Nanosheets-nanorods transformation during the non-isothermal decomposition of gadolinium acetate

Gadolinium oxy-carbonate and oxide nanostructures have been successfully obtained via simple non-isothermal heat treatment of gadolinium acetate precursor. Nanosheets of (GdO)2CO3 were developed as a consequence of heating the acetate precursor over the 400–500 °C range and these were stripped into...

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Published inCeramics international Vol. 46; no. 16; pp. 25467 - 25477
Main Authors Abu-Zied, Bahaa M., Obalová, Lucie, Pacultová, Kateřina, Karásková, Kateřina, Al-Fakeh, Maged S., Asiri, Abdullah M., Alminderej, Fahad M.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.11.2020
Subjects
CO2 hydrogenation
Gadolinium acetate
Nanocrystalline Gd2O3
Nanosheets
Non-isothermal decomposition
Rare earth oxides
Nanosheets
Gadolinium acetate
Non-isothermal decomposition
CO2 hydrogenation
Rare earth oxides
Nanocrystalline Gd2O3
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Abstract Gadolinium oxy-carbonate and oxide nanostructures have been successfully obtained via simple non-isothermal heat treatment of gadolinium acetate precursor. Nanosheets of (GdO)2CO3 were developed as a consequence of heating the acetate precursor over the 400–500 °C range and these were stripped into thin lamellar nanorods of cubic Gd2O3 when the heat treatment was applied at the 600–800 °C range. The analysis of N2 adsorption isotherms revealed the microporosity of both phases and the BET calculated surface areas showed a gradual decrease with the pretreatment temperature of Gd2O3. Surface inspection using XPS indicated the presence of Gd in 3+ valence states at the surfaces of (GdO)2CO3 and Gd2O3. H2-TPR results revealed the refractory nature of Gd2O3 nanoparticles against reduction. Moreover, a possible reaction of H2 and CO2 was suggested. The electrical conductivity has been measured during the decomposition of the gadolinium precursor and for the 500–800 °C pre-treated samples.
AbstractList Gadolinium oxy-carbonate and oxide nanostructures have been successfully obtained via simple non-isothermal heat treatment of gadolinium acetate precursor. Nanosheets of (GdO)2CO3 were developed as a consequence of heating the acetate precursor over the 400–500 °C range and these were stripped into thin lamellar nanorods of cubic Gd2O3 when the heat treatment was applied at the 600–800 °C range. The analysis of N2 adsorption isotherms revealed the microporosity of both phases and the BET calculated surface areas showed a gradual decrease with the pretreatment temperature of Gd2O3. Surface inspection using XPS indicated the presence of Gd in 3+ valence states at the surfaces of (GdO)2CO3 and Gd2O3. H2-TPR results revealed the refractory nature of Gd2O3 nanoparticles against reduction. Moreover, a possible reaction of H2 and CO2 was suggested. The electrical conductivity has been measured during the decomposition of the gadolinium precursor and for the 500–800 °C pre-treated samples.
Author Abu-Zied, Bahaa M.
Obalová, Lucie
Pacultová, Kateřina
Karásková, Kateřina
Al-Fakeh, Maged S.
Alminderej, Fahad M.
Asiri, Abdullah M.
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Keywords Nanosheets
Gadolinium acetate
Non-isothermal decomposition
CO2 hydrogenation
Rare earth oxides
Nanocrystalline Gd2O3
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Snippet Gadolinium oxy-carbonate and oxide nanostructures have been successfully obtained via simple non-isothermal heat treatment of gadolinium acetate precursor....
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SubjectTerms CO2 hydrogenation
Gadolinium acetate
Nanocrystalline Gd2O3
Nanosheets
Non-isothermal decomposition
Rare earth oxides
Title Nanosheets-nanorods transformation during the non-isothermal decomposition of gadolinium acetate
URI https://dx.doi.org/10.1016/j.ceramint.2020.07.017
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