Polyhedral oligomeric silsesquioxane containing gel polymer electrolyte based on a PMMA matrix
The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; and the organic substituents at the cage corners of POSS are more comp...
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| Published in | RSC advances Vol. 5; no. 57; pp. 4598 - 45918 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.01.2015
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; and the organic substituents at the cage corners of POSS are more compatible with GPEs. Therefore, POSS, as a hybrid modification filler, was added into GPE within a polymethyl methacrylate (PMMA) matrix. The results indicated that the amount of POSS addition was a critical factor for the ionic conductivity of prepared GPEs. When the POSS content was 7.5 wt%, the thermal stability was sufficient at the elevated temperature; the ionic conductivity of GPE reached 2.0 × 10
−3
S cm
−1
; the mechanism of conductivity followed typical Arrhenius behavior; the lithium ion transference number reached up to 0.33; the deposition/dissolution of lithium was highly reversible; the electrochemical stability window was high enough at 5.25 V and the compatibility with lithium electrolyte was satisfactory.
A polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; the organic substituents at the cage corners of POSS are more compatible with GPEs. |
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| AbstractList | The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; and the organic substituents at the cage corners of POSS are more compatible with GPEs. Therefore, POSS, as a hybrid modification filler, was added into GPE within a polymethyl methacrylate (PMMA) matrix. The results indicated that the amount of POSS addition was a critical factor for the ionic conductivity of prepared GPEs. When the POSS content was 7.5 wt%, the thermal stability was sufficient at the elevated temperature; the ionic conductivity of GPE reached 2.0 × 10
−3
S cm
−1
; the mechanism of conductivity followed typical Arrhenius behavior; the lithium ion transference number reached up to 0.33; the deposition/dissolution of lithium was highly reversible; the electrochemical stability window was high enough at 5.25 V and the compatibility with lithium electrolyte was satisfactory.
A polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; the organic substituents at the cage corners of POSS are more compatible with GPEs. The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; and the organic substituents at the cage corners of POSS are more compatible with GPEs. Therefore, POSS, as a hybrid modification filler, was added into GPE within a polymethyl methacrylate (PMMA) matrix. The results indicated that the amount of POSS addition was a critical factor for the ionic conductivity of prepared GPEs. When the POSS content was 7.5 wt%, the thermal stability was sufficient at the elevated temperature; the ionic conductivity of GPE reached 2.0 10 super(-3) S cm super(-1); the mechanism of conductivity followed typical Arrhenius behavior; the lithium ion transference number reached up to 0.33; the deposition/dissolution of lithium was highly reversible; the electrochemical stability window was high enough at 5.25 V and the compatibility with lithium electrolyte was satisfactory. The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar properties as can be accomplished with other inorganic nanoparticles; and the organic substituents at the cage corners of POSS are more compatible with GPEs. Therefore, POSS, as a hybrid modification filler, was added into GPE within a polymethyl methacrylate (PMMA) matrix. The results indicated that the amount of POSS addition was a critical factor for the ionic conductivity of prepared GPEs. When the POSS content was 7.5 wt%, the thermal stability was sufficient at the elevated temperature; the ionic conductivity of GPE reached 2.0 × 10 −3 S cm −1 ; the mechanism of conductivity followed typical Arrhenius behavior; the lithium ion transference number reached up to 0.33; the deposition/dissolution of lithium was highly reversible; the electrochemical stability window was high enough at 5.25 V and the compatibility with lithium electrolyte was satisfactory. |
| Author | Li, Xing Gong, Sheng-Dong Lin, Yuan-Hua Huang, Rui Cao, Hai-Jun Huang, Yun Yang, Man |
| AuthorAffiliation | Southwest Petroleum University Institute of Blood Transfusion School of Materials Science and Engineering Chinese Academy of Medical Sciences |
| AuthorAffiliation_xml | – name: Southwest Petroleum University – name: Institute of Blood Transfusion – name: School of Materials Science and Engineering – name: Chinese Academy of Medical Sciences |
| Author_xml | – sequence: 1 givenname: Yun surname: Huang fullname: Huang, Yun – sequence: 2 givenname: Sheng-Dong surname: Gong fullname: Gong, Sheng-Dong – sequence: 3 givenname: Rui surname: Huang fullname: Huang, Rui – sequence: 4 givenname: Hai-Jun surname: Cao fullname: Cao, Hai-Jun – sequence: 5 givenname: Yuan-Hua surname: Lin fullname: Lin, Yuan-Hua – sequence: 6 givenname: Man surname: Yang fullname: Yang, Man – sequence: 7 givenname: Xing surname: Li fullname: Li, Xing |
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| CitedBy_id | crossref_primary_10_1016_j_electacta_2018_05_012 crossref_primary_10_1016_j_memsci_2017_09_077 crossref_primary_10_1007_s10008_016_3434_x crossref_primary_10_1016_j_electacta_2020_135902 crossref_primary_10_1016_j_electacta_2019_134572 crossref_primary_10_1002_aenm_202101057 crossref_primary_10_1007_s10008_017_3877_8 crossref_primary_10_1007_s10008_017_3568_5 crossref_primary_10_1007_s10008_017_3761_6 crossref_primary_10_1007_s10853_020_05162_9 crossref_primary_10_1155_2019_2730849 crossref_primary_10_1002_mame_202400051 crossref_primary_10_1016_j_electacta_2018_04_040 crossref_primary_10_1002_ange_202210851 crossref_primary_10_1002_adfm_202304748 crossref_primary_10_1002_anie_202210851 crossref_primary_10_1039_C6TA00888G crossref_primary_10_1002_smm2_1121 |
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| Snippet | The present research is based on two expectations: a polyhedral oligomeric silsesquioxane (POSS) nano-cage can endow gel polymer electrolyte (GPE) with similar... |
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| SubjectTerms | Compatibility Deposition Electrolytes Ionic conductivity Lithium Nanoparticles Polyhedral oligomeric silsesquioxane Polymethyl methacrylates |
| Title | Polyhedral oligomeric silsesquioxane containing gel polymer electrolyte based on a PMMA matrix |
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