Phase transformations in an Aurivillius layer structured ferroelectric designed using the high entropy concept
A single phase four-layer Aurivillius structured ferroelectric ceramic, (Ca0.2Sr0.2Ba0.2Pb0.2Nd0.1Na0.1)Bi4Ti4O15 (6ABTO) was obtained using a high entropy design concept. The material, which has orthorhombic symmetry in space group A21am at room temperature, has Ca2+, Sr2+, Ba2+, Pb2+, Nd3+ and Na+...
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| Published in | Acta materialia Vol. 229; p. 117815 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.05.2022
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| Abstract | A single phase four-layer Aurivillius structured ferroelectric ceramic, (Ca0.2Sr0.2Ba0.2Pb0.2Nd0.1Na0.1)Bi4Ti4O15 (6ABTO) was obtained using a high entropy design concept. The material, which has orthorhombic symmetry in space group A21am at room temperature, has Ca2+, Sr2+, Ba2+, Pb2+, Nd3+ and Na+ distributed not only on the A sites of the perovskite layer but also in the bismuthate layer. 6ABTO shows complex ferroelectric behavior, with a Curie point of 557 °C. Four current peaks are observed in the current - electric field curve. These peaks are attributed to a combination of a field induced phase transition and domain wall switching, which is the first reported occurrence of such current - electric field behavior for an Aurivillius structured ferroelectric material. Despite the level of disorder between the A site cations in the perovskite layer and the Bi positions in the bismuthate layer, 6ABTO does not show the relaxor ferroelectric behavior, that is commonly observed in cases of such disorder. This suggests that relaxor behavior in ferroelectrics, may be more associated with the thermal stability of dipoles, rather than the presence of polar nano-regions formed as a result of chemical disorder. The nature of the high entropy effect in 6ABTO is discussed through comparison of results from isostructural compositions containing 5, 4 and 3 of the component cations
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| AbstractList | A single phase four-layer Aurivillius structured ferroelectric ceramic, (Ca0.2Sr0.2Ba0.2Pb0.2Nd0.1Na0.1)Bi4Ti4O15 (6ABTO) was obtained using a high entropy design concept. The material, which has orthorhombic symmetry in space group A21am at room temperature, has Ca2+, Sr2+, Ba2+, Pb2+, Nd3+ and Na+ distributed not only on the A sites of the perovskite layer but also in the bismuthate layer. 6ABTO shows complex ferroelectric behavior, with a Curie point of 557 °C. Four current peaks are observed in the current - electric field curve. These peaks are attributed to a combination of a field induced phase transition and domain wall switching, which is the first reported occurrence of such current - electric field behavior for an Aurivillius structured ferroelectric material. Despite the level of disorder between the A site cations in the perovskite layer and the Bi positions in the bismuthate layer, 6ABTO does not show the relaxor ferroelectric behavior, that is commonly observed in cases of such disorder. This suggests that relaxor behavior in ferroelectrics, may be more associated with the thermal stability of dipoles, rather than the presence of polar nano-regions formed as a result of chemical disorder. The nature of the high entropy effect in 6ABTO is discussed through comparison of results from isostructural compositions containing 5, 4 and 3 of the component cations
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| ArticleNumber | 117815 |
| Author | Abrahams, Isaac Reece, Michael J. Zhang, Man Xu, Xinzhao Yue, Yajun Ahmed, Shafique Gao, Feng Palma, Matteo Yan, Haixue Svec, Peter |
| Author_xml | – sequence: 1 givenname: Man orcidid: 0000-0002-1094-7279 surname: Zhang fullname: Zhang, Man organization: School of Engineering and Materials Science, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 2 givenname: Xinzhao surname: Xu fullname: Xu, Xinzhao organization: Department of Chemistry, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 3 givenname: Shafique surname: Ahmed fullname: Ahmed, Shafique organization: School of Engineering and Materials Science, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 4 givenname: Yajun surname: Yue fullname: Yue, Yajun organization: Department of Chemistry, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 5 givenname: Matteo orcidid: 0000-0001-8715-4034 surname: Palma fullname: Palma, Matteo organization: Department of Chemistry, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 6 givenname: Peter orcidid: 0000-0002-2257-3710 surname: Svec fullname: Svec, Peter organization: Institute of Physics, Slovak Academy of Sciences, Dúbravská Cesta 9, 845 11 Bratislava, Slovak Republic – sequence: 7 givenname: Feng orcidid: 0000-0002-5075-4076 surname: Gao fullname: Gao, Feng organization: NPU-QMUL Joint Research Institute of Advanced Materials and Structure, School of Materials Science and Engineering, Northwestern Polytechnical University, Xi'an, 710072, China – sequence: 8 givenname: Isaac orcidid: 0000-0002-8606-6056 surname: Abrahams fullname: Abrahams, Isaac email: i.abrahams@qmul.ac.uk organization: Department of Chemistry, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 9 givenname: Michael J. surname: Reece fullname: Reece, Michael J. organization: School of Engineering and Materials Science, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom – sequence: 10 givenname: Haixue orcidid: 0000-0002-4563-1100 surname: Yan fullname: Yan, Haixue email: h.x.yan@qmul.ac.uk organization: School of Engineering and Materials Science, Queen Mary University of London, Mile End Road, London, E1 4NS, United Kingdom |
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| Title | Phase transformations in an Aurivillius layer structured ferroelectric designed using the high entropy concept |
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