Synthesis and characterization of V(III), Cr(III) and Fe(III) hippurates
Hippurates of V(III), Cr(III) and Fe(III) were isolated as solids with the general formula; [V(hip) 3]·15H 2O, [Cr(hip) 3]·6H 2O and [Fe(hip) 3]·1.5H 2O. The compounds were characterized from elemental analysis, infrared spectra, 1H NMR, electronic spectra and thermogravimetric analysis and proof th...
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Published in | Journal of molecular structure Vol. 737; no. 2; pp. 139 - 145 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Elsevier B.V
04.03.2005
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Abstract | Hippurates of V(III), Cr(III) and Fe(III) were isolated as solids with the general formula; [V(hip)
3]·15H
2O, [Cr(hip)
3]·6H
2O and [Fe(hip)
3]·1.5H
2O. The compounds were characterized from elemental analysis, infrared spectra,
1H NMR, electronic spectra and thermogravimetric analysis and proof that metal–ligand coordination involves only via the carboxylate group. |
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AbstractList | Hippurates of V(III), Cr(III) and Fe(III) were isolated as solids with the general formula; [V(hip)
3]·15H
2O, [Cr(hip)
3]·6H
2O and [Fe(hip)
3]·1.5H
2O. The compounds were characterized from elemental analysis, infrared spectra,
1H NMR, electronic spectra and thermogravimetric analysis and proof that metal–ligand coordination involves only via the carboxylate group. |
Author | Sadeek, S.A. Refat, M.S. Teleb, S.M. El-Megharbel, S.M. |
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Cites_doi | 10.1016/S0277-5387(99)00162-X 10.1021/ja00511a014 10.1021/ja00529a020 10.1021/ic00138a024 10.1039/a709272e 10.1016/S0020-1693(00)81901-5 10.1039/p29740000784 10.1016/S0162-0134(01)00196-9 10.1002/andp.18290931104 10.1007/BF01913369 |
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Snippet | Hippurates of V(III), Cr(III) and Fe(III) were isolated as solids with the general formula; [V(hip)
3]·15H
2O, [Cr(hip)
3]·6H
2O and [Fe(hip)
3]·1.5H
2O. The... |
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SubjectTerms | 1H NMR Electronic spectra Hippuric acid TGA |
Title | Synthesis and characterization of V(III), Cr(III) and Fe(III) hippurates |
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