Core-shell Ag-Pd nanoparticles catalysts for efficient NO reduction by formic acid
The impact of nitrogen oxide on human beings has reached a point that can’t be ignored. Complex absorption is supposed to be a simple and efficient method to reduce nitrogen oxide emission. However, it is still a challenge to improve the regeneration rate of complex solution by changing the structur...
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Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 626; p. 127115 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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05.10.2021
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Abstract | The impact of nitrogen oxide on human beings has reached a point that can’t be ignored. Complex absorption is supposed to be a simple and efficient method to reduce nitrogen oxide emission. However, it is still a challenge to improve the regeneration rate of complex solution by changing the structure of catalyst. Herein, Ag-Pd nanoparticles (NPs) with core-shell structure were loaded on N-doped porous carbons (NPCs), and it was used as catalyst for Fe(Ⅱ)EDTA-NO reduction by formic acid. The results of X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), temperature programmed desorption (TPD) and transmission electron microscopy (TEM) confirmed that N atoms can improve the dispersion of NPs, and core-shell structure of Ag-Pd has been successfully prepared. Due to the good core-shell structure with fine electron exchange ability and suitable particle size of Ag-Pd NPs, the prepared catalyst has superior catalytic performances, and its TOF can reach 1995 h−1. Under mild conditions, denitrification rate could reach 91.04% with 98.51% N2 selectivity for only 5 min
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•Ag-Pd/NPCs with core-shell structure was synthesized by substitution method.•Ag-Pd/NPCs have significant catalytic activity on Fe(Ⅱ)EDTA-NO reduction by formic acid.•The surface N-doped and porous structure can improve the dispersion of nanoparticles (2 nm).•Ag as the core can greatly promote the catalytic activity of Pd as shell. |
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AbstractList | The impact of nitrogen oxide on human beings has reached a point that can’t be ignored. Complex absorption is supposed to be a simple and efficient method to reduce nitrogen oxide emission. However, it is still a challenge to improve the regeneration rate of complex solution by changing the structure of catalyst. Herein, Ag-Pd nanoparticles (NPs) with core-shell structure were loaded on N-doped porous carbons (NPCs), and it was used as catalyst for Fe(Ⅱ)EDTA-NO reduction by formic acid. The results of X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), temperature programmed desorption (TPD) and transmission electron microscopy (TEM) confirmed that N atoms can improve the dispersion of NPs, and core-shell structure of Ag-Pd has been successfully prepared. Due to the good core-shell structure with fine electron exchange ability and suitable particle size of Ag-Pd NPs, the prepared catalyst has superior catalytic performances, and its TOF can reach 1995 h−1. Under mild conditions, denitrification rate could reach 91.04% with 98.51% N2 selectivity for only 5 min
[Display omitted]
•Ag-Pd/NPCs with core-shell structure was synthesized by substitution method.•Ag-Pd/NPCs have significant catalytic activity on Fe(Ⅱ)EDTA-NO reduction by formic acid.•The surface N-doped and porous structure can improve the dispersion of nanoparticles (2 nm).•Ag as the core can greatly promote the catalytic activity of Pd as shell. |
ArticleNumber | 127115 |
Author | Zhang, Guangxu Wang, Zhanke Guo, Xuehua Wang, Haoqiang Liu, Shihao Hu, Zirui |
Author_xml | – sequence: 1 givenname: Shihao surname: Liu fullname: Liu, Shihao – sequence: 2 givenname: Xuehua surname: Guo fullname: Guo, Xuehua – sequence: 3 givenname: Zhanke orcidid: 0000-0002-7817-2617 surname: Wang fullname: Wang, Zhanke – sequence: 4 givenname: Zirui surname: Hu fullname: Hu, Zirui – sequence: 5 givenname: Haoqiang surname: Wang fullname: Wang, Haoqiang – sequence: 6 givenname: Guangxu surname: Zhang fullname: Zhang, Guangxu email: zhanggx2002@whut.edu.cn |
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