 microflakes having the advantage of higher hydrogen binding energy of Ni exhibits the enhanced catalytic performance due to strong electronic coupling at the metal-oxide interface and hydrogen spill over effect. Similar hybrid material composed of Cu-MoO3 does show improvement but not as good as Ni-MoO3. A decrease of ~36% is observed in the overpotential for Ni-coated MoO3 compared to pure MoO3 crystals indicating the positive contribution of Ni-coating. The hybrid Ni-MoO3 shows the new route to develop alternate transition metal oxide-based hybrid catalyst towards production of hydrogen fuel.
•Growth of MoO3 single crystal microflakes with layered structure provides catalytically active surface sites for HER.•Development of Cu and Ni-coated MoO3 hybrid material ensues a constructive synergism to lower the overpotential for HER.•Hydrogen spillover effect and electronically coupled Ni-MoO3 interface fosters the hydrogen evolution activity. |
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| AbstractList | Role of hybrid material with metal-oxide interface has been explored by coating 2 nm nickel on α-MoO3 single crystals for hydrogen evolution reaction (HER). The investigated aspects reveal that α-MoO3/Ni hybrid exhibits a remarkable performance in HER showing +6 mV onset potential and 37 mV overpotential at 10 mA/cm2 current density along with Tafel slope of 47 mV/dec. The single crystalline-stepped CVD-grown MoO3 microflakes having the advantage of higher hydrogen binding energy of Ni exhibits the enhanced catalytic performance due to strong electronic coupling at the metal-oxide interface and hydrogen spill over effect. Similar hybrid material composed of Cu-MoO3 does show improvement but not as good as Ni-MoO3. A decrease of ~36% is observed in the overpotential for Ni-coated MoO3 compared to pure MoO3 crystals indicating the positive contribution of Ni-coating. The hybrid Ni-MoO3 shows the new route to develop alternate transition metal oxide-based hybrid catalyst towards production of hydrogen fuel.
•Growth of MoO3 single crystal microflakes with layered structure provides catalytically active surface sites for HER.•Development of Cu and Ni-coated MoO3 hybrid material ensues a constructive synergism to lower the overpotential for HER.•Hydrogen spillover effect and electronically coupled Ni-MoO3 interface fosters the hydrogen evolution activity. |
| Author | Arya, Nitika Halder, Aditi Balakrishnan, Viswanath Avasthi, Piyush |
| Author_xml | – sequence: 1 givenname: Nitika surname: Arya fullname: Arya, Nitika organization: School of Engineering, Indian Institute of Technology, Mandi, Himachal Pradesh, 175005, India – sequence: 2 givenname: Piyush surname: Avasthi fullname: Avasthi, Piyush organization: School of Engineering, Indian Institute of Technology, Mandi, Himachal Pradesh, 175005, India – sequence: 3 givenname: Aditi orcidid: 0000-0003-0399-9705 surname: Halder fullname: Halder, Aditi organization: School of Basic Sciences, Indian Institute of Technology, Mandi, Himachal Pradesh, 175005, India – sequence: 4 givenname: Viswanath orcidid: 0000-0002-6015-770X surname: Balakrishnan fullname: Balakrishnan, Viswanath email: viswa@iitmandi.ac.in organization: School of Engineering, Indian Institute of Technology, Mandi, Himachal Pradesh, 175005, India |
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| Keywords | Single crystals Metal-oxide interface Hydrogen evolution reaction CVD growth Hydrogen spillover |
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| Snippet | Role of hybrid material with metal-oxide interface has been explored by coating 2 nm nickel on α-MoO3 single crystals for hydrogen evolution reaction (HER).... |
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| SubjectTerms | CVD growth Hydrogen evolution reaction Hydrogen spillover Metal-oxide interface Single crystals |
| Title | Nickel decorated MoO3 single crystal microflakes with multi-site functionality for enhanced hydrogen evolution reaction |
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