Morphology-controlled synthesis of ZnSnO3 hollow spheres and their n-butanol gas-sensing performance

ZnSnO3 hollow spheres were successfully synthesized via a mild hydrothermal strategy followed by an annealing process. Their microstructures, morphologies and chemical compositions were characterized by a variety of techniques, including X-ray diffraction, transmission electron microscopy and N2 ads...

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Published inCeramics international Vol. 47; no. 2; pp. 2471 - 2482
Main Authors Feng, Guoqing, Che, Yanhan, Song, Chengwen, Xiao, Jingkun, Fan, Xinfei, Sun, Shuang, Huang, Guohui, Ma, Yanchao
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 15.01.2021
Subjects
Gas-sensing
Hollow sphere
N-butanol
ZnSnO3
Hollow sphere
Gas-sensing
ZnSnO3
N-butanol
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Abstract ZnSnO3 hollow spheres were successfully synthesized via a mild hydrothermal strategy followed by an annealing process. Their microstructures, morphologies and chemical compositions were characterized by a variety of techniques, including X-ray diffraction, transmission electron microscopy and N2 adsorption-desorption. Due to rapid co-precipitation and self-assembly, a resultant hollowing process was achieved, and ZnSnO3 particles were reorganized into hollow structures. Furthermore, the possible formation mechanism was interpreted by means of several experiments under different reaction conditions. The as-fabricated ZnSnO3 sensors with hollow interiors and permeable surfaces were investigated with six volatile gases, which exhibited fast response and high selectivity to n-butanol at the much-lowered optimal temperature of 200 °C. In particular, the response time of the sensors based on ZnSnO3 hollow spheres was 3 s, implying that they are a potential candidate for n-butanol gas detection. In addition, the gas-sensing mechanism of the ZnSnO3 sensor was also investigated.
AbstractList ZnSnO3 hollow spheres were successfully synthesized via a mild hydrothermal strategy followed by an annealing process. Their microstructures, morphologies and chemical compositions were characterized by a variety of techniques, including X-ray diffraction, transmission electron microscopy and N2 adsorption-desorption. Due to rapid co-precipitation and self-assembly, a resultant hollowing process was achieved, and ZnSnO3 particles were reorganized into hollow structures. Furthermore, the possible formation mechanism was interpreted by means of several experiments under different reaction conditions. The as-fabricated ZnSnO3 sensors with hollow interiors and permeable surfaces were investigated with six volatile gases, which exhibited fast response and high selectivity to n-butanol at the much-lowered optimal temperature of 200 °C. In particular, the response time of the sensors based on ZnSnO3 hollow spheres was 3 s, implying that they are a potential candidate for n-butanol gas detection. In addition, the gas-sensing mechanism of the ZnSnO3 sensor was also investigated.
Author Feng, Guoqing
Xiao, Jingkun
Fan, Xinfei
Sun, Shuang
Ma, Yanchao
Che, Yanhan
Song, Chengwen
Huang, Guohui
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Snippet ZnSnO3 hollow spheres were successfully synthesized via a mild hydrothermal strategy followed by an annealing process. Their microstructures, morphologies and...
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StartPage 2471
SubjectTerms Gas-sensing
Hollow sphere
N-butanol
ZnSnO3
Title Morphology-controlled synthesis of ZnSnO3 hollow spheres and their n-butanol gas-sensing performance
URI https://dx.doi.org/10.1016/j.ceramint.2020.09.090
Volume 47
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