Molecular weight controlled sulfonated Poly(Arylene Ether)s and sulfonated Poly(Ether Ether ketone) polymer blends for fuel cell applications

We synthesized molecular weight-controlled and fluorine-containing PAEs (MWCPAEs) using decafluorobiphenyl (DFBP), 2-bis (4-hydroxyphenyl) propane (Bis A), and 2,2-Bis (4-hydroxyphenyl) hexafluoropropane (Bis AF). Later, commercially available PEEK and the MWCPAEs were sulfonated (SPEEK and SMWCPAE)...

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Published inInternational journal of hydrogen energy Vol. 48; no. 85; pp. 33297 - 33314
Main Authors Seden, Merve G., Baştürk, Emre, İnan, Tülay Y., Apohan, Nilhan K., Güngör, Atilla
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.10.2023
Subjects
Blend membrane
Controlled-molecular weight
DMFC
PEMFC
poly(arylene ether)
PEMFC
Controlled-molecular weight
poly(arylene ether)
DMFC
Blend membrane
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Abstract We synthesized molecular weight-controlled and fluorine-containing PAEs (MWCPAEs) using decafluorobiphenyl (DFBP), 2-bis (4-hydroxyphenyl) propane (Bis A), and 2,2-Bis (4-hydroxyphenyl) hexafluoropropane (Bis AF). Later, commercially available PEEK and the MWCPAEs were sulfonated (SPEEK and SMWCPAE) and blended to fabricate blend membranes (BMs). All BMs have been prepared by solution casting method in 5 wt%-20 wt% concentrations using N,N-dimethylacetamide. The effects of chemical structures, sulfonation levels, MW and compositions on the membrane properties are discussed. We obtained miscible and mechanically compatible BMs. The highest proton conductivity (238.9 mS/cm) was determined for SPEEK70/S-DFBP-Bis-A based blend membrane (Mw: 48.355, 5wt. %). All chemical, mechanical, thermal, and hydrolytic properties of the BMs are comparable with, or better than, that of Nafion. We suggest that designing polymeric structures with desired MWs and sulfonation levels may enable enhanced properties and can help to design materials with on demand properties. [Display omitted] •Molecular weights controlled Poly (arylene ether)s has been synthesized and sulfonated.•The blend membranes we prepared are miscible and mechanically compatible.•The proton conductivity value up to 238.9 mS/cm has been obtained.•BMs properties are comparable with, or better than, that of Nafion.•The membranes are suitable for PEMFC and DMFC applications.
AbstractList We synthesized molecular weight-controlled and fluorine-containing PAEs (MWCPAEs) using decafluorobiphenyl (DFBP), 2-bis (4-hydroxyphenyl) propane (Bis A), and 2,2-Bis (4-hydroxyphenyl) hexafluoropropane (Bis AF). Later, commercially available PEEK and the MWCPAEs were sulfonated (SPEEK and SMWCPAE) and blended to fabricate blend membranes (BMs). All BMs have been prepared by solution casting method in 5 wt%-20 wt% concentrations using N,N-dimethylacetamide. The effects of chemical structures, sulfonation levels, MW and compositions on the membrane properties are discussed. We obtained miscible and mechanically compatible BMs. The highest proton conductivity (238.9 mS/cm) was determined for SPEEK70/S-DFBP-Bis-A based blend membrane (Mw: 48.355, 5wt. %). All chemical, mechanical, thermal, and hydrolytic properties of the BMs are comparable with, or better than, that of Nafion. We suggest that designing polymeric structures with desired MWs and sulfonation levels may enable enhanced properties and can help to design materials with on demand properties. [Display omitted] •Molecular weights controlled Poly (arylene ether)s has been synthesized and sulfonated.•The blend membranes we prepared are miscible and mechanically compatible.•The proton conductivity value up to 238.9 mS/cm has been obtained.•BMs properties are comparable with, or better than, that of Nafion.•The membranes are suitable for PEMFC and DMFC applications.
Author Apohan, Nilhan K.
İnan, Tülay Y.
Güngör, Atilla
Seden, Merve G.
Baştürk, Emre
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Keywords PEMFC
Controlled-molecular weight
poly(arylene ether)
DMFC
Blend membrane
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Snippet We synthesized molecular weight-controlled and fluorine-containing PAEs (MWCPAEs) using decafluorobiphenyl (DFBP), 2-bis (4-hydroxyphenyl) propane (Bis A), and...
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SubjectTerms Blend membrane
Controlled-molecular weight
DMFC
PEMFC
poly(arylene ether)
Title Molecular weight controlled sulfonated Poly(Arylene Ether)s and sulfonated Poly(Ether Ether ketone) polymer blends for fuel cell applications
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