Microwave-assisted synthesis of α-hydroxy ketone and α-diketone and pyrazine derivatives from α-halo and α,α′-dibromo ketone
A novel reaction of α-halo ketone (α-bromo and α-chloro ketone) with irradiation under microwave gave the corresponding α-hydroxyketone and pyrazine derivative in good yields. In the case of α,α′-dibromo ketone, α-diketone was obtained. This reaction affords a new, clean and convenient synthetic met...
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| Published in | Tetrahedron letters Vol. 47; no. 52; pp. 9359 - 9364 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
OXFORD
Elsevier Ltd
25.12.2006
Elsevier |
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| Abstract | A novel reaction of α-halo ketone (α-bromo and α-chloro ketone) with irradiation under microwave gave the corresponding α-hydroxyketone and pyrazine derivative in good yields. In the case of α,α′-dibromo ketone, α-diketone was obtained. This reaction affords a new, clean and convenient synthetic method for α-hydroxyketone, α-diketone, α-chloro ketone and pyrazine derivative. |
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| AbstractList | A novel reaction of α-halo ketone (α-bromo and α-chloro ketone) with irradiation under microwave gave the corresponding α-hydroxyketone and pyrazine derivative in good yields. In the case of α,α′-dibromo ketone, α-diketone was obtained. This reaction affords a new, clean and convenient synthetic method for α-hydroxyketone, α-diketone, α-chloro ketone and pyrazine derivative. A novel reaction of alpha-halo ketone (alpha-bromo and alpha-chloro ketone) with irradiation under microwave gave the corresponding alpha-hydroxyketone and pyrazine derivative in good yields. In the case of alpha,alpha'-dibromo ketone, alpha-diketone was obtained. This reaction affords a new, clean and convenient synthetic method for alpha-hydroxyketone, alpha-diketone, alpha-chloro ketone and pyrazine derivative. (c) 2006 Elsevier Ltd. All rights reserved. |
| Author | Watanabe, Masashige Akira Horiuchi, C. Nakamura, Hiroaki Utsukihara, Takamitsu |
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| CitedBy_id | crossref_primary_10_1016_j_molstruc_2021_130492 crossref_primary_10_1039_C7RA11529F crossref_primary_10_1021_bm101272g crossref_primary_10_1039_c3ob41164h crossref_primary_10_1002_anie_201105876 crossref_primary_10_1002_chin_200714041 crossref_primary_10_1016_j_cclet_2007_10_022 crossref_primary_10_1021_jo300313v crossref_primary_10_1039_C4RA01043D crossref_primary_10_1080_00397911_2013_827208 crossref_primary_10_1021_acs_iecr_7b03824 crossref_primary_10_1021_acscatal_8b02208 crossref_primary_10_1002_jhet_5570450241 crossref_primary_10_1016_j_tetlet_2014_07_074 crossref_primary_10_1016_j_molcatb_2006_12_001 crossref_primary_10_1016_j_tet_2017_09_013 crossref_primary_10_1021_jm300281x crossref_primary_10_1080_17415990801959060 crossref_primary_10_1016_j_tet_2008_06_080 crossref_primary_10_1002_ange_201105876 crossref_primary_10_1002_ejoc_201403237 crossref_primary_10_1080_00397910802632589 crossref_primary_10_1002_ajoc_202100249 crossref_primary_10_1021_acs_orglett_6b02322 crossref_primary_10_1021_acs_joc_6b03032 |
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| Keywords | OXIDATION PHOTOIRRADIATION REDUCTION SILYL ENOL ETHERS CARBONYL-COMPOUNDS IODINATION STEP SYNTHESIS TITANIUM AZIDO KETONES METAL PEROXIDE REACTIONS |
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| Snippet | A novel reaction of α-halo ketone (α-bromo and α-chloro ketone) with irradiation under microwave gave the corresponding α-hydroxyketone and pyrazine derivative... A novel reaction of alpha-halo ketone (alpha-bromo and alpha-chloro ketone) with irradiation under microwave gave the corresponding alpha-hydroxyketone and... |
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| Title | Microwave-assisted synthesis of α-hydroxy ketone and α-diketone and pyrazine derivatives from α-halo and α,α′-dibromo ketone |
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