Separation system synthesis of fractional crystallization processes with heat integration
A methodology is presented for the synthesis of fractional crystallization processes with heat integration. The methodology is based on the construction of three networks. The first network is based on the identification of feasible thermodynamic states. Using equilibrium data for a candidate set of...
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Published in | Computers & chemical engineering Vol. 25; no. 4; pp. 595 - 602 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.05.2001
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Abstract | A methodology is presented for the synthesis of fractional crystallization processes with heat integration. The methodology is based on the construction of three networks. The first network is based on the identification of feasible thermodynamic states. Using equilibrium data for a candidate set of potential operation point temperatures, a network flow model is constructed to represent the set of potential separation flowsheet structures that can result. In this network the nodes correspond to multiple saturation points, solute intermediate, process feeds and end products. The second network is used to represent the variety of tasks that can be performed at each multiple saturation point. Multiple saturation nodes can be used for different tasks depending on the characteristic of the input and output streams. These tasks include cooling crystallization, evaporative crystallization, reactive crystallization, dissolution, and leaching, This multiple task condition for each equilibrium state is modelled using disjunctive programming and then converted into a mixed integer program. Heat integration is included using a heat exchanger network which can be regarded as a transhipment problem. The method is illustrated through the design of two salt separation examples. |
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AbstractList | A methodology is presented for the synthesis of fractional crystallization processes with heat integration. The methodology is based on the construction of three networks. The first network is based on the identification of feasible thermodynamic states. Using equilibrium data for a candidate set of potential operation point temperatures, a network flow model is constructed to represent the set of potential separation flowsheet structures that can result. In this network the nodes correspond to multiple saturation points, solute intermediate, process feeds and end products. The second network is used to represent the variety of tasks that can be performed at each multiple saturation point. Multiple saturation nodes can be used for different tasks depending on the characteristic of the input and output streams. These tasks include cooling crystallization, evaporative crystallization, reactive crystallization, dissolution, and leaching, This multiple task condition for each equilibrium state is modelled using disjunctive programming and then converted into a mixed integer program. Heat integration is included using a heat exchanger network which can be regarded as a transhipment problem. The method is illustrated through the design of two salt separation examples. |
Author | Cisternas, Luis A. Guerrero, Carmen P. Swaney, Ross E. |
Author_xml | – sequence: 1 givenname: Luis A. surname: Cisternas fullname: Cisternas, Luis A. email: lcisternas@uantof.cl organization: Department of Chemical Engineering, Universidad de Antofagasta, Casilla 170, Antofagasta, Chile – sequence: 2 givenname: Carmen P. surname: Guerrero fullname: Guerrero, Carmen P. organization: Department of Chemical Engineering, Universidad de Antofagasta, Casilla 170, Antofagasta, Chile – sequence: 3 givenname: Ross E. surname: Swaney fullname: Swaney, Ross E. organization: Department of Chemical Engineering, University of Wisconsin-Madison, 1415 Engineering Drive, Madison, WI 53706, USA |
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CitedBy_id | crossref_primary_10_1205_cherd07052 crossref_primary_10_1016_j_compchemeng_2004_02_006 crossref_primary_10_1016_S1093_0191_02_00128_4 crossref_primary_10_1146_annurev_chembioeng_061010_114129 crossref_primary_10_1002_aic_10768 crossref_primary_10_1002_aic_690490712 crossref_primary_10_1016_j_cep_2005_07_003 crossref_primary_10_3923_jas_2010_2989_2997 |
Cites_doi | 10.1002/aic.690420808 10.1002/aic.690450711 10.1002/aic.690430112 10.1021/ie00083a019 10.1016/0098-1354(83)85023-6 10.1021/ie00021a022 10.1021/ie9600856 10.1021/ie970335y 10.1016/0098-1354(91)87007-V |
