Synthesis of high-purity zircon, zirconia, and silica nanopowders from local zircon sand
High-purity zircon (ZrSiO4) nanopowder was successfully produced from Indonesian natural zircon sand using a low-cost purification approach via magnetic separation, immersion in HCl, and reaction with NaOH, followed by a top-down nanosizing process using wet ball-milling for 10 h and annealing at 20...
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| Published in | Ceramics international Vol. 45; no. 6; pp. 6639 - 6647 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
15.04.2019
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| Subjects | |
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| Abstract | High-purity zircon (ZrSiO4) nanopowder was successfully produced from Indonesian natural zircon sand using a low-cost purification approach via magnetic separation, immersion in HCl, and reaction with NaOH, followed by a top-down nanosizing process using wet ball-milling for 10 h and annealing at 200 °C for 2 h. Furthermore, polymorph zirconia (ZrO2 – amorphous, tetragonal, and monoclinic) and silica (SiO2 – amorphous and cristobalite) nanopowders were also successfully derived from the purified zircon powder using a bottom-up method via alkali fusion and co-precipitation processes followed by calcination. The crystallite size of the powders was estimated from X-ray diffraction (XRD) data analysis to give 40, 31, 61, and 149 nm, respectively, for the zircon, tetragonal- and monoclinic-zirconia, and cristobalite. Microstructural characteristics of the zircon, silica, and zirconia nanopowders were revealed in transmission electron microscopy (TEM) images which confirmed that the average sizes of the particles were in a good agreement with the XRD estimated values. |
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| AbstractList | High-purity zircon (ZrSiO4) nanopowder was successfully produced from Indonesian natural zircon sand using a low-cost purification approach via magnetic separation, immersion in HCl, and reaction with NaOH, followed by a top-down nanosizing process using wet ball-milling for 10 h and annealing at 200 °C for 2 h. Furthermore, polymorph zirconia (ZrO2 – amorphous, tetragonal, and monoclinic) and silica (SiO2 – amorphous and cristobalite) nanopowders were also successfully derived from the purified zircon powder using a bottom-up method via alkali fusion and co-precipitation processes followed by calcination. The crystallite size of the powders was estimated from X-ray diffraction (XRD) data analysis to give 40, 31, 61, and 149 nm, respectively, for the zircon, tetragonal- and monoclinic-zirconia, and cristobalite. Microstructural characteristics of the zircon, silica, and zirconia nanopowders were revealed in transmission electron microscopy (TEM) images which confirmed that the average sizes of the particles were in a good agreement with the XRD estimated values. |
| Author | Lestari, Novia Dwi Triwikantoro Musyarofah Nurlaila, Rizka Pratapa, Suminar Muwwaqor, Nibras Fuadi |
| Author_xml | – sequence: 1 orcidid: 0000-0002-7342-0685 surname: Musyarofah fullname: Musyarofah – sequence: 2 givenname: Novia Dwi surname: Lestari fullname: Lestari, Novia Dwi – sequence: 3 givenname: Rizka surname: Nurlaila fullname: Nurlaila, Rizka – sequence: 4 givenname: Nibras Fuadi surname: Muwwaqor fullname: Muwwaqor, Nibras Fuadi – sequence: 5 surname: Triwikantoro fullname: Triwikantoro – sequence: 6 givenname: Suminar surname: Pratapa fullname: Pratapa, Suminar email: suminar_pratapa@physics.its.ac.id |
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