Specimen Size Effect of Interface Strength Distribution Induced by Grain Structure of Cu Line

A new technique for the evaluation of local interface adhesion energy was applied to the interface between Cu and cap layer in a Cu damascene interconnect structure, which consists of both the interfacial fracture test and the finite-element simulation. After specimens in-plane dimensions of 1×1 μm,...

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Published inTRANSACTIONS OF THE JAPAN SOCIETY OF MECHANICAL ENGINEERS Series A Vol. 79; no. 799; pp. 354 - 358
Main Authors SUZUKI, Toshiaki, OMIYA, Masaki, NAKAMURA, Tomoji, CHEN, Chuantong, SHISHIDO, Nobuyuki, SUZUKI, Takashi, KOIWA, Kozo, KAMIYA, Shoji, SATO, Hisashi, NOKUO, Takeshi, NISHIDA, Masahiro
Format Journal Article
LanguageJapanese
Published The Japan Society of Mechanical Engineers 2013
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ISSN0387-5008
1884-8338
DOI10.1299/kikaia.79.354

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Abstract A new technique for the evaluation of local interface adhesion energy was applied to the interface between Cu and cap layer in a Cu damascene interconnect structure, which consists of both the interfacial fracture test and the finite-element simulation. After specimens in-plane dimensions of 1×1 μm, 5×5 μm and 10×10 μm fractured by focused ion beam (FIB), the interfacial fracture test was implemented by a novel system with nano-indenter in FIB-SEM dual-beam microscope. With the maximum load measured during the fracture test employed in an elastic-plastic simulation, interface adhesion energy was evaluated and almost equal among all types of specimens. On the other hand, the variation of the evaluated interface adhesion energy tends to be larger with the decreasing specimen size. With the result of electron backscattering diffraction analysis for Cu lines whose average grain size were 400nm diameter, it is suggested that local interface strength significantly varies depending on local grain distribution in a Cu interconnect structure.
AbstractList A new technique for the evaluation of local interface adhesion energy was applied to the interface between Cu and cap layer in a Cu damascene interconnect structure, which consists of both the interfacial fracture test and the finite-element simulation. After specimens in-plane dimensions of 1×1 μm, 5×5 μm and 10×10 μm fractured by focused ion beam (FIB), the interfacial fracture test was implemented by a novel system with nano-indenter in FIB-SEM dual-beam microscope. With the maximum load measured during the fracture test employed in an elastic-plastic simulation, interface adhesion energy was evaluated and almost equal among all types of specimens. On the other hand, the variation of the evaluated interface adhesion energy tends to be larger with the decreasing specimen size. With the result of electron backscattering diffraction analysis for Cu lines whose average grain size were 400nm diameter, it is suggested that local interface strength significantly varies depending on local grain distribution in a Cu interconnect structure.
Author NOKUO, Takeshi
SUZUKI, Takashi
KAMIYA, Shoji
SUZUKI, Toshiaki
KOIWA, Kozo
SATO, Hisashi
NAKAMURA, Tomoji
CHEN, Chuantong
SHISHIDO, Nobuyuki
OMIYA, Masaki
NISHIDA, Masahiro
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Cites_doi 10.1016/j.engfracmech.2008.06.011
10.1002/nme.1620090114
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References (4) Hellen, T. K. “On the Method of Virtual Crack Extensions”, International Journal for Numerical Methods in Engineering, Vol. 9, No.1 (1975), pp.187-207.
(2) Dauskardt, R. H., Lane, M., Ma, Q., Krishna, N. “Adhesion and debonding of multi-layer thin film structures”, Engineering Fracture Mechanics, Vol. 61, (1998), pp.141-162.
(3) Kamiya, S., Furuta, H., Omiya, M., Shimomura, H. “A novel evaluation method for interfacial adhesion strength in ductile dissimilar materials”, Engineering Fracture Mechanics, Vol. 75, (2008), pp.5007-5017.
(1) Kamiya, S., Sato, H., Nishida, M., Chen, C., Shishido, N., Omiya, M., Suzuki, T., Nakamura, T., Nokuo, T., Nagasawa, T. “Micro-Scale Evaluation of Interface Strength on the Patterned Structures in LSI Interconnects”, AIP Conference Proceedings, Vol. 1300, (2010), pp.33-38.
(5) 住田純也,大宮正毅,小岩康三,陳傳彤,宍戸信之,神谷庄司,佐藤尚,西田政弘,野久尾毅,長澤忠広,鈴木貴志,中村友二,“LSI配線界面局所強度評価のための弾塑性き裂進展シミュレーションの開発”, 日本機械学会東海支部第61期総会講演論文集, No. 123-1, (2012), 528.
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References_xml – reference: (3) Kamiya, S., Furuta, H., Omiya, M., Shimomura, H. “A novel evaluation method for interfacial adhesion strength in ductile dissimilar materials”, Engineering Fracture Mechanics, Vol. 75, (2008), pp.5007-5017.
– reference: (1) Kamiya, S., Sato, H., Nishida, M., Chen, C., Shishido, N., Omiya, M., Suzuki, T., Nakamura, T., Nokuo, T., Nagasawa, T. “Micro-Scale Evaluation of Interface Strength on the Patterned Structures in LSI Interconnects”, AIP Conference Proceedings, Vol. 1300, (2010), pp.33-38.
– reference: (2) Dauskardt, R. H., Lane, M., Ma, Q., Krishna, N. “Adhesion and debonding of multi-layer thin film structures”, Engineering Fracture Mechanics, Vol. 61, (1998), pp.141-162.
– reference: (5) 住田純也,大宮正毅,小岩康三,陳傳彤,宍戸信之,神谷庄司,佐藤尚,西田政弘,野久尾毅,長澤忠広,鈴木貴志,中村友二,“LSI配線界面局所強度評価のための弾塑性き裂進展シミュレーションの開発”, 日本機械学会東海支部第61期総会講演論文集, No. 123-1, (2012), 528.
– reference: (4) Hellen, T. K. “On the Method of Virtual Crack Extensions”, International Journal for Numerical Methods in Engineering, Vol. 9, No.1 (1975), pp.187-207.
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Snippet A new technique for the evaluation of local interface adhesion energy was applied to the interface between Cu and cap layer in a Cu damascene interconnect...
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StartPage 354
SubjectTerms Cu Grain
Local Interface Adhesion Strength
LSI Interconnect
Specimen Size Effect
Title Specimen Size Effect of Interface Strength Distribution Induced by Grain Structure of Cu Line
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