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References | Cisternas, Swaney (BIB5) 1998; 37 Turkay, Grossmann (BIB12) 1996; 35 Cisternas (BIB6) 1999; 45 Prabhudesai R. K. (1988). Leaching in Schweitzer P.A., Handbook of Separation Techniques for Chemical Engineers, second edition, McGraw-Hill, New York Berry, Ng (BIB2) 1996; 42 Papoulias, Grossmann (BIB8) 1983; 7 Berry, Dye, Ng (BIB3) 1997; 43 Raman, Grossmann (BIB11) 1991; 15 Rajagopal, Ng, Douglas (BIB10) 1988; 27 Bennett R. C. (1993). Crystallizer selection and design, in: Myerson A. (Ed.), Handbook of Industrial Crystallization, Butterworth-Heinemann Cisternas, Rudd (BIB4) 1993; 32 Linke, W. F., & Seidell, A. (1965). Solubilities of Inorganic and Metal Organic Compounds, American Chemical Society, Washington DC 10.1016/S0098-1354(01)00639-1_BIB9 Turkay (10.1016/S0098-1354(01)00639-1_BIB12) 1996; 35 Berry (10.1016/S0098-1354(01)00639-1_BIB2) 1996; 42 Cisternas (10.1016/S0098-1354(01)00639-1_BIB4) 1993; 32 10.1016/S0098-1354(01)00639-1_BIB7 Raman (10.1016/S0098-1354(01)00639-1_BIB11) 1991; 15 Rajagopal (10.1016/S0098-1354(01)00639-1_BIB10) 1988; 27 Cisternas (10.1016/S0098-1354(01)00639-1_BIB6) 1999; 45 10.1016/S0098-1354(01)00639-1_BIB1 Berry (10.1016/S0098-1354(01)00639-1_BIB3) 1997; 43 Papoulias (10.1016/S0098-1354(01)00639-1_BIB8) 1983; 7 Cisternas (10.1016/S0098-1354(01)00639-1_BIB5) 1998; 37 |
References_xml | – volume: 42 start-page: 2162 year: 1996 end-page: 2174 ident: BIB2 article-title: Separation of quaternary conjugate salt systems by fractional crystallization publication-title: American Institute of Chemical Engineering Journal contributor: fullname: Ng – volume: 45 start-page: 1477 year: 1999 end-page: 1487 ident: BIB6 article-title: Optimal design of crystallization-based separation schemes publication-title: American Institute of Chemical Engineering Journal contributor: fullname: Cisternas – volume: 35 start-page: 2611 year: 1996 end-page: 2623 ident: BIB12 article-title: Disjunctive programming techniques for the optimization of process systems with discontinuous investment costs-multiple size regions publication-title: Industrial Engineering and Chemical Research contributor: fullname: Grossmann – volume: 43 start-page: 91 year: 1997 end-page: 103 ident: BIB3 article-title: Synthesis of drowning-out crystallization-based separations publication-title: American Institute of Chemical Engineering Journal contributor: fullname: Ng – volume: 15 start-page: 73 year: 1991 end-page: 84 ident: BIB11 article-title: Relation between MILP modelling and logical inference for chemical process synthesis publication-title: Computers and Chemical Engineering contributor: fullname: Grossmann – volume: 37 start-page: 2761 year: 1998 end-page: 2769 ident: BIB5 article-title: Separation system synthesis for fractional crystallization from solution using a network flow model publication-title: Industrial Engineering and Chemistry contributor: fullname: Swaney – volume: 27 start-page: 2071 year: 1988 end-page: 2078 ident: BIB10 article-title: Design of solids processes: production of potash publication-title: Industrial Engineering and Chemical Research contributor: fullname: Douglas – volume: 7 start-page: 707 year: 1983 ident: BIB8 article-title: A structural optimization approach to process synthesis-II Heat recovery network publication-title: Computers and Chemical Engineering contributor: fullname: Grossmann – volume: 32 start-page: 1993 year: 1993 end-page: 2005 ident: BIB4 article-title: Process design for fractional crystallization from solution publication-title: Industrial Engineering and Chemistry Research contributor: fullname: Rudd – volume: 42 start-page: 2162 issue: 8 year: 1996 ident: 10.1016/S0098-1354(01)00639-1_BIB2 article-title: Separation of quaternary conjugate salt systems by fractional crystallization publication-title: American Institute of Chemical Engineering Journal doi: 10.1002/aic.690420808 contributor: fullname: Berry – volume: 45 start-page: 1477 issue: 7 year: 1999 ident: 10.1016/S0098-1354(01)00639-1_BIB6 article-title: Optimal design of crystallization-based separation schemes publication-title: American Institute of Chemical Engineering Journal doi: 10.1002/aic.690450711 contributor: fullname: Cisternas – volume: 43 start-page: 91 issue: 1 year: 1997 ident: 10.1016/S0098-1354(01)00639-1_BIB3 article-title: Synthesis of drowning-out crystallization-based separations publication-title: American Institute of Chemical Engineering Journal doi: 10.1002/aic.690430112 contributor: fullname: Berry – volume: 27 start-page: 2071 issue: 11 year: 1988 ident: 10.1016/S0098-1354(01)00639-1_BIB10 article-title: Design of solids processes: production of potash publication-title: Industrial Engineering and Chemical Research doi: 10.1021/ie00083a019 contributor: fullname: Rajagopal – ident: 10.1016/S0098-1354(01)00639-1_BIB7 – volume: 7 start-page: 707 issue: 6 year: 1983 ident: 10.1016/S0098-1354(01)00639-1_BIB8 article-title: A structural optimization approach to process synthesis-II Heat recovery network publication-title: Computers and Chemical Engineering doi: 10.1016/0098-1354(83)85023-6 contributor: fullname: Papoulias – volume: 32 start-page: 1993 year: 1993 ident: 10.1016/S0098-1354(01)00639-1_BIB4 article-title: Process design for fractional crystallization from solution 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SubjectTerms | Fractional crystallization Heat integration Process design Salt separation |
Title | Separation system synthesis of fractional crystallization processes with heat integration |
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