Impact of Ce2O3 on microstructure and properties of matrix-body for PDC drill bits synthesized via pressureless melt infiltration

The materials of matrix-body polycrystalline diamond composite (PDC) bits were fabricated through pressureless melt infiltration method at 1200 °C for 1 h within vacuum furnace using molten CuNi metallic binder, Ni and WC powders (including cast WC, spherical WC, and fine WC). Various weight ratios...

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Published inCeramics international Vol. 48; no. 18; pp. 26945 - 26953
Main Authors Zhou, Xinjun, Zhang, Zhengfu, Li, Xiulan, Zhang, Xudong, Li, Yuxi, Chen, Manjiao
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 15.09.2022
Subjects
Ce2O3
Mechanical properties
Microstructure
Pressureless melt infiltration
Mechanical properties
Ce2O3
WC
Microstructure
Pressureless melt infiltration
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Abstract The materials of matrix-body polycrystalline diamond composite (PDC) bits were fabricated through pressureless melt infiltration method at 1200 °C for 1 h within vacuum furnace using molten CuNi metallic binder, Ni and WC powders (including cast WC, spherical WC, and fine WC). Various weight ratios of Ce2O3/(WC + Ni + CuNi) ranging from 0 to 0.01 were added to matrix-body materials. The influence of Ce2O3 on the microstructure, phase formation, phase transformations, and related mechanical properties of matrix-body materials was thoroughly investigated. The results show that experimental temperature led to the decomposition of WC and partial dissolution of W and C in CuNi binder alloys. In matrix-body materials with no Ce2O3 addition, only new W2C phase was formed. With further increase in Ce2O3/(WC + Ni + CuNi) ratios, spherical WC was dispersed into smaller WC particles. Meanwhile, new phases (namely Ni2W4C, C, and W2C) were found. The material exhibited an optimal hardness (HRA = 93.7) and transverse rupture strength (1846.8 MPa) when Ce2O3/(WC + Ni + CuNi) ratio was 0.006. However, impact toughness was slightly decreased, while the highest value of 6.45 J cm−2 was measured for the sample with Ce2O3/(WC + Ni + CuNi) ratio of 0.01.
AbstractList The materials of matrix-body polycrystalline diamond composite (PDC) bits were fabricated through pressureless melt infiltration method at 1200 °C for 1 h within vacuum furnace using molten CuNi metallic binder, Ni and WC powders (including cast WC, spherical WC, and fine WC). Various weight ratios of Ce2O3/(WC + Ni + CuNi) ranging from 0 to 0.01 were added to matrix-body materials. The influence of Ce2O3 on the microstructure, phase formation, phase transformations, and related mechanical properties of matrix-body materials was thoroughly investigated. The results show that experimental temperature led to the decomposition of WC and partial dissolution of W and C in CuNi binder alloys. In matrix-body materials with no Ce2O3 addition, only new W2C phase was formed. With further increase in Ce2O3/(WC + Ni + CuNi) ratios, spherical WC was dispersed into smaller WC particles. Meanwhile, new phases (namely Ni2W4C, C, and W2C) were found. The material exhibited an optimal hardness (HRA = 93.7) and transverse rupture strength (1846.8 MPa) when Ce2O3/(WC + Ni + CuNi) ratio was 0.006. However, impact toughness was slightly decreased, while the highest value of 6.45 J cm−2 was measured for the sample with Ce2O3/(WC + Ni + CuNi) ratio of 0.01.
Author Chen, Manjiao
Zhou, Xinjun
Li, Yuxi
Li, Xiulan
Zhang, Xudong
Zhang, Zhengfu
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Ce2O3
WC
Microstructure
Pressureless melt infiltration
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Snippet The materials of matrix-body polycrystalline diamond composite (PDC) bits were fabricated through pressureless melt infiltration method at 1200 °C for 1 h...
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SubjectTerms Ce2O3
Mechanical properties
Microstructure
Pressureless melt infiltration
Title Impact of Ce2O3 on microstructure and properties of matrix-body for PDC drill bits synthesized via pressureless melt infiltration
URI https://dx.doi.org/10.1016/j.ceramint.2022.06.006
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