Water-soluble, mesoporous Fe3O4: Synthesis, characterization, and properties

Water-soluble, mesoporous Fe3O4 nanopowder is successfully prepared by one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in triethylene glycol (TEG). The formation of Fe3O4 is confirmed from X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and selected ar...

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Published inCeramics international Vol. 38; no. 8; pp. 6579 - 6584
Main Authors Asuha, S., Wan, H.L., Zhao, S., Deligeer, W., Wu, H.Y., Song, L., Tegus, O.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.12.2012
Subjects
Coercive force
Ethanol
Ethyl alcohol
Magnetite
Mesoporous
Nanocomposites
Nanomaterials
Nanostructure
Thermal decomposition
Transmission electron microscopy
Water-soluble
X-ray photoelectron spectroscopy
Magnetite
Mesoporous
Thermal decomposition
Water-soluble
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Abstract Water-soluble, mesoporous Fe3O4 nanopowder is successfully prepared by one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in triethylene glycol (TEG). The formation of Fe3O4 is confirmed from X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and selected area electron diffraction (SAED) measurements. The morphological and structural properties of the Fe3O4 nanopowder are characterized by transmission electron microscopy (TEM), nitrogen adsorption–desorption, and thermogravimetric analysis (TGA). Monodisperse, nearly spherical and highly crystalline Fe3O4 nanoparticles are obtained by this method. The Fe3O4 nanopowder is well dispersed in water and ethanol with a mesoporous structure, average pore size of 3.6nm, and Brunauner–Emmett–Teller (BET) surface area of 122m2/g. The room temperature magnetization hysteresis curve exhibits barely measurable values for coercivity and remanence, suggesting that the Fe3O4 nanopowder possesses superparamagnetic characteristics.
AbstractList Water-soluble, mesoporous Fe3O4 nanopowder was prepared by the one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in triethylene glycol. The formation of Fe3O4 was confirmed by XRD, XPS, and SAED measurements. The morphological and structural properties of the Fe3O4 nanopowder were characterised by TEM, nitrogen adsorption-desorption, and TGA. Monodisperse, nearly spherical and highly crystalline Fe3O4 nanoparticles were obtained by this method. The Fe3O4 nanopowder was well dispersed in water and ethanol with a mesoporous structure, average pore size of 3.6 nm, and BET surface area of 122 m2/g. The room temperature magnetisation hysteresis curve showed barely measurable values for coercivity and remanence, suggesting that the Fe3O4 nanopowder possesses superparamagnetic characteristics.
Water-soluble, mesoporous Fe3O4 nanopowder is successfully prepared by one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in triethylene glycol (TEG). The formation of Fe3O4 is confirmed from X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and selected area electron diffraction (SAED) measurements. The morphological and structural properties of the Fe3O4 nanopowder are characterized by transmission electron microscopy (TEM), nitrogen adsorption–desorption, and thermogravimetric analysis (TGA). Monodisperse, nearly spherical and highly crystalline Fe3O4 nanoparticles are obtained by this method. The Fe3O4 nanopowder is well dispersed in water and ethanol with a mesoporous structure, average pore size of 3.6nm, and Brunauner–Emmett–Teller (BET) surface area of 122m2/g. The room temperature magnetization hysteresis curve exhibits barely measurable values for coercivity and remanence, suggesting that the Fe3O4 nanopowder possesses superparamagnetic characteristics.
Author Song, L.
Zhao, S.
Wu, H.Y.
Asuha, S.
Wan, H.L.
Tegus, O.
Deligeer, W.
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Snippet Water-soluble, mesoporous Fe3O4 nanopowder is successfully prepared by one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in...
Water-soluble, mesoporous Fe3O4 nanopowder was prepared by the one-step thermal decomposition of an iron-urea complex ([Fe(NH2CONH2)6](NO3)3) in triethylene...
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SubjectTerms Coercive force
Ethanol
Ethyl alcohol
Magnetite
Mesoporous
Nanocomposites
Nanomaterials
Nanostructure
Thermal decomposition
Transmission electron microscopy
Water-soluble
X-ray photoelectron spectroscopy
Title Water-soluble, mesoporous Fe3O4: Synthesis, characterization, and properties
URI https://dx.doi.org/10.1016/j.ceramint.2012.05.042
https://search.proquest.com/docview/1221875695
https://search.proquest.com/docview/1692394556
Volume 38
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