Enhancing the electrocatalytic activity via hybridization of Cu(I/II) oxides with Co3O4 towards oxygen electrode reactions
Transition metal oxide based electrocatalysts (ECs) with mixed valence state have gained considerable attention in recent times. Herein, Co3O4–CuO/Cu2O/C nanostructure with mixed valence oxides is reported as an efficient bi-functional EC towards oxygen electrode reactions in alkaline medium. The EC...
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Published in | Journal of power sources Vol. 490; p. 229511 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.04.2021
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Abstract | Transition metal oxide based electrocatalysts (ECs) with mixed valence state have gained considerable attention in recent times. Herein, Co3O4–CuO/Cu2O/C nanostructure with mixed valence oxides is reported as an efficient bi-functional EC towards oxygen electrode reactions in alkaline medium. The EC displays higher current density of 6.2 mA cm−2 and mass activity of 12.9 mA mg−1 compared to that of commercially available Pt/C in 0.1 M KOH solution for oxygen reduction reaction (ORR). Rotating disk electrode measurements are used to understand the kinetics of the reaction and the EC is durable up to 1000 redox cycles. The material is highly stable up to 7000 s by retaining 99% of its initial current. The fast electron transfer is established by the smaller Tafel slope value of 83.6 mV dec−1. In addition, the prepared material is also active for oxygen evolution reaction (OER) in 0.1 M KOH solution. Thus, the nanostructure with different bimetallic active sites is found to be a potential material for oxygen electrocatalysis.
•A Co3O4–CuO/Cu2O material is employed as electrocatalyst for ORR/OER in alkaline medium.•The ORR follows a direct four electron pathway.•Performance of the material is much higher than the Pt/C under similar conditions.•The material is also active for OER.•The material is highly durable and stable. |
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AbstractList | Transition metal oxide based electrocatalysts (ECs) with mixed valence state have gained considerable attention in recent times. Herein, Co3O4–CuO/Cu2O/C nanostructure with mixed valence oxides is reported as an efficient bi-functional EC towards oxygen electrode reactions in alkaline medium. The EC displays higher current density of 6.2 mA cm−2 and mass activity of 12.9 mA mg−1 compared to that of commercially available Pt/C in 0.1 M KOH solution for oxygen reduction reaction (ORR). Rotating disk electrode measurements are used to understand the kinetics of the reaction and the EC is durable up to 1000 redox cycles. The material is highly stable up to 7000 s by retaining 99% of its initial current. The fast electron transfer is established by the smaller Tafel slope value of 83.6 mV dec−1. In addition, the prepared material is also active for oxygen evolution reaction (OER) in 0.1 M KOH solution. Thus, the nanostructure with different bimetallic active sites is found to be a potential material for oxygen electrocatalysis.
•A Co3O4–CuO/Cu2O material is employed as electrocatalyst for ORR/OER in alkaline medium.•The ORR follows a direct four electron pathway.•Performance of the material is much higher than the Pt/C under similar conditions.•The material is also active for OER.•The material is highly durable and stable. |
ArticleNumber | 229511 |
Author | Matus, Ekaterina V. Bharali, Pankaj Hazarika, Kumar Kashyap Yamada, Yusuke Kerzhentsev, Mikhail |
Author_xml | – sequence: 1 givenname: Kumar Kashyap surname: Hazarika fullname: Hazarika, Kumar Kashyap organization: Department of Chemical Sciences, Tezpur University, Napaam 784028, Assam, India – sequence: 2 givenname: Yusuke surname: Yamada fullname: Yamada, Yusuke organization: Department of Applied Chemistry & Bioengineering, Graduate School of Engineering, Osaka City University, Sumiyoshi-ku, Osaka 558-8585, Japan – sequence: 3 givenname: Ekaterina V. orcidid: 0000-0002-3470-9507 surname: Matus fullname: Matus, Ekaterina V. organization: Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, 630090, Novosibirsk, Russia – sequence: 4 givenname: Mikhail orcidid: 0000-0001-5988-9818 surname: Kerzhentsev fullname: Kerzhentsev, Mikhail organization: Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, 630090, Novosibirsk, Russia – sequence: 5 givenname: Pankaj orcidid: 0000-0003-3471-0468 surname: Bharali fullname: Bharali, Pankaj email: pankajb@tezu.ernet.in organization: Department of Chemical Sciences, Tezpur University, Napaam 784028, Assam, India |
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CitedBy_id | crossref_primary_10_1016_j_mtener_2021_100911 crossref_primary_10_1016_j_mcat_2021_112086 crossref_primary_10_1021_acsami_1c11730 crossref_primary_10_1039_D1NJ02061G crossref_primary_10_1149_1945_7111_ac4b25 crossref_primary_10_1016_j_mcat_2022_112569 crossref_primary_10_1021_acs_energyfuels_1c01388 crossref_primary_10_1039_D1RA06936E crossref_primary_10_1002_smll_202304863 crossref_primary_10_1021_acsaem_1c03748 crossref_primary_10_1002_cctc_202101472 crossref_primary_10_1016_j_cej_2024_150718 |
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Keywords | Electrocatalysis Oxygen evolution reaction Oxygen reduction reaction Mixed valence oxides |
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Snippet | Transition metal oxide based electrocatalysts (ECs) with mixed valence state have gained considerable attention in recent times. Herein, Co3O4–CuO/Cu2O/C... |
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SubjectTerms | Electrocatalysis Mixed valence oxides Oxygen evolution reaction Oxygen reduction reaction |
Title | Enhancing the electrocatalytic activity via hybridization of Cu(I/II) oxides with Co3O4 towards oxygen electrode reactions |
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