Microwave assisted synthesis of polyacrylamide grafted soya peptone and its application as water soluble adhesive
•SOYP-g-PAM was synthesized by ‘Microwave assisted method’.•Application of the synthesized grades as adhesive was studied.•SOYP-g-PAM showed excellent property.•The effect of percentage grafting, AM concentration and CAN concentration on breaking strength of Lap joint experiment was studied. Synthes...
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| Published in | Industrial crops and products Vol. 58; pp. 251 - 258 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.07.2014
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| Subjects | |
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| Abstract | •SOYP-g-PAM was synthesized by ‘Microwave assisted method’.•Application of the synthesized grades as adhesive was studied.•SOYP-g-PAM showed excellent property.•The effect of percentage grafting, AM concentration and CAN concentration on breaking strength of Lap joint experiment was studied.
Synthesis of polyacrylamide (PAM) grafted soya peptone was performed by the microwave assisted method using ceric ammonium nitrate (CAN) as free radical initiator. The synthesis was optimized by varying the acrylamide and CAN concentration. The grafting of the PAM chains on the peptone backbone was confirmed through various physicochemical techniques-intrinsic viscosity study, FTIR spectroscopy, elemental analysis (C, H, N, S and O), SEM and TGA. The applicability of this synthesized graft copolymer as a water soluble adhesive has been studied by fabricating a single lap joint of two wooden blocks using an aqueous paste of the graft copolymer as adhesive. After curing, the breaking point of the joint was determined using an UTM. |
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| AbstractList | •SOYP-g-PAM was synthesized by ‘Microwave assisted method’.•Application of the synthesized grades as adhesive was studied.•SOYP-g-PAM showed excellent property.•The effect of percentage grafting, AM concentration and CAN concentration on breaking strength of Lap joint experiment was studied.
Synthesis of polyacrylamide (PAM) grafted soya peptone was performed by the microwave assisted method using ceric ammonium nitrate (CAN) as free radical initiator. The synthesis was optimized by varying the acrylamide and CAN concentration. The grafting of the PAM chains on the peptone backbone was confirmed through various physicochemical techniques-intrinsic viscosity study, FTIR spectroscopy, elemental analysis (C, H, N, S and O), SEM and TGA. The applicability of this synthesized graft copolymer as a water soluble adhesive has been studied by fabricating a single lap joint of two wooden blocks using an aqueous paste of the graft copolymer as adhesive. After curing, the breaking point of the joint was determined using an UTM. |
| Author | Mishra, Sumit D.Mahto Rani, Priti Sen, Gautam |
| Author_xml | – sequence: 1 surname: D.Mahto fullname: D.Mahto organization: Department of Mechanical Engineering, Birla Institute of Technology, Mesra, Ranchi 835215, Jharkhand, India – sequence: 2 givenname: Priti surname: Rani fullname: Rani, Priti organization: Department of Applied Chemistry, Birla Institute of Technology, Mesra, Ranchi 835215, Jharkhand, India – sequence: 3 givenname: Sumit surname: Mishra fullname: Mishra, Sumit organization: Department of Applied Chemistry, Birla Institute of Technology, Mesra, Ranchi 835215, Jharkhand, India – sequence: 4 givenname: Gautam surname: Sen fullname: Sen, Gautam email: gsen06@gmail.com, gsen9@hotmail.com organization: Department of Applied Chemistry, Birla Institute of Technology, Mesra, Ranchi 835215, Jharkhand, India |
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| CitedBy_id | crossref_primary_10_1016_j_jes_2019_01_019 crossref_primary_10_1016_j_ijbiomac_2018_07_199 crossref_primary_10_1016_j_est_2020_101297 crossref_primary_10_1007_s10924_018_1213_8 crossref_primary_10_1021_acssuschemeng_5b01327 crossref_primary_10_1089_adt_2024_013 crossref_primary_10_1016_j_ijadhadh_2023_103601 crossref_primary_10_1002_pen_24499 crossref_primary_10_1002_maco_202414346 |
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| Keywords | Soya peptone Graft co polymer Microwave assisted synthesis Adhesive |
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| SubjectTerms | Adhesive Graft co polymer Microwave assisted synthesis Soya peptone |
| Title | Microwave assisted synthesis of polyacrylamide grafted soya peptone and its application as water soluble adhesive |
| URI | https://dx.doi.org/10.1016/j.indcrop.2014.04.013 |
| Volume | 58 |
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