Hydrophobic electrospun membrane of peppermint oil loaded zein with coating of methyltriethoxysilane for active packaging

Zein electrospun nanofibers are widely used as the vehicles to load bioactive entities for release control; however, the water absorption of zein always restricts their applications in food preservation. In this work, an active hydrophobic membrane of peppermint oil (PO) loaded zein (ZN) with coatin...

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Published inFood hydrocolloids Vol. 144; p. 109031
Main Authors Xia, Li, Li, Linlin, Xiao, Yewen, Xiao, Feng, Ji, Wei, Pang, Min, Wang, Hualin
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.11.2023
Subjects
Active packaging
Electrospinning
Hydrophobic membrane
Release kinetics
Zein
Electrospinning
Zein
Release kinetics
Active packaging
Hydrophobic membrane
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Abstract Zein electrospun nanofibers are widely used as the vehicles to load bioactive entities for release control; however, the water absorption of zein always restricts their applications in food preservation. In this work, an active hydrophobic membrane of peppermint oil (PO) loaded zein (ZN) with coating of methyltriethoxysilane (MTES) was developed for pork preservation. The fiber matrix of ZN was use for PO incorporation. The secondary structure of ZN and the feature of the relevant fibers are dependent on solvents of acetic acid and ethyl alcohol. In the composite structure, PO is hydrogen-bonded with ZN matrix; while the coating of MTES is bonded with fiber matrix by Si–O–C. The well-controlled release of PO predominantly follows the law of Fickian diffusion, endowing the membrane good antibacterial activity and antioxidant activity. The coating of MTES has no obvious influence on the bioactivities but provides the membrane outstanding hydrophobicity with water contact angle of 138 ± 5°. ZN-PO30-MTES can extend shelf life of pork by 100% (i.e., 24 h) at 25 °C, demonstrating its potential in food active packaging. [Display omitted] •An active hydrophobic electrospun membrane was developed for pork preservation.•Secondary structure of ZN and feature of fibers are dependent on solvents.•Release of peppermint oil from matrix is well controlled.•Coating of MTES endows membrane with water contact angle of 138 ± 5°.•Target membrane can effectively the extend shelf life of pork by 100% at 25 °C.
AbstractList Zein electrospun nanofibers are widely used as the vehicles to load bioactive entities for release control; however, the water absorption of zein always restricts their applications in food preservation. In this work, an active hydrophobic membrane of peppermint oil (PO) loaded zein (ZN) with coating of methyltriethoxysilane (MTES) was developed for pork preservation. The fiber matrix of ZN was use for PO incorporation. The secondary structure of ZN and the feature of the relevant fibers are dependent on solvents of acetic acid and ethyl alcohol. In the composite structure, PO is hydrogen-bonded with ZN matrix; while the coating of MTES is bonded with fiber matrix by Si–O–C. The well-controlled release of PO predominantly follows the law of Fickian diffusion, endowing the membrane good antibacterial activity and antioxidant activity. The coating of MTES has no obvious influence on the bioactivities but provides the membrane outstanding hydrophobicity with water contact angle of 138 ± 5°. ZN-PO30-MTES can extend shelf life of pork by 100% (i.e., 24 h) at 25 °C, demonstrating its potential in food active packaging. [Display omitted] •An active hydrophobic electrospun membrane was developed for pork preservation.•Secondary structure of ZN and feature of fibers are dependent on solvents.•Release of peppermint oil from matrix is well controlled.•Coating of MTES endows membrane with water contact angle of 138 ± 5°.•Target membrane can effectively the extend shelf life of pork by 100% at 25 °C.
ArticleNumber 109031
Author Wang, Hualin
Xiao, Yewen
Li, Linlin
Xiao, Feng
Pang, Min
Xia, Li
Ji, Wei
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Keywords Electrospinning
Zein
Release kinetics
Active packaging
Hydrophobic membrane
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Snippet Zein electrospun nanofibers are widely used as the vehicles to load bioactive entities for release control; however, the water absorption of zein always...
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SubjectTerms Active packaging
Electrospinning
Hydrophobic membrane
Release kinetics
Zein
Title Hydrophobic electrospun membrane of peppermint oil loaded zein with coating of methyltriethoxysilane for active packaging
URI https://dx.doi.org/10.1016/j.foodhyd.2023.109031
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