One-step environmentally friendly exfoliation and functionalization of hexagonal boron nitride by β-cyclodextrin-assisted ball milling
Hexagonal boron nitride nanosheets (BNNs) are gaining much attention owing to their extraordinary performance; however, difficulties remain in achieving their large-scale preparation and dispersion at high concentration in solvents. A facile yet efficient β-cyclodextrin-assisted mechanochemical exfo...
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| Published in | Ceramics international Vol. 46; no. 13; pp. 21084 - 21089 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.09.2020
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| Abstract | Hexagonal boron nitride nanosheets (BNNs) are gaining much attention owing to their extraordinary performance; however, difficulties remain in achieving their large-scale preparation and dispersion at high concentration in solvents. A facile yet efficient β-cyclodextrin-assisted mechanochemical exfoliation method is proposed to exfoliate and functionalize hexagonal boron nitride (h-BN). The β-cyclodextrin-assisted ball milling process gave a high yield of 60%, with the resultant BNNs being covalently grafted with hydroxyl, and well dispersed in water and other solvents. The concentration of the hydroxyl-functionalized boron nitride nanosheets (OH-BNNs) reached 3 mg/mL, and was stable for several weeks. Next, we fabricated a membrane based on the resulting OH-BNNs to effectively capture Congo red dye. This work not only offers an environmentally friendly, efficient, solvent-less and extremely cost-effective scalable production method, but also assists in our understanding of the mechanism of exfoliation and functionalization in other layered materials. |
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| AbstractList | Hexagonal boron nitride nanosheets (BNNs) are gaining much attention owing to their extraordinary performance; however, difficulties remain in achieving their large-scale preparation and dispersion at high concentration in solvents. A facile yet efficient β-cyclodextrin-assisted mechanochemical exfoliation method is proposed to exfoliate and functionalize hexagonal boron nitride (h-BN). The β-cyclodextrin-assisted ball milling process gave a high yield of 60%, with the resultant BNNs being covalently grafted with hydroxyl, and well dispersed in water and other solvents. The concentration of the hydroxyl-functionalized boron nitride nanosheets (OH-BNNs) reached 3 mg/mL, and was stable for several weeks. Next, we fabricated a membrane based on the resulting OH-BNNs to effectively capture Congo red dye. This work not only offers an environmentally friendly, efficient, solvent-less and extremely cost-effective scalable production method, but also assists in our understanding of the mechanism of exfoliation and functionalization in other layered materials. |
| Author | Yu, Haibin Ji, Dong Zhu, Yanjiao Wang, Zhen |
| Author_xml | – sequence: 1 givenname: Dong surname: Ji fullname: Ji, Dong organization: College of Chemistry and Molecular Science, Wuhan University, Wuhan, 430072, China – sequence: 2 givenname: Zhen surname: Wang fullname: Wang, Zhen organization: Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo, 315201, China – sequence: 3 givenname: Yanjiao surname: Zhu fullname: Zhu, Yanjiao organization: Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo, 315201, China – sequence: 4 givenname: Haibin surname: Yu fullname: Yu, Haibin email: haibinyu@nimte.ac.cn organization: Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo, 315201, China |
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