New sulfonated poly (ether ether ketone) composite membrane with the spherical bell-typed superabsorbent microspheres: Excellent proton conductivity and water retention properties at low humidity
Good proton conductivity and water retention are essential for proton exchange membranes (PEMs). However, proton conductivity of existing PEMs decreases sharply at low humidity, which seriously restricts the efficient and stable operation of fuel cell system. In this study, we design a spherical bel...
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Published in | Journal of power sources Vol. 452; p. 227823 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
Published |
Elsevier B.V
15.03.2020
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Abstract | Good proton conductivity and water retention are essential for proton exchange membranes (PEMs). However, proton conductivity of existing PEMs decreases sharply at low humidity, which seriously restricts the efficient and stable operation of fuel cell system. In this study, we design a spherical bell-typed superabsorbent microsphere with imidazole groups (SBSM) using the distillation-precipitation polymerization method, and incorporate it into sulfonated poly ether ether ketone (SPEEK) matrix to enhance proton conductivity. Benefited from the hygroscopic 3D framework of the superabsorbent core and the special hollow structure of SBSM, the composite membrane remarkably raises the water retention and proton conductivity. Meanwhile, the carboxylic acid, sulfonic acid and Lewis basic imidazole generate two types of “acid-base pairs”, which serves as proton acceptors and donors to accelerate the formation of low energy paths at the membrane interfaces. The composite membrane with 15 wt% fillers exhibits the highest water retention of 15.72% and the highest proton conductivity of 0.0284 S cm−1 at room temperature and 20% relative humidity (RH). These improvements are attributed to the unique structure of the SBSMs that provides a stable aqueous environment and additional proton conduction pathways in the membrane.
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•Novel spherical bell-typed superabsorbent microsphere with imidazole was prepared.•The SBSM exhibited a unique structure for excellent water-retaining properties.•An integrated SPEEK/SBSM composite membrane was successfully prepared.•The existence of “acid-base pairs” accelerated proton transfer inside the membrane.•Composite membrane enhanced low-humidity water retention and proton conductivity. |
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AbstractList | Good proton conductivity and water retention are essential for proton exchange membranes (PEMs). However, proton conductivity of existing PEMs decreases sharply at low humidity, which seriously restricts the efficient and stable operation of fuel cell system. In this study, we design a spherical bell-typed superabsorbent microsphere with imidazole groups (SBSM) using the distillation-precipitation polymerization method, and incorporate it into sulfonated poly ether ether ketone (SPEEK) matrix to enhance proton conductivity. Benefited from the hygroscopic 3D framework of the superabsorbent core and the special hollow structure of SBSM, the composite membrane remarkably raises the water retention and proton conductivity. Meanwhile, the carboxylic acid, sulfonic acid and Lewis basic imidazole generate two types of “acid-base pairs”, which serves as proton acceptors and donors to accelerate the formation of low energy paths at the membrane interfaces. The composite membrane with 15 wt% fillers exhibits the highest water retention of 15.72% and the highest proton conductivity of 0.0284 S cm−1 at room temperature and 20% relative humidity (RH). These improvements are attributed to the unique structure of the SBSMs that provides a stable aqueous environment and additional proton conduction pathways in the membrane.
[Display omitted]
•Novel spherical bell-typed superabsorbent microsphere with imidazole was prepared.•The SBSM exhibited a unique structure for excellent water-retaining properties.•An integrated SPEEK/SBSM composite membrane was successfully prepared.•The existence of “acid-base pairs” accelerated proton transfer inside the membrane.•Composite membrane enhanced low-humidity water retention and proton conductivity. |
ArticleNumber | 227823 |
Author | Song, Shidong Zhang, Huan Wei, Junfu Liu, Wei Luo, Ning Li, Peisen Yang, Xinlin Dai, Zhao |
Author_xml | – sequence: 1 givenname: Wei surname: Liu fullname: Liu, Wei email: liuhuiwen217@yahoo.com organization: State Key Laboratory of Separation Membranes and Membrane Processes, Tiangong University, Tianjin, 300387, PR China – sequence: 2 givenname: Ning surname: Luo fullname: Luo, Ning organization: State Key Laboratory of Separation Membranes and Membrane Processes, Tiangong University, Tianjin, 300387, PR China – sequence: 3 givenname: Peisen surname: Li fullname: Li, Peisen email: Lipeisen227@tju.edu.cn organization: Institute of Surface-Earth System Science, Tianjin University, Tianjin, 300072, PR China – sequence: 4 givenname: Xinlin surname: Yang fullname: Yang, Xinlin email: xlyang88@nankai.edu.cn organization: Key Laboratory of Functional Polymer Materials, Ministry of Education, Institute of Polymer Chemistry, College of Chemistry, Nankai University, Tianjin, 300071, PR China – sequence: 5 givenname: Zhao surname: Dai fullname: Dai, Zhao email: daizhao@gmail.com organization: School of Chemistry and Chemical Engineering, Tiangong University, Tianjin, 300387, PR China – sequence: 6 givenname: Shidong surname: Song fullname: Song, Shidong organization: School of Chemistry and Chemical Engineering, Tiangong University, Tianjin, 300387, PR China – sequence: 7 givenname: Junfu surname: Wei fullname: Wei, Junfu organization: State Key Laboratory of Separation Membranes and Membrane Processes, Tiangong University, Tianjin, 300387, PR China – sequence: 8 givenname: Huan surname: Zhang fullname: Zhang, Huan organization: State Key Laboratory of Separation Membranes and Membrane Processes, Tiangong University, Tianjin, 300387, PR China |
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Keywords | Proton conductivity Water retention Sulfonated poly (ether ether ketone) Composite membrane |
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Snippet | Good proton conductivity and water retention are essential for proton exchange membranes (PEMs). However, proton conductivity of existing PEMs decreases... |
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SubjectTerms | Composite membrane Proton conductivity Sulfonated poly (ether ether ketone) Water retention |
Title | New sulfonated poly (ether ether ketone) composite membrane with the spherical bell-typed superabsorbent microspheres: Excellent proton conductivity and water retention properties at low humidity |
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