Synthesis and properties of waterborne few-layer graphene oxide/poly(MMA-co-BuA) nanocomposites by in situ emulsion polymerization
[Display omitted] •Waterborne colloidal few-layer graphene oxide (FLGO) reinforced poly(MMA-co-BuA) nanocomposites were synthesized.•FLGO content significantly affected the colloidal and film properties of the nanocomposites.•Chemical interactions between FLGO and polymer occurred above 1wt% of FLGO...
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Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 531; pp. 56 - 66 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
20.10.2017
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Abstract | [Display omitted]
•Waterborne colloidal few-layer graphene oxide (FLGO) reinforced poly(MMA-co-BuA) nanocomposites were synthesized.•FLGO content significantly affected the colloidal and film properties of the nanocomposites.•Chemical interactions between FLGO and polymer occurred above 1wt% of FLGO content.•The incorporation of FLGO enhanced the colloidal and thermal stability, Tg and Young’s modulus of the nanocomposites.
Waterborne few-layer graphene oxide/poly(methyl methacrylate-co-butyl acrylate), FLGO/poly(MMA-co-BuA), nanocomposites were synthesized by in situ emulsion polymerization. The FLGO nanosheets used in this study was prepared by modified Hummers method and followed by an exfoliation process. The obtained FLGO and both latex and film forms of the nanocomposites were characterized in detail. It was found that the interactions between FLGO and copolymer matrix, and therefore the nanocomposite properties including colloidal, morphological, thermal and mechanical were directly dependent on the amount of FLGO in the composite composition. With the addition of 1% FLGO by weight (relative to the monomer), hydrodynamic diameters of the polymer particles in latex increased from 39.7nm to 92.0nm and moreover zeta potential value of this nanocomposite latex reached to −85mV. Also, the nanocomposite film of this nanocomposite showed significant improvements in glass transition temperature (Tg), thermal degradation temperatures and Young’s modulus values, comparing with other nanocomposites. The analysis results confirmed that the FLGO was chemically interacted with the poly(MMA-co-BuA), and also finely dispersed in the matrix. |
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AbstractList | [Display omitted]
•Waterborne colloidal few-layer graphene oxide (FLGO) reinforced poly(MMA-co-BuA) nanocomposites were synthesized.•FLGO content significantly affected the colloidal and film properties of the nanocomposites.•Chemical interactions between FLGO and polymer occurred above 1wt% of FLGO content.•The incorporation of FLGO enhanced the colloidal and thermal stability, Tg and Young’s modulus of the nanocomposites.
Waterborne few-layer graphene oxide/poly(methyl methacrylate-co-butyl acrylate), FLGO/poly(MMA-co-BuA), nanocomposites were synthesized by in situ emulsion polymerization. The FLGO nanosheets used in this study was prepared by modified Hummers method and followed by an exfoliation process. The obtained FLGO and both latex and film forms of the nanocomposites were characterized in detail. It was found that the interactions between FLGO and copolymer matrix, and therefore the nanocomposite properties including colloidal, morphological, thermal and mechanical were directly dependent on the amount of FLGO in the composite composition. With the addition of 1% FLGO by weight (relative to the monomer), hydrodynamic diameters of the polymer particles in latex increased from 39.7nm to 92.0nm and moreover zeta potential value of this nanocomposite latex reached to −85mV. Also, the nanocomposite film of this nanocomposite showed significant improvements in glass transition temperature (Tg), thermal degradation temperatures and Young’s modulus values, comparing with other nanocomposites. The analysis results confirmed that the FLGO was chemically interacted with the poly(MMA-co-BuA), and also finely dispersed in the matrix. |
Author | Ucar, Ezgi Sahinturk, Utkan Berber, Hale |
Author_xml | – sequence: 1 givenname: Hale surname: Berber fullname: Berber, Hale email: hberber@yildiz.edu.tr, haleberber@yahoo.com organization: Yildiz Technical University, Faculty of Chemical and Metallurgical Engineering, Department of Metallurgical and Materials Engineering, 34220 Istanbul, Turkey – sequence: 2 givenname: Ezgi surname: Ucar fullname: Ucar, Ezgi organization: Yildiz Technical University, Faculty of Chemical and Metallurgical Engineering, Department of Chemical Engineering, 34220 Istanbul, Turkey – sequence: 3 givenname: Utkan surname: Sahinturk fullname: Sahinturk, Utkan organization: Istanbul University, Vocational School of Technical Sciences, Department of Mechanical and Metal Technology, 34320 Istanbul, Turkey |
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CitedBy_id | crossref_primary_10_1016_j_mtchem_2023_101397 crossref_primary_10_1016_j_eurpolymj_2019_109249 crossref_primary_10_1016_j_apsusc_2018_06_023 crossref_primary_10_1016_j_progpolymsci_2021_101476 crossref_primary_10_1021_acsami_2c08981 crossref_primary_10_1016_j_reactfunctpolym_2019_104320 crossref_primary_10_1108_PRT_01_2020_0002 crossref_primary_10_1007_s10924_021_02162_x crossref_primary_10_1016_j_porgcoat_2022_106949 crossref_primary_10_1002_pc_25045 crossref_primary_10_1002_macp_202300185 crossref_primary_10_1002_pc_25600 crossref_primary_10_1016_j_molstruc_2018_06_011 |
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Keywords | Few-layer graphene oxide Waterborne polymer nanocomposites in situ emulsion polymerization Colloidal properties Poly(MMA-co-BuA) |
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•Waterborne colloidal few-layer graphene oxide (FLGO) reinforced poly(MMA-co-BuA) nanocomposites were synthesized.•FLGO content significantly... |
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SubjectTerms | Colloidal properties Few-layer graphene oxide in situ emulsion polymerization Poly(MMA-co-BuA) Waterborne polymer nanocomposites |
Title | Synthesis and properties of waterborne few-layer graphene oxide/poly(MMA-co-BuA) nanocomposites by in situ emulsion polymerization |
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