A new strategy for the fabrication of covalent organic framework-metal-organic framework hybrids via in-situ functionalization of ligands for improved hydrogen evolution reaction activity

The development of novel porous materials have attracted significant attention owing to its possible application in several fields. In this study, we designed a novel covalent organic framework-metal-organic framework (COF-MOF) material through an in-situ ligand self-assembly method. The in-situ mod...

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Published inChinese journal of catalysis Vol. 43; no. 3; pp. 811 - 819
Main Authors Zheng, Ling-Ling, Zhang, Long-Shuai, Chen, Ying, Tian, Lei, Jiang, Xun-Heng, Chen, Li-Sha, Xing, Qiu-Ju, Liu, Xiao-Zhen, Wu, Dai-She, Zou, Jian-Ping
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.03.2022
Subjects
COF/MOF hybrid
Covalent organic frameworks
Hydrogen evolution
In-situ
Metal-organic frameworks
Covalent organic frameworks
COF/MOF hybrid
In-situ
Metal-organic frameworks
Hydrogen evolution
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Abstract The development of novel porous materials have attracted significant attention owing to its possible application in several fields. In this study, we designed a novel covalent organic framework-metal-organic framework (COF-MOF) material through an in-situ ligand self-assembly method. The in-situ modified ligands not only act as nucleation sites to form Ti-MOF, but also as a channel to rapidly transfer photogenerated electrons without introducing additional chemical bonds. The photocatalytic hydrogen production rate achieved over B-CTF-Ti-MOF(1:1) was 1975 µmol·g−1·h−1 with an apparent quantum efficiency of 4.76%, which is 11.8 times higher than that of the pure CTF-1. In addition, compared with the sample prepared by separating the ligands (CTF-1/Ti-MOF), B-CTF-Ti-MOF shows excellent activity and stability. Finally, a reasonable photocatalytic mechanism was proposed using the results of electrochemical tests and spectral analyses. This study provides a universal method for the construction of highly efficient and stable COF/MOF materials with excellent properties. Well-designed unique covalent organic framework-metal-organic framework hybrids (B-CTF-Ti-MOF) were constructed by using in-situ functionalized ligands as nucleation sites and electronic transmission channels to boost the photocatalytic performance of the material.
AbstractList The development of novel porous materials have attracted significant attention owing to its possible application in several fields. In this study, we designed a novel covalent organic framework-metal-organic framework (COF-MOF) material through an in-situ ligand self-assembly method. The in-situ modified ligands not only act as nucleation sites to form Ti-MOF, but also as a channel to rapidly transfer photogenerated electrons without introducing additional chemical bonds. The photocatalytic hydrogen production rate achieved over B-CTF-Ti-MOF(1:1) was 1975 µmol·g−1·h−1 with an apparent quantum efficiency of 4.76%, which is 11.8 times higher than that of the pure CTF-1. In addition, compared with the sample prepared by separating the ligands (CTF-1/Ti-MOF), B-CTF-Ti-MOF shows excellent activity and stability. Finally, a reasonable photocatalytic mechanism was proposed using the results of electrochemical tests and spectral analyses. This study provides a universal method for the construction of highly efficient and stable COF/MOF materials with excellent properties. Well-designed unique covalent organic framework-metal-organic framework hybrids (B-CTF-Ti-MOF) were constructed by using in-situ functionalized ligands as nucleation sites and electronic transmission channels to boost the photocatalytic performance of the material.
Author Wu, Dai-She
Zheng, Ling-Ling
Jiang, Xun-Heng
Zou, Jian-Ping
Liu, Xiao-Zhen
Chen, Ying
Tian, Lei
Zhang, Long-Shuai
Chen, Li-Sha
Xing, Qiu-Ju
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– sequence: 8
  givenname: Xiao-Zhen
  surname: Liu
  fullname: Liu, Xiao-Zhen
  organization: Key Laboratory of Poyang Lake Environment and Resource Utilization of Ministry of Education, School of Resources Environmental and Chemical Engineering, Nanchang University, Nanchang 330031, Jiangxi, China
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  givenname: Dai-She
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– sequence: 10
  givenname: Jian-Ping
  surname: Zou
  fullname: Zou, Jian-Ping
  email: zjp_112@126.com
  organization: Key Laboratory of Jiangxi Province for Persistent Pollutants Control and Resources Recycle, Nanchang Hangkong University, Nanchang 330063, Jiangxi, China
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Keywords Covalent organic frameworks
COF/MOF hybrid
In-situ
Metal-organic frameworks
Hydrogen evolution
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Snippet The development of novel porous materials have attracted significant attention owing to its possible application in several fields. In this study, we designed...
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SubjectTerms COF/MOF hybrid
Covalent organic frameworks
Hydrogen evolution
In-situ
Metal-organic frameworks
Title A new strategy for the fabrication of covalent organic framework-metal-organic framework hybrids via in-situ functionalization of ligands for improved hydrogen evolution reaction activity
URI https://dx.doi.org/10.1016/S1872-2067(21)63892-5
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